Standard Test Method for Distillation of Petroleum Products at Atmospheric Pressure

SCOPE
1.1 This test method covers the atmospheric distillation of petroleum products using a laboratory batch distillation unit to determine quantitatively the boiling range characteristics of such products as natural gasolines, light and middle distillates, automotive spark-ignition engine fuels, aviation gasolines, aviation turbine fuels, 1-D and 2-D regular and low sulfur diesel fuels, special petroleum spirits, naphthas, white spirits, kerosines, and Grades 1 and 2 burner fuels.
1.2 The test method is designed for the analysis of distillate fuels; it is not applicable to products containing appreciable quantities of residual material.
1.3 This test method covers both manual and automated instruments.
Note 1—Interlaboratory consensus test data have been obtained in the last few years under the CS92 program. The statistical equivalency between the manual and the automated procedure is currently under study, based on data from this program obtained between 1994 and 1998.
1.4 Unless otherwise noted, the values stated in SI units are to be regarded as the standard. The values given in parentheses are provided for information only.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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Publication Date
30-Apr-2004
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ASTM D86-04b - Standard Test Method for Distillation of Petroleum Products at Atmospheric Pressure
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
An American National Standard
Designation: D 86 – 04b
Standard Test Method for
1
Distillation of Petroleum Products at Atmospheric Pressure
ThisstandardisissuedunderthefixeddesignationD86;thenumberimmediatelyfollowingthedesignationindicatestheyearoforiginal
adoptionor,inthecaseofrevision,theyearoflastrevision.Anumberinparenthesesindicatestheyearoflastreapproval.Asuperscript
epsilon (e) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
2
1. Scope* 2.2 ASTM Standards:
D97 Test Method for Pour Point of Petroleum Products
1.1 This test method covers the atmospheric distillation of
D323 Test Method for Vapor Pressure of Petroleum Prod-
petroleum products using a laboratory batch distillation unit to
ucts (Reid Method)
determine quantitatively the boiling range characteristics of
D2892 Test Method for Distillation of Crude Petroleum
such products as natural gasolines, light and middle distillates,
(15-Theoretical Plate Column)
automotive spark-ignition engine fuels, aviation gasolines,
D4057 Practice for Manual Sampling of Petroleum and
aviation turbine fuels, 1-D and 2-D regular and low sulfur
Petroleum Products
diesel fuels, special petroleum spirits, naphthas, white spirits,
D4177 Practice for Automatic Sampling of Petroleum and
kerosines, and Grades 1 and 2 burner fuels.
Petroleum Products
1.2 The test method is designed for the analysis of distillate
D4953 Test Method for Vapor Pressure of Gasoline and
fuels; it is not applicable to products containing appreciable
Gasoline-Oxygenate Blends (Dry Method)
quantities of residual material.
D5190 Test Method forVapor Pressure of Petroleum Prod-
1.3 This test method covers both manual and automated
ucts (Automatic Method)
instruments.
D5191 Test Method forVapor Pressure of Petroleum Prod-
NOTE 1—Interlaboratory consensus test data have been obtained in the
ucts (Mini Method)
last few years under the CS92 program. The statistical equivalency
D5482 Test Method forVapor Pressure of Petroleum Prod-
betweenthemanualandtheautomatedprocedureiscurrentlyunderstudy,
ucts (Mini Method-Atmospheric)
based on data from this program obtained between 1994 and 1998.
D5949 Test Method for Pour Point of Petroleum Products
1.4 Unless otherwise noted, the values stated in SI units are
(Automatic Pressure Pulsing Method)
toberegardedasthestandard.Thevaluesgiveninparentheses
D5950 Test Method for Pour Point of Petroleum Products
are provided for information only.
(Automatic Tilt Method)
1.5 This standard does not purport to address all of the
D5985 Test Method for Pour Point of Petroleum Products
safety concerns, if any, associated with its use. It is the
(Rotational Method)
responsibility of the user of this standard to establish appro-
E1 Specification forASTM Liquid-in-GlassThermometers
priate safety and health practices and determine the applica-
E77 Test Method for Inspection and Verification of Ther-
bility of regulatory limitations prior to use.
mometers
E1272 Specification for Laboratory Glass Graduated Cyl-
2. Referenced Documents
inders
2.1 All standards are subject to revision, and parties to
E 1405 Specification for Laboratory Glass Distillation
agreement on this test method are to apply the most recent
Flasks
edition of the standards indicated below, unless otherwise
3
2.3 Energy Institute Standards:
specified,suchasincontractualagreementsorregulatoryrules
IP 69 Determination of Vapour Pressure—Reid Method
where earlier versions of the method(s) identified may be
IP 123 Petroleum Products—Determination of Distillation
required.
Characteristics
IP 394 Determination of Air Saturated Vapour Pressure
1
This test method is under the jurisdiction of ASTM Committee D02 on
Petroleum Products and Lubricants and is the direct responsibility of Subcommittee 2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
D02.08 on Volatility.
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
In the IP, the equivalent test method is published under the designation IP123.
Standards volume information, refer to the standard’s Document Summary page on
It is under the jurisdiction of the Standardization Committee.
the ASTM website.
Current edition approved May 1, 2004. Published June 2004. Originally
3
Available from the Energy Institute, 61 New Cavendish St., London, W1G
approved in 1921. Last previous edition approved in 2004 as D86-04a.
7AR, UK.
*A Summary of Changes section appears at the end of this standard.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
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D86–04b
IP Standard Methods forAnalysis and Testing of Petroleum a lower temperature than the immersed portion, resulti
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