Paper and board - Paper and board intended to come into contact with foodstuffs - Determination of aluminium in aqueous extracts

This document specifies a test method for the determination of aluminium in aqueous extracts.
It is applicable to paper and board with extractable aluminium content of at least 0,2 mg/l.
Aluminium extract levels below those given can be measured using this document if sensitive equipment is available and if all other laboratory conditions fulfil the requirements for trace element analysis.

Papier und Pappe - Papier und Pappe für den Kontakt mit Lebensmitteln - Bestimmung von Aluminium in wässrigen Extrakten

Dieses Dokument legt ein Prüfverfahren für die Bestimmung von Aluminium in wässrigen Extrakten fest.
Es ist anwendbar für Papier und Pappe mit einem extrahierbaren Aluminiumgehalt von mindestens 0,2 mg/l.
Niedrigere Extraktgehalte an Aluminium können unter Anwendung dieses Dokuments gemessen werden, wenn empfindliche Geräte zur Verfügung stehen und alle anderen Laboratoriumsbedingungen die Anforderungen für die Spurenelementanalyse erfüllen.

Papier et carton - Papiers et cartons destinés à entrer en contact avec les denrées alimentaires - Détermination de l’aluminium dans un extrait aqueux

Le présent document spécifie une méthode d'essai pour la détermination de l’aluminium dans des extraits aqueux.
Il est applicable aux papiers et cartons dont la teneur en aluminium extractible est d’au moins 0,2 mg/l.
Des teneurs en extrait d’aluminium inférieures à celles indiquées peuvent être mesurées en suivant le présent document si un appareillage sensible est disponible et si toutes les autres conditions dans le laboratoire satisfont aux exigences de l’analyse des éléments à l’état de traces.

Papir, karton in lepenka - Papir, karton in lepenka, namenjeni neposrednemu stiku z živili - Ugotavljanje aluminija v vodnih ekstraktih

Ta dokument določa preskusno metodo za ugotavljanje aluminija v vodnih ekstraktih. Uporablja se za papir, karton in lepenko z vsebnostjo aluminija, ki ga je mogoče ekstrahirati, vsaj 0,2 mg/l.
Stopnje ekstrahiranega aluminija pod navedeno vrednostjo je mogoče izmeriti z uporabo tega dokumenta, če je na voljo občutljiva oprema in če vsi drugi laboratorijski pogoji izpolnjujejo zahteve za analizo elementov v sledeh.

General Information

Status
Published
Public Enquiry End Date
10-Jan-2023
Publication Date
12-Feb-2024
Current Stage
6060 - National Implementation/Publication (Adopted Project)
Start Date
24-Jan-2024
Due Date
30-Mar-2024
Completion Date
13-Feb-2024

Overview

EN 17917:2023 - Paper and board intended to come into contact with foodstuffs - Determination of aluminium in aqueous extracts - defines a laboratory test method to quantify aluminium (Al) released from paper and board into aqueous extracts. The method is intended for materials with extractable aluminium at or above 0.2 mg/L, although lower levels can be measured with suitably sensitive instrumentation and trace-analysis conditions.

Key topics and requirements

  • Scope: Applies to cold or hot aqueous extracts prepared according to EN 645 (cold) or EN 647 (hot).
  • Analytical principle: Determination by ICP‑OES (inductively coupled plasma optical emission spectrometry) or ICP‑MS; graphite‑furnace AAS allowed if validated.
  • Sample prep: Filter extracts (0.45 µm membrane), stabilize with nitric acid (1.0 mL HNO3 per 100 mL extract).
  • Reagents & lab grade: Use water grade 1 per EN ISO 3696 and trace‑element‑grade reagents; washware with dilute nitric acid to reduce blanks.
  • Calibration: Prepare calibration solutions covering measured range (example 0.2–5 mg/L). Include calibration blank and account for blank values from reagents and equipment.
  • Instrument settings: Suggested ICP‑OES wavelengths: 396.152, 308.215, 237.312 nm. For ICP‑MS measure isotope 27Al.
  • Quality control: Run certified reference materials, monitor blanks, match acid concentrations between samples and standards, avoid contamination/adsorption.
  • Results expression: Calculate mg/L of extract while correcting for blank, sample moisture content and sample mass. Include required information in test report.

Practical applications and users

  • Food contact compliance testing: Laboratories verifying paper and board meet safety requirements for food packaging and food-contact articles.
  • Packaging manufacturers and converters: Routine quality control of incoming paper/board materials and finished packaging to monitor extractable aluminium.
  • Regulatory bodies and auditors: Evaluation of material safety and conformity with national/EU food contact legislation.
  • R&D and supplier qualification: Assess effects of coatings, additives or recycling streams on aluminium extractability.

Related standards

  • EN 645 - Preparation of a cold water extract (paper and board)
  • EN 647 - Preparation of a hot water extract (paper and board)
  • EN ISO 3696 - Water for analytical laboratory use
  • ISO GUIDE 30 - Reference materials terminology

Keywords: EN 17917:2023, aluminium determination, paper and board, food contact materials, aqueous extracts, ICP‑OES, ICP‑MS, aluminium testing, extractable aluminium.

Standard
SIST EN 17917:2024
English language
8 pages
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Frequently Asked Questions

SIST EN 17917:2024 is a standard published by the Slovenian Institute for Standardization (SIST). Its full title is "Paper and board - Paper and board intended to come into contact with foodstuffs - Determination of aluminium in aqueous extracts". This standard covers: This document specifies a test method for the determination of aluminium in aqueous extracts. It is applicable to paper and board with extractable aluminium content of at least 0,2 mg/l. Aluminium extract levels below those given can be measured using this document if sensitive equipment is available and if all other laboratory conditions fulfil the requirements for trace element analysis.

This document specifies a test method for the determination of aluminium in aqueous extracts. It is applicable to paper and board with extractable aluminium content of at least 0,2 mg/l. Aluminium extract levels below those given can be measured using this document if sensitive equipment is available and if all other laboratory conditions fulfil the requirements for trace element analysis.

SIST EN 17917:2024 is classified under the following ICS (International Classification for Standards) categories: 67.250 - Materials and articles in contact with foodstuffs; 85.060 - Paper and board. The ICS classification helps identify the subject area and facilitates finding related standards.

You can purchase SIST EN 17917:2024 directly from iTeh Standards. The document is available in PDF format and is delivered instantly after payment. Add the standard to your cart and complete the secure checkout process. iTeh Standards is an authorized distributor of SIST standards.

Standards Content (Sample)


SLOVENSKI STANDARD
01-marec-2024
Papir, karton in lepenka - Papir, karton in lepenka, namenjeni neposrednemu stiku
z živili - Ugotavljanje aluminija v vodnih ekstraktih
Paper and board - Paper and board intended to come into contact with foodstuffs -
Determination of aluminium in aqueous extracts
Papier und Pappe - Papier und Pappe für den Kontakt mit Lebensmitteln - Bestimmung
von Aluminium in wässrigen Extrakten
Papier et carton - Papiers et cartons destinés à entrer en contact avec les denrées
alimentaires - Détermination de l’aluminium dans un extrait aqueux
Ta slovenski standard je istoveten z: EN 17917:2023
ICS:
67.250 Materiali in predmeti v stiku z Materials and articles in
živili contact with foodstuffs
85.060 Papir, karton in lepenka Paper and board
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

EN 17917
EUROPEAN STANDARD
NORME EUROPÉENNE
December 2023
EUROPÄISCHE NORM
ICS 67.250; 85.060
English Version
Paper and board - Paper and board intended to come into
contact with foodstuffs - Determination of aluminium in
aqueous extracts
Papier et carton - Papiers et cartons destinés à entrer Papier und Pappe - Papier und Pappe für den Kontakt
en contact avec les denrées alimentaires - mit Lebensmitteln - Bestimmung von Aluminium in
Détermination de l'aluminium dans un extrait aqueux wässrigen Extrakten
This European Standard was approved by CEN on 20 November 2023.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and
United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2023 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN 17917:2023 E
worldwide for CEN national Members.

Contents Page
European foreword . 3
1 Scope . 4
2 Normative references . 4
3 Terms and definitions . 4
4 Principle . 4
5 Reagents . 4
6 Apparatus . 5
7 Preparation of sample . 5
8 Procedure . 5
8.1 General. 5
8.2 Preparation of calibration solutions . 5
8.3 Determination of calibration blank . 5
8.4 Determination of aluminium . 5
8.4.1 General. 5
8.4.2 Suggested spectrometer settings . 6
8.4.3 Determination of blank value. 6
9 Expression of results . 6
10 Test report . 6
11 Precision . 7
Bibliography . 8

European foreword
This document (EN 17917:2023) has been prepared by Technical Committee CEN/TC 172 “Pulp, paper
and board”, the secretariat of which is held by DIN.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by June 2024, and conflicting national standards shall be
withdrawn at the latest by June 2024.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
This document is one in a series of standards for the determination of metals in aqueous extracts of paper
and board intended for contact with food.
Any feedback and questions on this document should be directed to the users’ national standards body.
A complete listing of these bodies can be found on the CEN website.
According to the CEN-CENELEC Internal Regulations, the national standards organisations of the
following countries are bound to impl
...

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