SIST EN 15691:2009

Ethanol as a blending component for gasoline - Determination of total dry residue (involatile material) - Gravimetric method

This European Standard specifies a procedure for the determination of dry residue in ethanol by desiccation method in the range 0,1 to 1 % m/V. The total dry residue or total dry matter includes all matter that is non-volatile under specified physical conditions.

Ethanol zur Verwendung als Blendkomponente in Ottokraftstoff - Bestimmung des gesamten Trockenrückstandes (nichtflüchtige Bestandteile) - Gravimetrisches Verfahren

Diese Europäische Norm legt ein Verfahren zur Bestimmung des gesamten Trockenrückstandes im Bereich
von 10 mg/100 ml bis 25 mg/100 ml fest. Die gravimetrische Bestimmung erfolgt durch Trocknung.
ANMERKUNG Das in einem Ringversuch [2] beschriebene Prüfverfahren wurde bis herab zu 3,5 mg/100 ml geprüft.
Dabei hat sich jedoch eine ungenügende Präzision ergeben.
WARNUNG - Die Anwendung dieses Dokuments kann den Einsatz gefährlicher Stoffe, Arbeitsgänge
und Geräte mit sich bringen. Diese Norm gibt nicht vor, alle mit ihrer Anwendung verbundenen
Sicherheitsprobleme anzusprechen. Der Anwender dieser Norm ist dafür verantwortlich, vorher
angemessene Maßnahmen zu ergreifen und die Anwendbarkeit einschränkender Vorschriften zu
ermitteln.

Ethanol comme constituant d'essence - Détermination de la residue totale (matérial involatil) - Méthode gravimetrique

La présente Norme européenne prescrit une méthode pour la mesure de la teneur en résidu sec de l'éthanol,
dans un domaine allant de (10 à 25) mg/100 ml, le résidu étant obtenu par méthode gravimétrique
(dessiccation).
NOTE Au cours d’une étude interlaboratoires [2], la méthode décrite a été testée sur de plus faibles quantités, avec
un minimum de 3,5 mg/100 ml, mais la fidélité s’avère insuffisante à de tels niveaux.
AVERTISSEMENT — L'utilisation du présent document peut impliquer l'intervention de produits,
d'opérations et d'équipements à caractère dangereux. La présente norme européenne n'est pas
censée aborder tous les problèmes de sécurité concernés par son usage. Il est de la responsabilité de
l'utilisateur de consulter et d'établir des règles de sécurité et d'hygiène appropriées et de déterminer
l'applicabilité des restrictions réglementaires avant utilisation.

Etanol kot komponenta za dodajanje motornemu bencinu - Določevanje celotnega suhega ostanka (nehlapna snov) - Gravimetrična metoda

General Information

• Status: Withdrawn
• Public Enquiry End Date: 29-Nov-2007
• Publication Date: 06-May-2009
• Withdrawal Date: 28-Jun-2023
• ICS: 71.080.60 - Alcohols. Ethers
• ICS: 75.160.20 - Liquid fuels
• Technical Committee: NAD - Petroleum products, lubricants and related products
• Current Stage: 9900 - Withdrawal (Adopted Project)
• Start Date: 28-Jun-2023
• Due Date: 21-Jul-2023
• Completion Date: 29-Jun-2023
• Ref Project: EN 15691:2009 - Ethanol as a blending component for petrol - Determination of dry residue (involatile material) - Gravimetric method

Relations

• Replaced By: SIST EN 15691:2023 - Ethanol as a blending component for petrol - Determination of dry residue (involatile material) - Gravimetric method
• Effective Date: 01-Sep-2023

Standards Content (Sample)

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Ethanol zur Verwendung als Blendkomponente in Ottokraftstoff - Bestimmung des gesamten Trockenrückstandes (nichtflüchtige Bestandteile) - Gravimetrisches VerfahrenEthanol comme constituant d'essence - Détermination de la residue totale (matérial involatil) - Méthode gravimetriqueEthanol as a blending component for gasoline - Determination of total dry residue (involatile material) - Gravimetric method75.160.20Liquid fuels71.080.60Alkoholi. EtriAlcohols. EthersICS:Ta slovenski standard je istoveten z:EN 15691:2009SIST EN 15691:2009en,fr,de01-junij-2009SIST EN 15691:2009SLOVENSKI
STANDARD



SIST EN 15691:2009



EUROPEAN STANDARDNORME EUROPÉENNEEUROPÄISCHE NORMEN 15691March 2009ICS 75.160.20 English VersionEthanol as a blending component for petrol - Determination ofdry residue (involatile material) - Gravimetric methodEthanol comme base de mélange à l'essence -Détermination du résidu sec (produits non volatils) -Méthode gravimétriqueEthanol zur Verwendung als Blendkomponente inOttokraftstoff - Bestimmung des Trockenrückstandes(nichtflüchtige Bestandteile) - Gravimetrisches VerfahrenThis European Standard was approved by CEN on 24 January 2009.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained on application to the CEN Management Centre or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as theofficial versions.CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland,France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMITÉ EUROPÉEN DE NORMALISATIONEUROPÄISCHES KOMITEE FÜR NORMUNGManagement Centre:
Avenue Marnix 17,
B-1000 Brussels© 2009 CENAll rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN 15691:2009: ESIST EN 15691:2009



EN 15691:2009 (E) 2 Contents Page Foreword .31Scope .42Normative references .43Principle .44Apparatus .45Sampling .45.1Preparation of samples .45.2Verification and quality control .56Procedure .57Calculation .58Expression of results .59Precision .59.1General .59.2Repeatability, r .69.3Reproducibility, R .610Test report .6Bibliography .7 SIST EN 15691:2009



EN 15691:2009 (E) 3 Foreword This document (EN 15691:2009) has been prepared by Technical Committee CEN/TC 19 “Gaseous and liquid fuels, lubricants and related products of petroleum, synthetic and biological origin”, the secretariat of which is held by NEN. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by September 2009, and conflicting national standards shall be withdrawn at the latest by September 2009. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN [and/or CENELEC] shall not be held responsible for identifying any or all such patent rights. This document was prepared by CEN/TC 19’s Ethanol Task Force under responsibility of its Working Group 21 and is based on a test method mentioned in a European Wine Regulation [1]. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg,
...

SLOVENSKI STANDARD
oSIST prEN 15691:2007
01-november-2007
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VXKHJDRVWDQNDQHKODSQDVQRY*UDYLPHWULþQDPHWRGD
Ethanol as a blending component for gasoline - Determination of total dry residue
(involatile material) - Gravimetric method
Ethanol zur Verwendung als Blendkomponente in Ottokraftstoff - Bestimmung des
gesamten Trockenrückstandes (nichtflüchtige Bestandteile) - Gravimetrisches Verfahren
Ethanol comme constituant d'essence - Détermination de la residue totale (matérial
involatil) - Méthode gravimetrique
Ta slovenski standard je istoveten z: prEN 15691
ICS:
75.160.20 7HNRþDJRULYD Liquid fuels
oSIST prEN 15691:2007 en
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------
EUROPEAN STANDARD
DRAFT
prEN 15691
NORME EUROPÉENNE
EUROPÄISCHE NORM
May 2007
ICS 75.160.20

English Version
Ethanol as a blending component for petrol - Determination of
total dry residue (involatile material) - Gravimetric method
Ethanol comme constituant d'essence - Détermination de la Ethanol zur Verwendung als Blendkomponente in
residue totale (matérial involatil) - Méthode gravimetrique Ottokraftstoff - Bestimmung des gesamten
Trockenrückstandes (nichtflüchtige Bestandteile) -
Gravimetrisches Verfahren
This draft European Standard is submitted to CEN members for enquiry. It has been drawn up by the Technical Committee CEN/TC 19.
If this draft becomes a European Standard, CEN members are bound to comply with the CEN/CENELEC Internal Regulations which
stipulate the conditions for giving this European Standard the status of a national standard without any alteration.
This draft European Standard was established by CEN in three official versions (English, French, German). A version in any other language
made by translation under the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the
same status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland,
France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,
Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.
Recipients of this draft are invited to submit, with their comments, notification of any relevant patent rights of which they are aware and to
provide supporting documentation.
Warning : This document is not a European Standard. It is distributed for review and comments. It is subject to change without notice and
shall not be referred to as a European Standard.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
Management Centre: rue de Stassart, 36  B-1050 Brussels
© 2007 CEN All rights of exploitation in any form and by any means reserved Ref. No. prEN 15691:2007: E
worldwide for CEN national Members.

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prEN 15691:2007 (E)
Contents Page
Foreword.3
1 Scope.4
2 Principle.4
3 Apparatus.4
4 Sampling.4
4.1 Preparation of samples .4
4.2 Quality control.5
5 Procedure.5
6 Calculation.5
7 Expression of results.5
8 Precision.5
8.1 General.5
8.2 Repeatability, r .6
8.3 Reproducibility, R .6
9 Test report.6
Bibliography .7

2

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prEN 15691:2007 (E)
Foreword
This document (prEN 15691:2007) has been prepared by Technical Committee CEN/TC 19 “Gaseous and
liquid fuels, lubricants and related products of petroleum, synthetic and biological origin”, the secretariat of
which is held by NEN.
This document is currently submitted to the CEN Enquiry.
This document was prepared by CEN/TC 19’s Ethanol Task Force under its Working Group 21 and is based
on a test method ment
...