EN 15662:2018

Foods of plant origin - Multimethod for the determination of pesticide residues using GC- and LC-based analysis following acetonitrile extraction/partitioning and clean-up by dispersive SPE - Modular QuEChERS-method

This European Standard stipulates a method for the analysis of pesticide residues in foods of plant origin, such as fruits (including dried fruits), vegetables, cereals and many processed products thereof by using GC, GC-MS(/MS), and/or LC-MS(/MS). The method has been collaboratively studied on a large number of commodity/pesticide combinations. Precision data are summarized in FprCEN/TR 17063. Guidelines for calibration are outlined in FprCEN/TS 17061.

Pflanzliche Lebensmittel - Multiverfahren zur Bestimmung von Pestizidrückständen mit GC und LC nach Acetonitril-Extraktion/Verteilung und Reinigung mit dispersiver SPE - Modulares QuEChERS-Verfahren

Diese Europäische Norm beschreibt ein Verfahren für die Analyse von Pestizidrückständen in pflanzlichen Lebensmitteln wie z. B. Früchten (einschließlich Trockenfrüchten), Gemüse (einschließlich getrocknetem Gemüse), Getreide und vielen verarbeiteten Erzeugnissen aus diesen Produkten unter Verwendung von GC, GC MS(/MS) und/oder LC MS(/MS). Das Verfahren wurde im Ringversuch mit einer großen Anzahl an Rohstoff /Pestizidkombinationen geprüft. Die Präzisionsdaten sind in CEN/TR 17063 zusammen¬gefasst. Leitfäden für die Kalibrierung sind in CEN/TS 17061 angegeben.

Aliments d'origine végétale - Multiméthode de détermination des résidus de pesticides par analyse CG et CL après extraction/partition avec de l'acétonitrile et purification par SPE dispersive - Méthode modulaire QuEChERS

La présente Norme européenne décrit une méthode d’analyse CG, CG-SM(/SM) et/ou CL-SM(/SM) des résidus de pesticides dans les aliments d’origine végétale, notamment les fruits (y compris les fruits secs), les légumes (y compris les légumes secs), les céréales et les nombreux produits transformés dérivés de ceux-ci. La méthode a fait l’objet d’un essai interlaboratoires portant sur un grand nombre de combinaisons denrée/pesticide. Les données de fidélité sont résumées dans le CEN/TR 17063. Les lignes directrices relatives à l’étalonnage sont données dans le CEN/TS 17061.

Hrana rastlinskega izvora - Večelementna metoda za določanje ostankov pesticidov z uporabo analize na osnovi GC in LC po delitvi in izpiranju acetonitrila z disperzivno SPE - Modularna metoda QuEChERS

Ta evropski standard določa metodo za analizo ostankov pesticidov v živilih rastlinskega izvora, kot so sadje (vključno s suhim sadjem), zelenjava, žitarice in številni predelani izdelki rastlinskega izvora z uporabo GC, GC-MS(/MS) in/ali LC-MS(/MS). Ta metoda je bila raziskana z večstranskimi študijami na veliki količini kombinacij proizvodov in pesticidov. Podatki o natančnosti so povzeti v standardu FprCEN/TR 17063. Smernice za umerjanje so opisane v standardu FprCEN/TS 17061.

General Information

• Status: Published
• Publication Date: 22-May-2018
• Withdrawal Date: 29-Nov-2018
• ICS: 67.050 - General methods of tests and analysis for food products
• Technical Committee: CEN/TC 275 - Food analysis - Horizontal methods
• Drafting Committee: CEN/TC 275/WG 3 - Pesticides and PCB's in foods of animal origin
• Current Stage: 9060 - Closure of 2 Year Review Enquiry - Review Enquiry
• Start Date: 02-Dec-2023
• Completion Date: 02-Dec-2023
• Directive: 882/2004 - Regulation (EC) No 882/2004 of the European Parliament and of the Council of 29 April 2004 onofficial controls performed to ensure the verification of compliance with feed and food law, animal health and animal welfare rules
• Ref Project: SIST EN 15662:2018 - Foods of plant origin - Multimethod for the determination of pesticide residues using GC- and LC-based analysis following acetonitrile extraction/partitioning and clean-up by dispersive SPE - Modular QuEChERS-method

Relations

• Replaces: EN 15662:2008 - Foods of plant origin - Determination of pesticide residues using GC-MS and/or LC-MS/MS following acetonitrile extraction/partitioning and clean-up by dispersive SPE - QuEChERS-method
• Effective Date: 30-Sep-2015

Standards Content (Sample)

SLOVENSKI STANDARD
SIST EN 15662:2018
01-julij-2018
1DGRPHãþD
SIST EN 15662:2009
+UDQDUDVWOLQVNHJDL]YRUD9HþHOHPHQWQDPHWRGD]DGRORþDQMHRVWDQNRY
SHVWLFLGRY]XSRUDERDQDOL]HQDRVQRYL*&LQ/&SRGHOLWYLLQL]SLUDQMXDFHWRQLWULOD
]GLVSHU]LYQR63(0RGXODUQDPHWRGD4X(&K(56
Foods of plant origin - Multimethod for the determination of pesticide residues using GC-
and LC-based analysis following acetonitrile extraction/partitioning and clean-up by
dispersive SPE - Modular QuEChERS-method
Pflanzliche Lebensmittel - Multiverfahren zur Bestimmung von Pestizidrückständen mit
GC und LC nach Acetonitril-Extraktion/Verteilung und Reinigung mit dispersiver SPE -
Modulares QuEChERS-Verfahren
Aliments d'origine végétale - Multiméthode de détermination des résidus de pesticides
par analyse CG et CL après extraction/partition avec de l'acétonitrile et purification par
SPE dispersive - Méthode modulaire QuEChERS
Ta slovenski standard je istoveten z: EN 15662:2018
ICS:
67.050 Splošne preskusne in General methods of tests and
analizne metode za živilske analysis for food products
proizvode
SIST EN 15662:2018 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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SIST EN 15662:2018

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SIST EN 15662:2018


EN 15662
EUROPEAN STANDARD

NORME EUROPÉENNE

May 2018
EUROPÄISCHE NORM
ICS 67.050 Supersedes EN 15662:2008
English Version

Foods of plant origin - Multimethod for the determination
of pesticide residues using GC- and LC-based analysis
following acetonitrile extraction/partitioning and clean-up
by dispersive SPE - Modular QuEChERS-method
Aliments d'origine végétale - Multiméthode de Pflanzliche Lebensmittel - Multiverfahren zur
détermination des résidus de pesticides par analyse CG Bestimmung von Pestizidrückständen mit GC und LC
et CL après extraction/partition avec de l'acétonitrile nach Acetonitril-Extraktion/Verteilung und Reinigung
et purification par SPE dispersive - Méthode modulaire mit dispersiver SPE - Modulares QuEChERS-Verfahren
QuEChERS
This European Standard was approved by CEN on 27 December 2017.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.

This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

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Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and United Kingdom.





EUROPEAN COMMITTEE FOR STANDARDIZATION
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EUROPÄISCHES KOMITEE FÜR NORMUNG

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© 2018 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN 15662:2018 E
worldwide for CEN national Members.

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SIST EN 15662:2018
EN 15662:2018 (E)
Contents Page
European foreword . 3
1 Scope . 4
2 Normative references . 4
3 Principle . 4
4 Preparation and storage of the samples . 4
5 Procedure. 5
6 Evaluation of results . 15
7 Confirmatory tests .
...