Bitumen and bituminous binders - Determination of adhesivity of bituminous emulsions by water immersion test

This document specifies a method for determining the adhesion of a bituminous emulsion coated onto aggregate when immersed in water.
The method considers two different aspects of adhesivity, i.e. immediate adhesivity and water effect on binder adhesion.
The method may be used with a reference aggregate. In that case, it measures the intrinsic adhesion behaviour of a bituminous emulsion. The method may also be used with a specific aggregate as used on a job site.
WARNING -The use of this document may involve hazardous materials, operations and equipment. This document does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this document to establish appropriate safety and health practices and to determine the applicability of regulatory limitations prior to use.

Bitumen und bitumenhaltige Bindemittel - Bestimmung des Haftverhaltens von Bitumenemulsionen bei Wasserlagerung

Dieses Dokument legt ein Verfahren zur Bestimmung der Haftung eines Bindemittelüberzuges aus Bitumenemulsion an Gesteinskörnung bei Wasserlagerung fest.
Das Verfahren berücksichtigt zwei verschiedene Aspekte des Haftverhaltens, d. h. das unmittelbare Haft-verhalten und die Wirkung von Wasser auf die Haftung des Bindemittels.
Das Verfahren kann mit einer Referenz Gesteinskörnung angewendet werden. In diesem Falle misst es das eigentliche Haftungsverhalten einer Bitumenemulsion. Das Verfahren kann ebenso mit einer spezifischen Gesteinskörnung angewendet werden, wie sie auch auf einer Baustelle verwendet wird.
WARNUNG — Die Anwendung dieses Dokuments kann gefährliche Substanzen, Arbeitsgänge und Ausrüstung einschließen. In diesem Dokument werden nicht alle Sicherheitsprobleme angesprochen, die mit seiner Anwendung verbunden sind. Es liegt in der Verantwortung des Anwenders dieses Dokuments, geeignete Sicherheits  und Gesundheitsschutzmaßnahmen vorzusehen und vorher zu klären, ob einschränkende Vorschriften zu berücksichtigen sind.

Bitumes et liants bitumineux - Détermination de l'adhésivité des émulsions de bitume par l'essai d'immersion dans l'eau

Le présent document décrit une méthode permettant de déterminer les propriétés d’adhésion d’une émulsion bitumieuse bitume vis-à-vis de granulats, en immersion dans l’eau.
La méthode prend en compte deux aspects distincts de l'adhésivité, à savoir l'adhésivité immédiate et l'effet de l'eau sur l'adhésion du liant.
La méthode peut être mise en oeuvre avec un granulat de référence. Dans ce cas, elle mesure l’aptitude à l’adhésivité intrinsèque de l’émulsion bitumieuse. La méthode peut également être mise en oeuvre avec un granulat spécifique utilisé sur chantier.
AVERTISSEMENT - L'utilisation de ce document implique l'intervention de produits, d'opérations et d'équipements à caractère dangereux. Le présent document n'est pas censé aborder tous les problèmes de sécurité concernés par son usage. Il est de la responsabilité de l'utilisateur de ce document de consulter et d'établir des règles de sécurité et d'hygiène appropriées et de déterminer l'applicabilité des restrictions réglementaires avant utilisation.

Bitumen in bitumenska veziva - Določanje adhezije bitumenskih emulzij s preskusom potapljanja v vodo

General Information

Status
Published
Public Enquiry End Date
19-Dec-2019
Publication Date
18-May-2021
Technical Committee
Current Stage
6060 - National Implementation/Publication (Adopted Project)
Start Date
07-Apr-2021
Due Date
12-Jun-2021
Completion Date
19-May-2021

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SLOVENSKI STANDARD
SIST EN 13614:2021
01-julij-2021
Nadomešča:
SIST EN 13614:2011
Bitumen in bitumenska veziva - Določanje adhezije bitumenskih emulzij s
preskusom potapljanja v vodo

Bitumen and bituminous binders - Determination of adhesivity of bituminous emulsions

by water immersion test
Bitumen und bitumenhaltige Bindemittel - Bestimmung des Haftverhaltens von
Bitumenemulsionen bei Wasserlagerung

Bitumes et liants bitumineux - Détermination de l'adhésivité des émulsions de bitume par

l'essai d'immersion dans l'eau
Ta slovenski standard je istoveten z: EN 13614:2021
ICS:
75.140 Voski, bitumni in drugi naftni Waxes, bituminous materials
proizvodi and other petroleum products
91.100.50 Veziva. Tesnilni materiali Binders. Sealing materials
SIST EN 13614:2021 en,fr,de

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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SIST EN 13614:2021
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SIST EN 13614:2021
EN 13614
EUROPEAN STANDARD
NORME EUROPÉENNE
March 2021
EUROPÄISCHE NORM
ICS 75.140; 91.100.50 Supersedes EN 13614:2011
English Version
Bitumen and bituminous binders - Determination of
adhesivity of bituminous emulsions by water immersion
test

Bitumes et liants bitumineux - Détermination de Bitumen und bitumenhaltige Bindemittel -

l'adhésivité des émulsions bitumineuses par l'essai Bestimmung des Haftverhaltens von

d'immersion dans l'eau Bitumenemulsionen bei Wasserlagerung
This European Standard was approved by CEN on 1 March 2021.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this

European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references

concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN

member.

This European Standard exists in three official versions (English, French, German). A version in any other language made by

translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management

Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,

Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,

Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and

United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels

© 2021 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN 13614:2021 E

worldwide for CEN national Members.
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SIST EN 13614:2021
EN 13614:2021 (E)
Contents Page

European foreword ....................................................................................................................................................... 3

1 Scope .................................................................................................................................................................... 4

2 Normative references .................................................................................................................................... 4

3 Terms and definitions ................................................................................................................................... 4

4 Principle ............................................................................................................................................................. 5

5 Reagents and materials ................................................................................................................................. 5

6 Apparatus ........................................................................................................................................................... 5

7 Sampling ............................................................................................................................................................. 6

8 Procedure........................................................................................................................................................... 6

8.1 General ................................................................................................................................................................ 6

8.2 Determination of immediate adhesivity ................................................................................................. 6

8.3 Water effect on binder adhesion ............................................................................................................... 7

8.3.1 General ................................................................................................................................................................ 7

9 Expression of results ...................................................................................................................................... 7

10 Precision ............................................................................................................................................................. 8

11 Test report ......................................................................................................................................................... 8

Annex A (informative) Guidance for the marking of coated surface area ................................................. 9

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SIST EN 13614:2021
EN 13614:2021 (E)
European foreword

This document (EN 13614:2021) has been prepared by Technical Committee CEN/TC 336 “Bituminous

binders”, the secretariat of which is held by AFNOR.

This European Standard shall be given the status of a national standard, either by publication of an

identical text or by endorsement, at the latest by September 2021, and conflicting national standards shall

be withdrawn at the latest by September 2021.

Attention is drawn to the possibility that some of the elements of this document may be the subject of

patent rights. CEN shall not be held responsible for identifying any or all such patent rights.

This document supersedes EN 13614:2011.
The main changes with respect to the previous edition are listed below:

— curing and conditioning the coated aggregates within a heat resistant glass dish in the form of a

monolayer of materials instead of placing them into a beaker (8.2.4 and 8.3.5);

— making the assessment under water, which can be replaced if dirty, with the help of an appropriate

desk lamp (8.2.5 and 8.3.7);

— no requirements for a specific thermometer (6.9) since room temperature can be checked with

ordinary means. After drying, aggregates are to be left to cool down to room temperature before

starting the test procedure (8.1 and 8.3.1);

— acceptable tolerance on conditioning time (8.3.6) is reduced from ± 4 h to ± 2 h;

— guidance for the marking of covered surface area (Annex A) is improved by complementing the

sketches with actual pictures.

According to the CEN-CENELEC Internal Regulations, the national standards organisations of the

following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia,

Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland,

Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Republic of North

Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United

Kingdom.
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SIST EN 13614:2021
EN 13614:2021 (E)
1 Scope

This document specifies a method for determining the adhesion of a bituminous emulsion coated onto

aggregate when immersed in water.

The method considers two different aspects of adhesivity, i.e. immediate adhesivity and water effect on

binder adhesion.

The method may be used with a reference aggregate. In that case, it measures the intrinsic adhesion

behaviour of a bituminous emulsion. The method may also be used with a specific aggregate as used on a

job site.

WARNING — The use of this document may involve hazardous materials, operations and equipment.

This document does not purport to address all of the safety problems associated with its use. It is the

responsibility of the user of this document to establish appropriate safety and health practices and to

determine the applicability of regulatory limitations prior to use.
2 Normative references

The following documents are referred to in the text in such a way that some or all of their content

constitutes requirements of this document. For dated references, only the edition cited applies. For

undated references, the latest edition of the referenced document (including any amendments) applies.

EN 58, Bitumen and bituminous binders — Sampling bituminous binders
EN 12594, Bitumen and bituminous binders — Preparation of test samples

EN 13043, Aggregates for bituminous mixtures and surface treatments for roads, airfields and other

trafficked areas

EN 13808, Bitumen and bituminous binders — Framework for specifying cationic bituminous emulsions

EN 1428, Bitumen and bituminous binders — Determination of water content in bituminous emulsions —

Azeotropic distillation method

EN 1431, Bitumen and bituminous binders — Determination of residual binder and oil distillate from

bitumen emulsions by distillation

EN 16849, Bitumen and bituminous binders — Determination of water content in bituminous emulsions —

Method using a drying balance

EN ISO 3696, Water for analytical laboratory use — Specification and test methods (ISO 3696)

3 Terms and definitions
For the purposes of this document, the following terms and definitions apply.

ISO and IEC maintain terminological databases for use in standardization at the following addresses:

— IEC Electropedia: available at http://www.electropedia.org/
— ISO Online browsing platform: available at https://www.iso.org/obp
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SIST EN 13614:2021
EN 13614:2021 (E)
3.1
adhesion

ability of a binder to coat the surface of an aggregate and to remain bonded over time in the presence of

water
3.2
adhesivity
qualitative assessment of the measurement of the adhesion
3.3
immediate adhesivity

qualitative assessment of the ability of the binder from a bituminous emulsion to resist the action of water

just after coating of the aggregate
3.4
water effect on binder adhesion
qualitative assessment of the
...

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