Standard Guide for Deposition on Glassware During Mechanical Dishwashing

SIGNIFICANCE AND USE
3.1 This test method is intended as a laboratory screening test to determine performance of the detergent under actual use conditions, but will not necessarily predict performance under all end-use conditions.
SCOPE
1.1 This guide covers a procedure for measuring performance of a mechanical dishwashing detergent in terms of the buildup of spots and film on glassware. It is designed to evaluate household automatic dishwasher detergents but can be used as a screening test for institutional and commercial dishwashing products.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Publication Date
31-Dec-2022
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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D3556 − 23
Standard Guide for
1
Deposition on Glassware During Mechanical Dishwashing
This standard is issued under the fixed designation D3556; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 4.2 Clear Undecorated Glass Tumblers,from8to15per
machine, a larger number being used if it is planned to remove
1.1 This guide covers a procedure for measuring perfor-
one tumbler at intervals throughout the test (see Note 5 in
mance of a mechanical dishwashing detergent in terms of the
Section 6.7.3). Ten tumblers simplify scoring.
buildup of spots and film on glassware. It is designed to
4.2.1 Before each use, even if new, the glass tumblers may
evaluatehouseholdautomaticdishwasherdetergentsbutcanbe
be cleaned in a machine, first in a 1 % solution of citric acid
used as a screening test for institutional and commercial
and then with a household automatic dishwashing detergent at
dishwashing products.
the manufacturer’s recommended use level, each in a normal
1.2 This standard does not purport to address all of the
wash cycle. Use deionized or distilled water for the rinses
safety concerns, if any, associated with its use. It is the
during this cleaning procedure. Do not use the drying cycle of
responsibility of the user of this standard to establish appro-
the machine until the tumblers appear to be free of soil or film.
priate safety, health, and environmental practices and deter-
No “water break” (droplet formation) should be evident when
mine the applicability of regulatory limitations prior to use.
the tumblers have been rinsed.
1.3 This international standard was developed in accor-
4.3 Standard Tableware (Note 2) (optional, see Section 6):
dance with internationally recognized principles on standard-
4.3.1 Suggested tableware is as follows, Dinner plates,
ization established in the Decision on Principles for the
10 in.diameter,Saladplates,7 in.diameter,Cerealbowls,6 in.
Development of International Standards, Guides and Recom-
diameter, Saucers, 6 in. diameter, and Cutlery, stainless steel.
mendations issued by the World Trade Organization Technical
Barriers to Trade (TBT) Committee.
NOTE 1—A mixture of china and plastic dishes is recommended but is
not essential; any standard quality type of dishware is satisfactory.
2. Summary of Test Method
4.3.2 For each machine used, six dinner plates, six knives,
2.1 Glass tumblers are given multiple washes in a mechani-
six forks, and six spoons are required, plus optionally enough
cal dishwasher in the presence of food soil and the levels of
of the other dishes to fill the lower rack of each machine (see
spotting and filming allowed by the detergents under test are
Section 6).
compared visually.
4.4 Light Box for Visual Evaluation of Tumblers—A typical
light box is rectangular, open to the front, and has dead black
3. Significance and Use
insidesurfaces.Itislargeenoughtoholdupto15tumblersside
3.1 This test method is intended as a laboratory screening
by side. Fluorescent lights are mounted in the base of the box
test to determine performance of the detergent under actual use
in such a manner that light passes up through the tumblers. It
conditions, but will not necessarily predict performance under
is preferable to have the light come only through the tumblers
all end-use conditions.
and have the area surrounding them blocked out by suitable
means. Adding dividers between tumblers is also recom-
4. Apparatus
mended to aid in the assessment.
4.1 Automatic Dishwasher(s)—Typical household machines
should be selected. If more than one machine is required, pairs
5. Materials and Manufacture
with consecutive production numbers are recommended. For
2
5.1 Standard Food Soil Components: nonfat powdered
further refinement, two or more pairs of differing makes,
milk, margarine, and wheat-based cooked cereal (optional).
models, or ages (pair to pair) may be used.
5.2 Standard Food Soil Preparation—A mixture of 80
weight % of margarine and 20 weight % of powdered milk is
1
This guide is under the jurisdiction of ASTM Committee D12 on Soaps and
prepared.The margarine is warmed until fluid (not over 100 °F
Other Detergents, and is the direct responsibility of Subcommittee D12.16 on Hard
(37.8 °C)) and the powdered milk is sifted in and mixed
Surface Cleaning.
Current edition approved Jan. 1, 2023. Published January 2023. Originally
approved in 1976 as D3556–76 T. Last previous edition approved in 2014 as
2
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D3556 − 14 D3556 − 23
Standard Guide for
1
Deposition on Glassware During Mechanical Dishwashing
This standard is issued under the fixed designation D3556; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This guide covers a procedure for measuring performance of a mechanical dishwashing detergent in terms of the buildup of
spots and film on glassware. It is designed to evaluate household automatic dishwasher detergents but can be used as a screening
test for institutional and commercial dishwashing products.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety safety, health, and healthenvironmental practices and determine the
applicability of regulatory limitations prior to use.
1.3 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Summary of Test Method
2.1 Glass tumblers are given multiple washes in a mechanical dishwasher in the presence of food soil and the levels of spotting
and filming allowed by the detergents under test are compared visually.
3. Significance and Use
3.1 This test method is intended as a laboratory screening test to determine performance of the detergent under actual use
conditions, but will not necessarily predict performance under all end-use conditions.
4. Apparatus
4.1 Automatic Dishwasher(s)—Typical household machines should be selected. If more than one machine is required, pairs with
consecutive production numbers are recommended. For further refinement, two or more pairs of differing makes, models, or ages
(pair to pair) may be used.
4.2 Clear Undecorated Glass Tumblers, from 8 to 15 per machine, a larger number being used if it is planned to remove one
tumbler at intervals throughout the test (see Note 5 in Section 66.7.3). Ten tumblers simplify scoring.
4.2.1 Before each use, even if new, the glass tumblers may be cleaned in a machine, first in a 1 % solution of citric acid and then
with a household automatic dishwashing detergent at the manufacturer’s recommended use level, each in a normal wash cycle. Use
deionized or distilled water for the rinses during this cleaning procedure. Do not use the drying cycle of the machine until the
1
This guide is under the jurisdiction of ASTM Committee D12 on Soaps and Other Detergents, and is the direct responsibility of Subcommittee D12.16 on Hard Surface
Cleaning.
Current edition approved Nov. 1, 2014Jan. 1, 2023. Published December 2014 January 2023. Originally approved in 1976 as D3556–76 T. Last previous edition approved
in 20092014 as D3556–85(2009).D3556–14. DOI: 10.1520/D3556-14.10.1520/D3556-23.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

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D3556 − 23
tumblers appear to be free of soil or film. No “water break” (droplet formation) should be evident when the tumblers have been
rinsed. Any other procedure (such as hand washing and polishing) which yields tumblers that are spot- and film-free may be used.
4.3 Standard Tableware (Note 2) (optional, see Section 6):
4.3.1 Suggested tableware is as follows, Dinner plates, 10-in.10 in. diameter, Salad plates, 7-in.7 in. diameter, Cereal bowls,
6-in.6 in. diameter, Saucers, 6-in.6 in. diameter, and Cutlery, stainless steel.
NOTE 1—A mixture of china and plastic dishes is recommended but is not essential; any standard quality type of dishware is satisfactory.
4.3.2 For each machine used, six dinner plates, six knives, six forks, and six spoons are required, plus optionally enough of the
other dishes to fill the lower rack of each machine (see Section 6).
4.4 Light Box for Visual Evaluation of Tumblers—A typical light box is rectangular, open to the front, and has dead black inside
surfaces. It is large enough to hold up to 15 tumblers side by side. Fluorescent lights are mounted in the base of the box in such
a manner that light passes up through the tum
...

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