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ASTM D7202-11

(Test Method)

Standard Test Method for Determination of Beryllium in the Workplace Using Field-Based Extraction and Optical Fluorescence Detection

Standard Test Method for Determination of Beryllium in the Workplace Using Field-Based Extraction and Optical Fluorescence Detection

SIGNIFICANCE AND USE
Exposure to beryllium can cause a potentially fatal disease, and occupational exposure limits for beryllium in air and on surfaces have been established to reduce exposure risks to potentially affected workers (4, 5). Sampling and analytical methods for beryllium are needed in order to meet the challenges relating to exposure assessment and risk reduction. Field-portable sampling and analysis methods, such as the procedure described in this test method, are desired in order to facilitate on-site measurement of beryllium. On-site beryllium analysis results can then be used as a basis for management of protection of human health.
SCOPE
1.1 This test method is intended for use in the determination of beryllium by sampling workplace air and surface dust.
1.2 This test method assumes that air and surface samples are collected using appropriate and applicable ASTM International standard practices for sampling of workplace air and surface dust. These samples are typically collected using air filter sampling, vacuum sampling or wiping techniques. See Guide E1370 for guidance on air sampling strategies, and Guide D7659 for guidance on selection of surface sampling techniques.
1.3 Determination of beryllium in soil is not within the scope of this test method. See Test Method D7458 for determination of beryllium in soil samples.
1.4 This test method includes a procedure for on-site extraction (dissolution) of beryllium in weakly acidic medium (pH of 1 % aqueous ammonium bifluoride is 4.8), followed by field analysis of aliquots of the extract solution using a beryllium-specific-optically fluorescent dye.
1.5 The procedure is targeted for on-site use in the field for occupational and environmental hygiene monitoring purposes.
1.6 No detailed operating instructions are provided because of differences among various makes and models of suitable fluorometric instruments. Instead, the analyst shall follow the instructions provided by the manufacturer of the particular instrument. This test method does not address comparative accuracy of different devices or the precision between instruments of the same make and model.
1.7 The values stated in SI units are to be regarded as standard.
1.8 This test method contains notes that are explanatory and not part of mandatory requirements of the standard.
1.9 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
30-Sep-2011
ICS
13.040.30 - Workplace atmospheres
Technical Committee
D22 - Air Quality
Drafting Committee
D22.04 - Workplace Air Quality
Current Stage
Ref Project

Relations

Replaces
ASTM D7202-06 - Standard Test Method for Determination of Beryllium in the Workplace Using Field-Based Extraction and Fluorescence Detection
Effective Date
01-Oct-2011
Replaced By
ASTM D7202-14 - Standard Test Method for Determination of Beryllium in the Workplace by Extraction and Optical Fluorescence Detection
Effective Date
01-Apr-2014
Referred By
ASTM D8404-21 - Standard Practice for Preparation of Soil Samples by Ammonium Bifluoride-Nitric Acid Digestion for Subsequent Analysis for Metals and Metalloids
Effective Date
01-Oct-2011
Referred By
ASTM D7458-21 - Standard Test Method for Determination of Beryllium in Soil and Sediment Using Ammonium Bifluoride Extraction and Fluorescence Detection
Effective Date
01-Oct-2011
Referred By
ASTM D8208-19 - Standard Practice for Collection of Non-Fibrous Nanoparticles Using a Nanoparticle Respiratory Deposition (NRD) Sampler
Effective Date
01-Oct-2011
Referred By
ASTM D7439-21 - Standard Test Method for Determination of Elements in Airborne Particulate Matter by Inductively Coupled Plasma–Mass Spectrometry
Effective Date
01-Oct-2011
Referred By
ASTM D7035-21 - Standard Test Method for Determination of Metals and Metalloids in Airborne Particulate Matter by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
Effective Date
01-Oct-2011
Referred By
ASTM D7707-21 - Standard Specification for Wipe Sampling Materials for Beryllium in Surface Dust
Effective Date
01-Oct-2011
Referred By
ASTM D7659-21 - Standard Guide for Strategies for Surface Sampling of Metals and Metalloids for Worker Protection
Effective Date
01-Oct-2011
Referred By
ASTM D8344-20 - Standard Practice for Ammonium Bifluoride and Nitric Acid Digestion of Airborne Dust and Dust-Wipe Samples for the Determination of Metals and Metalloids
Effective Date
01-Oct-2011

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ASTM D7202-11 - Standard Test Method for Determination of Beryllium in the Workplace Using Field-Based Extraction and Optical Fluorescence DetectionASTM D7202-11 - Standard Test Method for Determination of Beryllium in the Workplace Using Field-Based Extraction and Optical Fluorescence Detection
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D7202 − 11
StandardTest Method for
Determination of Beryllium in the Workplace Using Field-
1
Based Extraction and Optical Fluorescence Detection
This standard is issued under the fixed designation D7202; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 1.9 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the
1.1 Thistestmethodisintendedforuseinthedetermination
responsibility of the user of this standard to establish appro-
of beryllium by sampling workplace air and surface dust.
priate safety and health practices and determine the applica-
1.2 This test method assumes that air and surface samples
bility of regulatory limitations prior to use.
are collected using appropriate and applicableASTM Interna-
tional standard practices for sampling of workplace air and
2. Referenced Documents
surface dust. These samples are typically collected using air
2
2.1 ASTM Standards:
filter sampling, vacuum sampling or wiping techniques. See
D1193Specification for Reagent Water
Guide E1370 for guidance on air sampling strategies, and
D1356Terminology Relating to Sampling and Analysis of
Guide D7659 for guidance on selection of surface sampling
Atmospheres
techniques.
D4840Guide for Sample Chain-of-Custody Procedures
1.3 Determination of beryllium in soil is not within the D5337Practice for Flow RateAdjustment of Personal Sam-
scope of this test method. See Test Method D7458 for pling Pumps
determination of beryllium in soil samples. D6966Practice for Collection of Settled Dust Samples
Using Wipe Sampling Methods for Subsequent Determi-
1.4 This test method includes a procedure for on-site ex-
nation of Metals
traction (dissolution) of beryllium in weakly acidic medium
D7035Test Method for Determination of Metals and Met-
(pH of 1% aqueous ammonium bifluoride is 4.8), followed by
alloids in Airborne Particulate Matter by Inductively
field analysis of aliquots of the extract solution using a
Coupled Plasma Atomic Emission Spectrometry (ICP-
beryllium-specific-optically fluorescent dye.
AES)
1.5 The procedure is targeted for on-site use in the field for
D7144Practice for Collection of Surface Dust by Micro-
occupational and environmental hygiene monitoring purposes.
vacuum Sampling for Subsequent Metals Determination
D7296Practice for Collection of Settled Dust Samples
1.6 No detailed operating instructions are provided because
Using Dry Wipe Sampling Methods for Subsequent De-
of differences among various makes and models of suitable
termination of Beryllium and Compounds
fluorometric instruments. Instead, the analyst shall follow the
D7458Test Method for Determination of Beryllium in Soil,
instructions provided by the manufacturer of the particular
Rock, Sediment, and Fly Ash Using Ammonium Bifluo-
instrument. This test method does not address comparative
ride Extraction and Fluorescence Detection
accuracy of different devices or the precision between instru-
D7659Guide for Strategies for Surface Sampling of Metals
ments of the same make and model.
and Metalloids for Worker Protection
1.7 The values stated in SI units are to be regarded as
D7707SpecificationforWipeSamplingMaterialsforBeryl-
standard.
lium in Surface Dust
E691Practice for Conducting an Interlaboratory Study to
1.8 Thistestmethodcontainsnotesthatareexplanatoryand
Determine the Precision of a Test Method
not part of mandatory requirements of the standard.
E882Guide for Accountability and Quality Control in the
Chemical Analysis Laboratory
1
This test method is under the jurisdiction of ASTM Committee D22 on Air
Quality and is the direct responsibility of Subcommittee D22.04 on WorkplaceAir
2
Quality. For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Current edition approved Oct. 1, 2011. Published October 2011. Originally contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
approved in 2005. Last previous edition approved in 2006 as D7202-06. DOI: Standards volume information, refer to the standard’s Document Summary page on
10.1520/D7202-11. the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D7202 − 11
E1370Guide for Air Sampling Strategies for Worker and tate out due to the high alkalinity of the detection solution (1).
Workplace Protection In case the sample is suspected of having fluorescent organic
E1792Specification for Wipe Sampling Materials for Lead contaminants that are suspected to be present,
...

This document is not anASTM standard and is intended only to provide the user of anASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation:D7202–06 Designation:D7202–11
Standard Test Method for
Determination of Beryllium in the Workplace Using Field-
1
Based Extraction and Optical Fluorescence Detection
This standard is issued under the fixed designation D7202; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This test method is intended for use in the determination of beryllium by sampling workplace air and surface dust.
1.2 This test method assumes that air and surface samples are collected using appropriate and applicableASTM International
standard practices for sampling of workplace air and surface dust. These samples are typically collected using air filter sampling,
vacuum sampling or wiping techniques. See Guide E1370 for guidance on air sampling strategies, and Guide D7659 for guidance
on selection of surface sampling techniques.
1.3This 1.3 Determination of beryllium in soil is not within the scope of this test method. See Test Method D7458 for
determination of beryllium in soil samples.
1.4 Thistestmethodincludesaprocedureforon-siteextraction(dissolution)ofberylliuminweaklyacidicmedium(pHof1%
aqueous ammonium bifluoride is 4.8), followed by field analysis of aliquots of the extract solution using a beryllium-specific-
optically fluorescent dye.
1.4The1.5 The procedure is targeted for on-site use in the field for occupational and environmental hygiene monitoring
purposes.
1.5No1.6 No detailed operating instructions are provided because of differences among various makes and models of suitable
fluorometric instruments. Instead, the analyst shall follow the instructions provided by the manufacturer of the particular
instrument. This test method does not address comparative accuracy of different devices or the precision between instruments of
the same make and model.
1.6The1.7 The values stated in SI units are to be regarded as standard.
1.7This1.8 This test method contains notes that are explanatory and not part of mandatory requirements of the standard.
1.81.9 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
D1193 Specification for Reagent Water
D1356 Terminology Relating to Sampling and Analysis of Atmospheres
D4840 Guide for Sample Chain-of-Custody Procedures
D5337 Practice for Flow Rate Calibration of Personal Sampling Pumps
D6966 PracticeforCollectionofSettledDustSamplesUsingWipeSamplingMethodsforSubsequentDeterminationofMetals
D7035 TestMethodforDeterminationofMetalsandMetalloidsinAirborneParticulateMatterbyInductivelyCoupledPlasma
Atomic Emission Spectrometry (ICP-AES)
D7144 Practice for Collection of Surface Dust by Micro-vacuum Sampling for Subsequent Metals Determination
D7296 Practice for Collection of Settled Dust Samples Using Dry Wipe Sampling Methods for Subsequent Determination of
Beryllium and Compounds
D7458 Test Method for Determination of Beryllium in Soil, Rock, Sediment, and Fly Ash Using Ammonium Bifluoride
Extraction and Fluorescence Detection
D7659 Guide for Strategies for Surface Sampling of Metals and Metalloids for Worker Protection
1
This test method is under the jurisdiction ofASTM Committee D22 onAir Quality and is the direct responsibility of Subcommittee D22.04 onWorkplaceAtmospheres.
Air Quality.
Current edition approved Oct. 1, 2006.2011. Published November 2006.October 2011. Originally approved in 2005. Last previous edition approved in 20052006 as
D7202-056. DOI: 10.1520/D7202-06.10.1520/D7202-11.
2
ForreferencedASTMstandards,visittheASTMwebsite,www.astm.org,orcontactASTMCustomerServiceatservice@astm.org.For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D7202–11
D7707 Specification for Wipe Sampling Materials for Beryllium in Surface Dust
E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
E882 Guide for Accountability and Quality Control in the C
...

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1.2 Guidance provided by this standard is intended for sampling of metals and metalloids on surfaces for subsequent analysis using methods such as atomic spectrometry, mass spectrometry, X-ray fluorescence, or molecular fluorescence. Guidance for evaluation of data after sample analysis is included.  
1.3 Sampling for volatile organometallic species (for example, trimethyl tin) is not within the scope of this guide.  
1.4 Sampling to determine levels of metals or metalloids on the skin is not within the scope of this guide.  
1.5 Sampling for airborne particulate matter is not within the scope of this guide. Guide E1370 provides information on air sampling strategies.  
1.6 Where surface sampling is prescribed by law or regulation, this guide is not intended to take the place of any requirements that may be specified in such law or regulation.  
1.7 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D8405-21(Test Method)
Standard Test Method for Evaluating PM2.5 Sensors or Sensor Systems Used in Indoor Air Applications

SIGNIFICANCE AND USE
5.1 Poor indoor air quality has been implicated in significant adverse acute and chronic impacts on occupant health and performance. The ability to assess the components contributing to poor indoor air quality is critical for determining best practices for improving indoor air quality.  
5.2 Measurement of pollutants in indoor environments using sensors and sensor systems provides information needed to improve indoor air quality through pollutant source control, ventilation, filtration or other treatments.  
5.3 This method uses a test characterization chamber system equipped with reference monitor(s) to evaluate the response of test sensors or test sensor systems to specific types of particles (for example, salt, polystyrene latex, or dust). To facilitate reproducible results, the test particles used within this method are standardized and have known properties. The user is cautioned that a single particle type is not representative of all particles found indoors. The relative response of test sensors or test sensor systems to a reference monitor can vary by a factor of two for different particle types (for example, primary or secondary, organic or inorganic, outdoor or indoor origin; see 6.11.3 for further discussion). Furthermore, the user is cautioned that the lower limit of particle size detection for optical test sensors and test sensor systems is generally 0.3 μm in diameter; particles below this size are generally undetected and may represent a significant health concern as well.
SCOPE
1.1 This test method uses a chamber system to evaluate the performance of stationary PM2.5 sensors (sensors) and particle sensor systems (sensor systems) subjected to various test conditions, including temperature, relative humidity, PM2.5 concentration, and coarse PM interferent concentration.  
1.1.1 This test method covers sensors and sensor systems that can be continuously powered and continuously operated for the duration of any test described in this method through line power or an internal battery of sufficient output. This test method is not meant to evaluate sensors or sensor systems without these capabilities.  
1.1.2 This test method evaluates the performance of sensors and sensor systems that allow users to collect data in a systemic manner to assess the capabilities and limitations of these devices.  
1.1.3 This test method is not meant to evaluate sensors or sensor systems without data storage and recording capabilities.  
1.1.4 This test method is not intended to evaluate indoor air quality sensors and sensor systems for purposes of regulation of outdoor air, homeland security, law enforcement or forensic activity.  
1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.3 The text of this standard references notes and footnotes that provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM E1370-21(Guide)
Standard Guide for Air Sampling Strategies for Worker and Workplace Protection

SIGNIFICANCE AND USE
4.1 This guide describes standard approaches used to formulate air sampling strategies before actual air sampling occurs.  
4.2 For most workplace air sampling purposes, and for the majority of materials sampled, air sampling strategies are matters of choice. Air sampling in the workplace may be done for single or multiple purposes, such as health impact, hazard or risk assessment, compliance assessment, or investigation of complaints. Problems can arise when a single air sampling strategy is expected to satisfy multiple diverse purposes.  
4.2.1 Proper consideration of limitations of cost, space, power requirements, equipment, analytical methods, training and personnel result in a best available strategy for each purpose.  
4.2.2 A strategy designed to satisfy multiple purposes must be a compromise among several alternatives, and will not be optimum for any one purpose; however, the strategy should be appropriate for the intended purpose(s).  
4.2.3 The purpose or purposes for sampling should be explicitly stated before a sampling strategy is selected in order to ensure that the sampling strategy is appropriate for the intended use. Good sampling practice, legal requirements, cost of the sampling program, and the utility of the results may be markedly different for different intended sampling purposes.  
4.3 This guide is intended for use by those who are preparing to evaluate air quality in a work environment of a location by air sampling, or who wish to obtain an understanding of what information can be obtained by carrying out air sampling.  
4.4 This guide should not be used as a stand-alone document to evaluate any given airborne contaminant(s).  
4.5 This guide cannot take the place of sound professional judgment in development and execution of any sampling strategy. In most instances, a strategy based on a standard practice or method will need to be adjusted due to conditions encountered in the field. Documentation of any professional judgments appli...
SCOPE
1.1 This guide describes criteria to be used in defining air sampling strategies for workplace health and safety monitoring or evaluation. Sampling criteria such as duration, frequency, number, location, method, equipment, and timing are all considered.  
1.2 Where air sampling is prescribed by law or regulation, this guide is not intended to take the place of any requirements that may be specified in such law or regulation.  
1.3 Guidance for surface sampling strategies for metals and metalloids is provided in Guide D7659.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D8404-21(Practice)
Standard Practice for Preparation of Soil Samples by Ammonium Bifluoride-Nitric Acid Digestion for Subsequent Analysis for Metals and Metalloids

SIGNIFICANCE AND USE
5.1 There is a need to monitor the content of metals and metalloids in order to determine the presence of potential hazards. Hence, effective and efficient methods are required for the preparation of soil samples for determination of metals and metalloids present therein.  
5.2 This practice may be used for the digestion of soil samples that are collected during various construction and renovation and hazard survey activities in and around buildings and related structures. The practice is also suitable for the digestion of soil samples for metal and metalloid analyses collected from other locations, such as near roads and steel structures. For some other extraction procedures, see Practices D3974.  
5.3 This practice is intended to be used to prepare samples that have been collected for hazard assessment purposes but may be used for other applications such as, for example, monitoring the effectiveness of remediation activities.  
5.4 This practice may be capable of determining metals and metalloids bound within matrices, such as silica, that are not soluble in nitric acid alone.  
5.5 This practice includes drying and homogenization steps to help assure that reported results are representative of the sample and are independent of potential differences in soil moisture levels among different sampling locations or changing weather conditions.
SCOPE
1.1 This practice covers drying, homogenization, and ammonium bifluoride-nitric acid digestion of soil samples and associated quality control (QC) samples for the determination of metals and metalloids using laboratory atomic spectrometry analysis techniques such as inductively coupled plasma mass spectrometry (ICP-MS), inductively coupled plasma atomic emission spectrometry (ICP-AES), flame atomic absorption spectrometry (FAAS), and graphite furnace atomic absorption spectrometry (GFAAS). For ammonium bifluoride-nitric acid digestion of airborne dust and dust-wipe samples for the determination of metals and metalloids, see Practice D8344.  
1.2 This practice is based on U.S. EPA SW 846, Test Method 3050, Test Method D7202, and Practice D8344.  
1.3 This practice contains notes that are explanatory and are not part of the mandatory requirements of this standard.  
1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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