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ASTM D2968-22

(Test Method)

Standard Test Method for Med and Kemp Fibers in Wool and Other Animal Fibers by Microprojection

Standard Test Method for Med and Kemp Fibers in Wool and Other Animal Fibers by Microprojection

SIGNIFICANCE AND USE
5.1 Test Method D2968 for the determination of med and kemp fibers by microprojection may be used for the acceptance testing of commercial shipments of wool and other animal fibers, but caution is advised since only a few types of animal fibers have been subjected to interlaboratory tests to ascertain the precision of tests for med and kemp fibers by this test method. Comparative tests as directed in 5.1.1 may be advisable.  
5.1.1 In case of a dispute arising from differences in reported test results when using Test Method D2968 for acceptance testing of commercial shipments, the purchaser and the supplier should conduct comparative tests to determine if there is a statistical bias between their laboratories. Competent statistical assistance is recommended for the investigation of bias. As a minimum, the two parties should take a group of test specimens which are as homogeneous as possible and which are from a lot of material of the type in question. The test specimens should then be randomly assigned in equal numbers to each laboratory for testing. The average results from the two laboratories should be compared using Student's t-test for unpaired data and an acceptable probability level chosen by the two parties before testing is begun. If a bias is found, either its cause must be found and corrected, or the purchaser and the supplier must agree to interpret future test results in view of the known bias.  
5.2 Knowledge of the incidence of med fibers and kemp fibers in wool and other animal fibers is of importance to manufacturers of woven or knitted fabrics because of the apparent dye resistance and light reflectance qualities of these fibers. This is not to imply that all kemp fibers will resist dye and all med fibers will accept dye normally. In practice, a proportion of kemp fibers will appear normal after dyeing and a proportion of med fibers will appear chalky white after dyeing. From the perspective of visual and aesthetic problems, medullated fibers hav...
SCOPE
1.1 This test method covers the determination by microprojection of the percentage of medullated fibers (med and kemp fibers) in wool or other animal fibers such as mohair, cashmere, alpaca, or camel's hair in their various forms.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
31-May-2022
ICS
59.060.10 - Natural fibres
Technical Committee
D13 - Textiles
Drafting Committee
D13.13 - Wool and Felt
Current Stage
Ref Project

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ASTM D2968-22 - Standard Test Method for Med and Kemp Fibers in Wool and Other Animal Fibers by MicroprojectionASTM D2968-22 - Standard Test Method for Med and Kemp Fibers in Wool and Other Animal Fibers by Microprojection
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ASTM D2968-22 - Standard Test Method for Med and Kemp Fibers in Wool and Other Animal Fibers by Microprojection
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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D2968 − 22
Standard Test Method for
Med and Kemp Fibers in Wool and Other Animal Fibers by
1
Microprojection
This standard is issued under the fixed designation D2968; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 4. Summary of Test Method
1.1 This test method covers the determination by micropro- 4.1 Themagnifiedimagesofaspecimenoftheanimalfibers
jection of the percentage of medullated fibers (med and kemp are examined. All medullated fibers are measured and classed
fibers)inwoolorotheranimalfiberssuchasmohair,cashmere, as either med fibers or kemp fibers. The observed numbers of
alpaca, or camel’s hair in their various forms. med and kemp fibers are expressed as percentages of the total
number of fiber images examined.
1.2 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the
5. Significance and Use
responsibility of the user of this standard to establish appro-
5.1 Test Method D2968 for the determination of med and
priate safety, health, and environmental practices and deter-
mine the applicability of regulatory limitations prior to use. kempfibersbymicroprojectionmaybeusedfortheacceptance
testing of commercial shipments of wool and other animal
1.3 This international standard was developed in accor-
dance with internationally recognized principles on standard- fibers, but caution is advised since only a few types of animal
fibers have been subjected to interlaboratory tests to ascertain
ization established in the Decision on Principles for the
Development of International Standards, Guides and Recom- the precision of tests for med and kemp fibers by this test
method. Comparative tests as directed in 5.1.1 may be advis-
mendations issued by the World Trade Organization Technical
Barriers to Trade (TBT) Committee. able.
5.1.1 In case of a dispute arising from differences in
2. Referenced Documents
reported test results when using Test Method D2968 for
2
2.1 ASTM Standards: acceptance testing of commercial shipments, the purchaser and
D123 Terminology Relating to Textiles the supplier should conduct comparative tests to determine if
D2130 Test Method for Diameter ofWool and OtherAnimal there is a statistical bias between their laboratories. Competent
3
Fibers by Microprojection (Withdrawn 2022) statistical assistance is recommended for the investigation of
D4845 Terminology Relating to Wool bias.As a minimum, the two parties should take a group of test
specimens which are as homogeneous as possible and which
3. Terminology
are from a lot of material of the type in question. The test
3.1 For all terminology related to D13.13, Wool and Felt,
specimens should then be randomly assigned in equal numbers
see Terminology D4845. to each laboratory for testing.The average results from the two
3.1.1 The following terms are relevant to this standard:
laboratories should be compared using Student’s t-test for
kemp fiber; med fiber; medulla, in mammalian hair fibers; unpaireddataandanacceptableprobabilitylevelchosenbythe
medullated fiber; wool. two parties before testing is begun. If a bias is found, either its
cause must be found and corrected, or the purchaser and the
3.2 FordefinitionsofallothertextiletermsseeTerminology
suppliermustagreetointerpretfuturetestresultsinviewofthe
D123.
known bias.
1 5.2 Knowledge of the incidence of med fibers and kemp
This test method is under the jurisdiction ofASTM Committee D13 on Textiles
and is the direct responsibility of Subcommittee D13.13 on Wool and Felt.
fibers in wool and other animal fibers is of importance to
CurrenteditionapprovedJune1,2022.PublishedJuly2022.Originallyapproved
manufacturers of woven or knitted fabrics because of the
in 1971. Last previous edition approved in 2013 as D2968 – 13 which was
apparent dye resistance and light reflectance qualities of these
withdrawn in January 2022 and reinstated in June 2022. DOI: 10.1520/D2968-22.
2
fibers. This is not to imply that all kemp fibers will resist dye
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
and all med fibers will accept dye normally. In practice, a
Standards volume information, refer to the standard’s Document Summary page on
proportion of kemp fibers will appear normal after dyeing and
the ASTM website.
3 a proportion of med fibers will appear chalky white after
The last approved version
...

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ASTM D1574-22(Test Method)
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5.1 Test Method D1574 is considered satisfactory for acceptance testing since the method has been used extensively in the trade for acceptance testing.  
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5.3 The residues obtained in this test may be subjected to chemical analysis for identification and assay of the component materials, if desired.  
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1.1 This test method covers the determination of the amount of extractable matter in samples of all forms of wool, except grease wool, that is extractable with a non-flammable vapor degreasing and cleaning solvent.  
1.2 This test method does not cover the determination of the amounts of different components in the extracted matter nor their identification.  
1.3 This test method is suitable for use with other animal fibers.  
Note 1: The determination of extractable matter in yarns and in felts is covered in Test Methods D2257 and D461. For the determination of alcohol-extractable matter in oven-dry scoured wool, refer to Test Methods D584 and D1334.  
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ASTM D2524-22(Test Method)
Standard Test Method for Breaking Tenacity of Wool Fibers, Flat Bundle Method— 18 in. (3.2 mm) Gage Length

SIGNIFICANCE AND USE
5.1 Test Method D2524 for testing wool fibers for tenacity is considered satisfactory for acceptance testing when the participating laboratories, using a reference wool, have shown acceptable between-laboratory precision. It is recommended that any program of acceptance testing be preceded by an interlaboratory check in the laboratory of the purchaser and the laboratory of the seller on replicate specimens of samples of the material to be evaluated. In cases of dispute, the statistical bias, if any, between the laboratory of the purchaser and the seller should be determined with each comparison being based on testing randomized specimens from one sample of material of the type being evaluated.  
5.2 Values obtained from flat bundle tenacity show a good correlation with values obtained from single fiber tests and require much less time.  
5.3 The basic differences between the procedures described in Test Method D2524 and those described in Test Method D1294 lie in the manner of clamping the bundles and the shorter gage length employed. The special clamps used in this method allow quicker and easier bundle preparation; however, for Test Method D1294 no special clamps are required. Closer agreement with single fiber tenacity is also obtained with Test Method D2524 than when using the procedure in Test Method D1294.  
5.4 As the observed tenacity of fibers depends in part on the type of tensile testing machine used and the time required to break the specimen, results obtained with the different types of machines which may be used in this method will not necessarily agree. The machines specifically designed for bundle testing are CRL testers which operate at a loading rate of 1 kgf/s and therefore reach the breaking force at variable times in the order of 5 s. CRE and CRT type machines would be expected to produce somewhat different results not only because of the inherent difference in operation but because CRE and CRT type machines are to be operated at a rate to ac...
SCOPE
1.1 This test method covers the determination of the breaking tenacity of wool fibers as a flat bundle with a 1/8 in. (3.2 mm) clamp separation.  
1.2 This test method is especially adapted to the fiber bundle clamps and strength testing instruments specified, but may be used on other tensile testing machines when equipped with appropriate adapters to accommodate the prescribed clamps.  
1.3 This test method is applicable to wool in any form which can be hand-combed into small bundles of parallelized fibers.  
Note 1: Other test methods for measuring breaking tenacity of fiber bundles include Test Methods D1294, D1445, and D540.  
1.4 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Standard Test Method for Color Measurement of Flax Fiber

SIGNIFICANCE AND USE
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SCOPE
1.1 This test method covers the instrumental color measurement of flax fiber.  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D8394-21(Test Method)
Standard Test Method for Automated Measurement of Maturity, Fineness, Ribbon Width, and Micronaire of Cotton Fibers

SIGNIFICANCE AND USE
5.1 Cotton fiber that is on average finer and more mature is more desirable than coarse or immature fiber, although distinction between these qualities cannot be made quickly and accurately using current test methods. Immature fibers break more easily during processing and have a tendency to form into neps (small entanglements) during processing in the spinning mill. These consequences adversely affect yarn and fabric quality and appearance. Yarn and fabric produced from immature fiber is typically also less lustrous and does not take up dye consistently so yarn and fabric appearance may be different after dyeing.  
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5.2.1 Fine fibers are required for fine count yarn manufacture and fiber fineness affects yarn count, evenness and strength. Both fineness and ribbon width are strong genetic traits evident between species and affected by growing conditions within species.  
5.2.2 Micronaire has traditionally been used as a measure of fiber fineness although the value actually measures fiber specific surface area or surface area per unit weight. As a result, micronaire varies concomitantly with both maturity and fineness (see Fig. 2). Maturity and fineness are related to micronaire via Lord’s equation.4
FIG. 2 Relationship Between Micronaire (X), Fineness (H), and Maturity (M)  
5.3 Cottonscope values have been judged against fineness, maturity and ribbon width values produced by examination of thousands of individual, magnified fiber cross-sections. Relationships with equivalent values by these and other older test methods are highly significant5,6 particularly if the number of cross-sections analyzed is high (>3000) and the cross-sections are carefully prepared and measured. Cottonscope measures approximately 20,...
SCOPE
1.1 This test method covers the determination of linear density (gravimetric fineness hereafter stated as fineness), maturity, micronaire, and ribbon width of cotton fibers from a loose, chemically untreated sample taken before harvest, during ginning, during mill processing or unraveled from raw (undyed) yarn or fabric.  
1.2 This test method requires the use of an integrated instrument, for example, the Cottonscope (see Fig. 1), that measures the maturity, fineness, ribbon width, and micronaire of cotton fiber.2
FIG. 1 Cottonscope Instrument
Note 1: For another test method to determine the maturity of cotton fibers, refer to Test Method D1442.  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D1447-07(2021)(Test Method)
Standard Test Method for Length and Length Uniformity of Cotton Fibers by Photoelectric Measurement

SIGNIFICANCE AND USE
5.1 This test method is considered satisfactory for acceptance testing when the levels of the laboratories are controlled by the use of the same reference standard cotton samples because the current estimates of between-laboratory precision are acceptable under these conditions. If there are differences of practical significance between reported test results for two laboratories (or more), comparative tests should be performed to determine if there is a statistical bias between them, using competent statistical assistance. As a minimum, ensure the test samples to be used are as homogeneous as possible, are drawn from the material from which the disparate test results were obtained, and are randomly assigned in equal numbers to each laboratory for testing. The test from the two laboratories should be compared using a statistical test for unpaired data, at a probability level chosen prior to the testing series. If a bias is found, either its cause must be found and corrected, or future test results for that material must be adjusted in consideration of the known bias.  
5.2 Fibrograph measurements provide a relatively fast method for determining the length and length uniformity of the fibers in a sample of cotton in a reproducible manner.  
5.3 Results of the Fibrograph length tests do not necessarily agree with those obtained by other methods for measuring lengths of cotton fibers because of the effect of fiber crimp and other factors.  
5.4 Fibrograph tests are more objective than commercial staple length classifications and also provide additional information on fiber length uniformity of cotton fibers. The cotton quality information provided by these results is used in research studies and quality surveys, in checking commercial staple length classifications, in assembling bales of cotton into uniform lots, and for other purposes.  
5.5 Fibrograph measurements are based on the assumptions that a fiber is caught randomly along its length.
SCOPE
1.1 This test method covers the measurement of the length and length uniformity of cotton fibers by use of photoelectric measurement. The test method is applicable to fibers taken from raw or partially processed cotton (up to card mat) or some types of cotton waste, but not to fibers from blends of cotton with other fibers or to fibers recovered from cotton yarns, fabrics or to 100 % synthetic fibers.  
1.2 This test method is especially adapted for determining the length and length uniformity of cotton fibers by models of the Digital Fibrograph, hereafter referred to as Fibrograph.
Note 1: Instructions for the use of Manual and Servo Fibrograph Models were included in the text of Test Method D1447 in 1971 and previous editions.
Note 2: For other methods covering the measurement of the length of cotton fibers refer to Test Method D1440.  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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