Plastics — Simple heat release test using a conical radiant heater and a thermopile detector

This document specifies a method suitable for the production control or product development purposes for assessing the heat release rate of essentially flat products exposed in the horizontal orientation to controlled levels of radiant heating with an external igniter. The heat release rate is determined by the use of a thermopile instead of the more accurate oxygen consumption techniques. The time to ignition and sustained flaming are also measured in this test. The mass loss of the test specimen can also be measured optionally.

Plastiques — Essai simple pour la détermination du débit calorifique au moyen d'un radiateur conique et d'une sonde à thermopile

Le présent document spécifie une méthode adaptée au contrôle de la production ou au développement de produit permettant l’évaluation du débit calorifique de produits essentiellement plats exposés suivant une orientation horizontale à des niveaux contrôlés de chaleur rayonnante, avec un dispositif d’allumage externe. Le débit calorifique est déterminé au moyen d’une thermopile plutôt qu’à l’aide de techniques plus précises de consommation d’oxygène. Le temps d’allumage et la flamme persistante sont aussi mesurés pendant cet essai. La perte de masse de l’éprouvette peut aussi être mesurée de manière facultative.

General Information

Status
Published
Publication Date
30-Aug-2023
Current Stage
6060 - International Standard published
Start Date
31-Aug-2023
Due Date
21-Sep-2023
Completion Date
31-Aug-2023
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ISO 13927:2023 - Plastics — Simple heat release test using a conical radiant heater and a thermopile detector Released:31. 08. 2023
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INTERNATIONAL ISO
STANDARD 13927
Third edition
2023-08
Plastics — Simple heat release test
using a conical radiant heater and a
thermopile detector
Plastiques — Essai simple pour la détermination du débit calorifique
au moyen d'un radiateur conique et d'une sonde à thermopile
Reference number
© ISO 2023
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting on
the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address below
or ISO’s member body in the country of the requester.
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Published in Switzerland
ii
Contents Page
Foreword .v
Introduction . vi
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Symbols . 2
5 Principle . 2
6 Apparatus . 2
6.1 General . 2
6.2 Cone-shaped radiant electrical heater . 4
6.3 Heat flux controller . 4
6.4 Chimney and thermopiles . . 5
6.5 Specimen holder . 5
6.6 Retainer frame . 5
6.7 Fume extraction system. 7
6.8 Ignition circuit . 8
6.9 Ignition timer . 8
6.10 Heat flux meter . 8
6.11 Calibration burner . 8
6.12 Data collection system . . 8
7 Suitability of a product for testing .10
7.1 Surface characteristics . 10
7.2 Asymmetrical products . 10
7.3 Thin materials . 10
7.4 Composite specimens . 10
7.5 Dimensionally unstable materials . 10
7.6 Materials that require testing under compression . 11
8 Specimen construction and preparation .12
8.1 Specimens .12
8.2 Conditioning of specimens .12
8.3 Preparation . 13
8.3.1 Specimen wrapping .13
8.3.2 Specimen preparation .13
8.3.3 Preparing specimens of materials that require testing under compression.13
9 Calibration .14
9.1 Heater calibration . 14
9.2 Thermopile calibration . 14
9.2.1 General . 14
9.2.2 Initial calibration . 14
9.2.3 Daily calibration . . .15
10 Test procedure .15
10.1 General precautions . 15
10.2 Initial preparation .15
10.3 Procedure . 16
11 Precision .16
12 Test report .16
Annex A (normative) Calibration of the heat flux meter .18
Annex B (informative) Guidance notes for operators .19
iii
Annex C (informative) Guidance on measuring mass loss during testing .20
Annex D (informative) Example of thermopile calibration — Relation of heat release and
thermopile output .21
Annex E (informative) Calculation of effective critical heat flux for ignition .23
Bibliography .24
iv
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.
ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular, the different approval criteria needed for the
different types of ISO document should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see www.iso.org/directives).
ISO draws attention to the possibility that the implementation of this document may involve the use
of (a) patent(s). ISO takes no position concerning the evidence, validity or applicability of any claimed
patent rights in respect thereof. As of the date of publication of this document, ISO had not received
notice of (a) patent(s) which may be required to implement this document. However, implementers are
cautioned that this may not represent the latest information, which may be obtained from the patent
database available at www.iso.org/patents. ISO shall not be held responsible for identifying any or all
such patent rights.
Any trade name used in this document is information given for the convenience of users and does not
constitute an endorsement.
For an explanation of the voluntary nature of standards, the meaning of ISO specific terms and
expressions related to conformity assessment, as well as information about ISO's adherence to
the World Trade Organization (WTO) principles in the Technical Barriers to Trade (TBT), see
www.iso.org/iso/foreword.html.
This document was prepared by Technical Committee ISO/TC 61, Plastics, Subcommittee SC 4, Burning
behaviour, in collaboration with the European Committee for Standardization (CEN) Technical
Committee CEN/TC 249, Plastics, in accordance with the Agreement on technical cooperation between
ISO and CEN (Vienna Agreement).
This third edition cancels and replaces the second edition (ISO 13927:2015), which has been technically
revised.
The main changes are as follows:
— the normative references have been updated to the latest editions (see Clause 2);
— use of mass flow rate of methane gas corresponding to the net heat of combustion for calibration of
the thermopile has been added in Clause 9;
— a new Annex D giving an example of thermopile calibration has been added and subsequent annex
has been renamed as Annex E.
Any feedback or questions on this document should be directed to the user’s national standards body. A
complete listing of these bodies can be found at www.iso.org/members.html.
v
Introduction
...

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