Standard Test Method for Sediment in Crude Oils and Fuel Oils by the Extraction Method

SIGNIFICANCE AND USE
5.1 A knowledge of the sediment content of crude oils and fuel oils is important both to the operation of refining and the buying or selling of these commodities.
SCOPE
1.1 This test method covers the determination of sediment in crude oils and fuel oils by extraction with toluene. The precision applies to a range of sediment levels from 0.01 % to 0.40 % mass, although higher levels may be determined.
Note 1: Precision on recycled oils and crankcase oils is unknown and additional testing is required to determine that precision.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see 6.1.1.6 and 7.1.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
30-Jun-2022
Current Stage
Ref Project

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Standards Content (Sample)

This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D473 − 22
Manual of Petroleum Measurement Standards (MPMS), Chapter 10.1
Standard Test Method for
Sediment in Crude Oils and Fuel Oils by the Extraction
1
Method
This standard is issued under the fixed designation D473; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope* D4057Practice for Manual Sampling of Petroleum and
Petroleum Products (API MPMS Chapter 8.1)
1.1 This test method covers the determination of sediment
D4175Terminology Relating to Petroleum Products, Liquid
in crude oils and fuel oils by extraction with toluene. The
Fuels, and Lubricants
precision applies to a range of sediment levels from 0.01% to
D4177Practice for Automatic Sampling of Petroleum and
0.40% mass, although higher levels may be determined.
Petroleum Products (API MPMS Chapter 8.2)
NOTE 1—Precision on recycled oils and crankcase oils is unknown and
D5854Practice for Mixing and Handling of Liquid Samples
additional testing is required to determine that precision.
of Petroleum and Petroleum Products (API MPMS Chap-
1.2 The values stated in SI units are to be regarded as
ter 8.3)
standard. No other units of measurement are included in this
E29Practice for Using Significant Digits in Test Data to
standard.
Determine Conformance with Specifications
3
1.3 This standard does not purport to address all of the
2.2 API Standards:
safety concerns, if any, associated with its use. It is the
Chapter 1Terms and Definitions Database
responsibility of the user of this standard to establish appro-
Chapter 8.1Manual Sampling of Petroleum and Petroleum
priate safety, health, and environmental practices and deter-
Products (ASTM Practice D4057)
mine the applicability of regulatory limitations prior to use.
Chapter 8.2Automatic Sampling of Petroleum and Petro-
For specific warning statements, see 6.1.1.6 and 7.1.
leum Products (ASTM Practice D4177)
1.4 This international standard was developed in accor-
Chapter 8.3Mixing and Handling of Liquid Samples of
dance with internationally recognized principles on standard-
Petroleum and Petroleum Products (ASTM Practice
ization established in the Decision on Principles for the
D5854)
Development of International Standards, Guides and Recom- 4
2.3 ISO Standard:
mendations issued by the World Trade Organization Technical
5272 Toluene for industrial use—Specifications
Barriers to Trade (TBT) Committee.
3. Terminology
2. Referenced Documents
3.1 For definitions of terms used in this standard test
2
2.1 ASTM Standards:
method, refer to Terminology D4175 and the API MPMS
Chapter 1 Terms and Definitions Database.
1
This test method is under the jurisdiction of ASTM Committee D02 on
4. Summary of Test Method
Petroleum Products, Liquid Fuels, and Lubricants and the API Committee on
Petroleum Measurement, and is the direct responsibility of Subcommittee D02.02
4.1 Extract test portion of a representative oil sample,
/COMQ, the joint ASTM-API Committee on Hydrocarbon Measurement for
contained in a refractory thimble, with hot toluene until the
Custody Transfer (Joint ASTM-API). This test method has been approved by the
residue reaches constant mass.The mass of residue, calculated
sponsoring committees and accepted by the Cooperating Societies in accordance
with established procedures. as a percentage, is reported as sediment by extraction.
CurrenteditionapprovedJuly1,2022.PublishedJuly2022.Originallyapproved
ɛ1
in 1938. Last previous edition approved in 2017 as D473–07 (2017) . DOI:
10.1520/D0473-22.
2 3
For referenced ASTM standards, visit the ASTM website, www.astm.org, or Available from American Petroleum Institute (API), 1220 L. St., NW,
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Washington, DC 20005-4070, http://api-ec.api.org.
4
Standards volume information, refer to the standard’s Document Summary page on Available fromAmerican National Standards Institute (ANSI), 25 W. 43rd St.,
the ASTM website. 4th Floor, New York, NY 10036, http://www.ansi.org.
*A Summary of Changes section appears at the end of this standard
© Jointly copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, USA and the American Petroleum Institute (API), 1220 L Street NW, Washington DC 20005, USA
1

---------------------- Page: 1 ----------------------
D473 − 22
NOTE 1—Apparatus B shows the water cu
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
´1
Designation: D473 − 07 (Reapproved 2017) D473 − 22
Manual of Petroleum Measurement Standards (MPMS), Chapter 10.1
Standard Test Method for
Sediment in Crude Oils and Fuel Oils by the Extraction
1
Method
This standard is issued under the fixed designation D473; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1
ε NOTE—Footnote 1 was corrected editorially in August 2017.
1. Scope Scope*
1.1 This test method covers the determination of sediment in crude oils and fuel oils by extraction with toluene. The precision
applies to a range of sediment levels from 0.01 % to 0.40 % mass, although higher levels may be determined.
NOTE 1—Precision on recycled oils and crankcase oils is unknown and additional testing is required to determine that precision.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety safety, health, and healthenvironmental practices and determine the
applicability of regulatory limitations prior to use. For specific warning statements, see 5.1.1.66.1.1.6 and 6.17.1.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
D4057 Practice for Manual Sampling of Petroleum and Petroleum Products (API MPMS Chapter 8.1)
D4175 Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
D4177 Practice for Automatic Sampling of Petroleum and Petroleum Products (API MPMS Chapter 8.2)
D5854 Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products (API MPMS Chapter 8.3)
E29 Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
3
2.2 API Standards:
Chapter 1 Terms and Definitions Database
Chapter 8.1 Manual Sampling of Petroleum and Petroleum Products (ASTM Practice D4057)
1
This test method is under the jurisdiction of ASTM Committee D02 on Petroleum Products, Liquid Fuels, and Lubricants and the API Committee on Petroleum
Measurement, and is the direct responsibility of Subcommittee D02.02 /COMQ, the joint ASTM-API Committee on Hydrocarbon Measurement for Custody Transfer (Joint
ASTM-API). This test method has been approved by the sponsoring committees and accepted by the Cooperating Societies in accordance with established procedures.
Current edition approved June 1, 2017July 1, 2022. Published July 2017July 2022. Originally approved in 1938. Last previous edition approved in 20122017 as D473 – 07
ɛ1
(2012)(2017) . DOI: 10.1520/D0473-07R17E01.10.1520/D0473-22.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
3
Available from American Petroleum Institute (API), 1220 L. St., NW, Washington, DC 20005-4070, http://api-ec.api.org.
*A Summary of Changes section appears at the end of this standard
© Jointly copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, USA and the American Petroleum Institute (API), 1220 L Street NW, Washington DC 20005, USA
1

---------------------- Page: 1 ----------------------
D473 − 22
NOTE 1—Apparatus B shows the water cup in position.
FIG. 1 Extraction Apparatus for Determination of Sediment
Chapter 8.2 Automatic Sampling of Petroleum and Petroleum Products (ASTM Practice D4177)
Chapter 8.3 Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products (ASTM Practice D5854)
4
2.3 ISO Standard:
5272 Toluene for industrial use—Specifications
3. Terminology
3.1 For definitions of terms used in this standard test method, refer to Terminology D4175 and the API MPMS Chapter 1 Terms
and Definitions Database.
4. Summary
...

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