ASTM D802-02(2022)
(Test Method)Standard Test Methods for Sampling and Testing Pine Oils
Standard Test Methods for Sampling and Testing Pine Oils
SIGNIFICANCE AND USE
3.1 The testing procedures described in these test methods have been in use for many years and emphasize the physical properties of pine oil rather than its chemical composition. Test Methods D6387 describe a capillary gas chromatography method which is suitable for determining both the major and minor components found in pine oils.
SCOPE
1.1 These test methods cover procedures for sampling and testing pine oils, and are applicable to both natural pine oils derived from pine stumps either by the steam and solvent process or by destructive distillation, and also to synthetic pine oils obtained by the chemical hydration of terpene hydrocarbons.
1.2 The procedures given in these test methods appear in the following order:
Section
Sampling
4
Appearance
5
Color
6
Specific Gravity
7
Refractive Index
8
Composition
9
Moisture
10
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
General Information
- Status
- Published
- Publication Date
- 30-Nov-2022
- Technical Committee
- D01 - Paint and Related Coatings, Materials, and Applications
- Drafting Committee
- D01.34 - Pine Chemicals and Hydrocarbon Resins
Relations
- Effective Date
- 01-Oct-2023
- Effective Date
- 01-Jun-2020
- Effective Date
- 01-Jan-2019
- Effective Date
- 01-Dec-2014
- Effective Date
- 01-Nov-2012
- Effective Date
- 01-Nov-2012
- Effective Date
- 01-Nov-2012
- Effective Date
- 01-Jun-2010
- Effective Date
- 01-Jul-2008
- Effective Date
- 01-Jun-2008
- Effective Date
- 01-Jun-2007
- Effective Date
- 01-Dec-2005
- Effective Date
- 15-May-2005
- Effective Date
- 15-May-2005
- Effective Date
- 01-Dec-2003
Overview
ASTM D802-02(2022): Standard Test Methods for Sampling and Testing Pine Oils is an international ASTM standard that outlines procedures for sampling and testing the physical properties of both natural and synthetic pine oils. These comprehensive test methods focus on essential quality attributes such as appearance, color, specific gravity, refractive index, moisture content, and overall composition. The standard provides guidance suitable for natural pine oils derived from pine stumps via steam or solvent processes and synthetic pine oils obtained by chemically hydrating terpene hydrocarbons.
The testing procedures are administered in accordance with recognized global standardization principles, as outlined by the WTO Technical Barriers to Trade (TBT) Committee.
Key Topics
Sampling Procedures
- Ensures representative sampling of pine oil batches.
- Referenced standards: ASTM D268 and ASTM E300.
Appearance and Clarity
- Assessment for clarity, absence of foreign matter, and separated water.
Color Measurement
- Comparison using standardized color scales, such as Gardner (ASTM D6166) and platinum-cobalt (ASTM D1209).
Specific Gravity
- Determined accurately at 15.6 °C, which is vital for product consistency and quality control.
Refractive Index
- Measured at 20 °C, with correction factors for deviations, reflecting purity and formulation integrity.
Moisture Content
- Measured reliably using the Karl Fischer reagent, with reference to ASTM D890, ensuring product quality is maintained during storage and transport.
Composition Analysis
- Capillary gas chromatography (refer to ASTM D6387) is recommended to determine both major and minor terpene components present in pine oil.
Applications
The sampling and testing of pine oils using ASTM D802-02(2022) is critical for numerous industries, including:
Industrial Chemicals and Cleaning Products
Consistent product quality is crucial where pine oils are used for their solvent and fragrance properties.Paints, Coatings, and Adhesives
Ensures batch-to-batch uniformity, meeting requirements for physical characteristics.Pharmaceutical and Cosmetic Formulations
Guarantees purity and identifies contaminants that could affect safety or efficacy.Quality Assurance in Manufacturing
Provides manufacturers and suppliers with reliable methods to verify compliance before product shipment or acceptance.
These standardized methods help manufacturers, laboratories, and regulatory bodies maintain consistent quality and safety of pine oil-based products, facilitating domestic and international trade.
Related Standards
The following ASTM standards are referenced or related to the procedures described in ASTM D802-02(2022):
- ASTM D268 - Guide for Sampling and Testing Volatile Solvents and Chemical Intermediates
- ASTM D803 - Test Methods for Testing Tall Oil
- ASTM D890 - Test Method for Water in Liquid Pine Chemicals
- ASTM D1209 - Test Method for Color of Clear Liquids (Platinum-Cobalt Scale)
- ASTM D6166 - Test Method for Color Determination of Pine Chemicals (Gardner Color)
- ASTM D6387 - Test Methods for Composition of Turpentine and Related Terpene Products by Capillary Gas Chromatography
- ASTM E300 - Practice for Sampling Industrial Chemicals
Practical Value
Applying ASTM D802-02(2022) assures quality control for pine oil production and supply. Adhering to these test methods not only fosters regulatory compliance and customer satisfaction but also streamlines trade by establishing verifiable, reproducible benchmarks for physical characterization. Ensuring the integrity of pine oil at each stage - from raw material to finished product - is simplified by following this standard's detailed methodologies.
Keywords: pine oils, ASTM D802, sampling, testing, physical properties, quality control, gas chromatography, industrial chemicals, terpene alcohols.
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Frequently Asked Questions
ASTM D802-02(2022) is a standard published by ASTM International. Its full title is "Standard Test Methods for Sampling and Testing Pine Oils". This standard covers: SIGNIFICANCE AND USE 3.1 The testing procedures described in these test methods have been in use for many years and emphasize the physical properties of pine oil rather than its chemical composition. Test Methods D6387 describe a capillary gas chromatography method which is suitable for determining both the major and minor components found in pine oils. SCOPE 1.1 These test methods cover procedures for sampling and testing pine oils, and are applicable to both natural pine oils derived from pine stumps either by the steam and solvent process or by destructive distillation, and also to synthetic pine oils obtained by the chemical hydration of terpene hydrocarbons. 1.2 The procedures given in these test methods appear in the following order: Section Sampling 4 Appearance 5 Color 6 Specific Gravity 7 Refractive Index 8 Composition 9 Moisture 10 1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
SIGNIFICANCE AND USE 3.1 The testing procedures described in these test methods have been in use for many years and emphasize the physical properties of pine oil rather than its chemical composition. Test Methods D6387 describe a capillary gas chromatography method which is suitable for determining both the major and minor components found in pine oils. SCOPE 1.1 These test methods cover procedures for sampling and testing pine oils, and are applicable to both natural pine oils derived from pine stumps either by the steam and solvent process or by destructive distillation, and also to synthetic pine oils obtained by the chemical hydration of terpene hydrocarbons. 1.2 The procedures given in these test methods appear in the following order: Section Sampling 4 Appearance 5 Color 6 Specific Gravity 7 Refractive Index 8 Composition 9 Moisture 10 1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
ASTM D802-02(2022) is classified under the following ICS (International Classification for Standards) categories: 67.200.10 - Animal and vegetable fats and oils; 87.060.20 - Binders. The ICS classification helps identify the subject area and facilitates finding related standards.
ASTM D802-02(2022) has the following relationships with other standards: It is inter standard links to ASTM D6387-19(2023), ASTM D803-15(2020), ASTM D6387-19, ASTM D6387-99(2014)e1, ASTM D803-12, ASTM D890-12, ASTM D6166-12, ASTM D6387-99(2010)e1, ASTM D6166-08, ASTM D890-98(2008), ASTM D268-01(2007), ASTM D6387-99(2005), ASTM D1209-05e1, ASTM D1209-05, ASTM D890-98(2003). Understanding these relationships helps ensure you are using the most current and applicable version of the standard.
ASTM D802-02(2022) is available in PDF format for immediate download after purchase. The document can be added to your cart and obtained through the secure checkout process. Digital delivery ensures instant access to the complete standard document.
Standards Content (Sample)
This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D802 − 02 (Reapproved 2022)
Standard Test Methods for
Sampling and Testing Pine Oils
This standard is issued under the fixed designation D802; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D268 Guide for Sampling and Testing Volatile Solvents and
Chemical Intermediates for Use in Paint and Related
1.1 These test methods cover procedures for sampling and
Coatings and Material
testing pine oils, and are applicable to both natural pine oils
D803 Test Methods for Testing Tall Oil
derived from pine stumps either by the steam and solvent
D890 Test Method for Water in Liquid Pine Chemicals
process or by destructive distillation, and also to synthetic pine
D1209 Test Method for Color of Clear Liquids (Platinum-
oils obtained by the chemical hydration of terpene hydrocar-
Cobalt Scale)
bons.
D6166 Test Method for Color of Pine Chemicals and Re-
1.2 Theproceduresgiveninthesetestmethodsappearinthe
lated Products (Instrumental Determination of Gardner
following order:
Color)
Section
D6387 Test Methods for Composition of Turpentine and
Sampling 4
Related Terpene Products by Capillary Gas Chromatogra-
Appearance 5
phy
Color 6
Specific Gravity 7
E300 Practice for Sampling Industrial Chemicals
Refractive Index 8
Composition 9
3. Significance and Use
Moisture 10
3.1 The testing procedures described in these test methods
1.3 The values stated in SI units are to be regarded as
have been in use for many years and emphasize the physical
standard. No other units of measurement are included in this
properties of pine oil rather than its chemical composition.Test
standard.
Methods D6387 describe a capillary gas chromatography
1.4 This standard does not purport to address all of the
method which is suitable for determining both the major and
safety concerns, if any, associated with its use. It is the
minor components found in pine oils.
responsibility of the user of this standard to establish appro-
priate safety, health, and environmental practices and deter-
4. Sampling
mine the applicability of regulatory limitations prior to use.
4.1 Sample the material in accordance with the procedure
1.5 This international standard was developed in accor-
described in Guide D268 and Practice E300.
dance with internationally recognized principles on standard-
ization established in the Decision on Principles for the
5. Appearance
Development of International Standards, Guides and Recom-
5.1 Examine a portion of the sample after agitation to
mendations issued by the World Trade Organization Technical
determine its clarity and freedom from foreign matter and
Barriers to Trade (TBT) Committee.
separated water.
2. Referenced Documents
6. Color
2.1 ASTM Standards:
6.1 Compare the color of the sample in any suitable or
designated apparatus with the accepted or specific color
1 standard.Accepted color standards are the Gardner color scale
These test methods are under the jurisdiction of ASTM Committee D01 on
Paint and Related Coatings, Materials, and Applications and are the direct found in Test Method D6166 and the platinum-cobalt scale
responsibility of Subcommittee D01.34 on Pine Chemicals and Hydrocarbon
found in Test Method D1209.
Resins.
Current edition approved Dec. 1, 2022. Published December 2022. Originally
7. Specific Gravity
approved in 1944. Last previous edition approved in 2017 as D802 – 02 (2017).
DOI: 10.1520/D0802-02R22.
7.1 Determine the specific gravity at 15.6/15.6 °C by any
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
convenient method, reporting the value
...
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