Plastics - Polyamides - Determination of e-caprolactam and w-laurolactam by gas chromatography (ISO 11337:2010)

ISO 11337:2010 specifies a method for determining epsilon‑caprolactam and omega‑laurolactam in polyamides by gas chromatography. It is suitable particularly for the determination of epsilon‑caprolactam in polyamide 6 and omega‑laurolactam in polyamide 12. Bearing in mind that gas chromatography offers a wide range of possible conditions, the method specified is that shown to have been suitable in practice.
Two variants of the basic method are specified:
Method A is an extraction method with boiling methanol, and the extract is injected into a gas chromatograph.
Method B is a method using a solvent, and the solution is injected into a gas chromatograph.

Kunststoffe - Polyamide - Gaschromatographische Bestimmung von ε-Caprolactam und w-Laurolactam (ISO 11337:2010)

Diese Internationale Norm legt ein gaschromatographisches Verfahren zur Bestimmung des -Caprolactamgehaltes und des -Laurolactamgehaltes in Polyamiden fest. Es ist besonders zur Bestimmung von -Caprolactam in Polyamid 6 und von -Laurolactam in Polyamid 12 geeignet. Unter Berücksichtigung der Tatsache, dass die Gaschromatographie einen ausgedehnten Bereich von Möglichkeiten bietet, hat sich das festgelegte Verfahren in der Praxis als geeignet erwiesen.
Zwei Verfahren sind in dieser Internationalen Norm festgelegt:
Verfahren A ist ein Extraktionsverfahren unter Anwendung von siedendem Methanol, bei dem die Extrakte in einen Gaschromatographen injiziert werden;
Verfahren B ist ein Verfahren unter Anwendung eines Lösemittels, bei dem die Lösung direkt in einen Gaschromatographen injiziert wird.

Plastiques - Polyamides - Détermination du e-caprolactame et du w-laurolactame par chromatographie en phase gazeuse (ISO 11337:2010)

L'ISO 11337:2010 spécifie une méthode de dosage du epsilon-caprolactame et du omega-laurolactame dans les polyamides par chromatographie en phase gazeuse. Elle convient particulièrement au dosage du epsilon-caprolactame dans le polyamide 6 et du omega-laurolactame dans le polyamide 12. Compte tenu du fait que la chromatographie en phase gazeuse présente un large éventail de conditions possibles, la méthode spécifiée est celle qui a fait ses preuves dans la pratique.
Deux variantes de la méthode de base sont spécifiées:
Méthode A, par extraction au méthanol en ébullition, où les extraits sont injectés dans un chromatographe en phase gazeuse.
Méthode B, utilisant un solvant, où la solution est injectée directement dans un chromatographe en phase gazeuse.

Polimerni materiali - Poliamidi - Določanje e-kaprolaktama in w-laurolaktama s plinsko kromatografijo (ISO 11337:2010)

Ta mednarodni standard opredeljuje metodo za določanje ε-kaprolaktama in ω-lavrolaktama v poliamidih s plinsko kromatografijo. Primerna je zlasti za določanje ε-kaprolaktama v poliamidu 6 in ω-lavrolaktama v poliamidu 12. Z upoštevanjem, da plinska kromatografija ponuja širok razpon mogočih pogojev, je določena metoda tista, ki je bila dokazano primerna v praksi.
Določeni sta dve različici osnovne metode:
⎯ Metoda A je ekstrakcijska metoda, pri kateri se izvleček po metanolnem vrenju vbrizga v plinski kromatograf.
⎯ Metoda B je metoda, pri kateri se uporablja topilo, raztopina pa se vbrizga v plinski kromatograf.

General Information

Status
Withdrawn
Publication Date
14-Dec-2010
Withdrawal Date
31-Jan-2023
Technical Committee
Drafting Committee
Current Stage

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SLOVENSKI STANDARD
SIST EN ISO 11337:2011
01-november-2011
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SIST EN ISO 11337:2004
SIST EN ISO 11337:2004/AC:2009
3ROLPHUQLPDWHULDOL3ROLDPLGL'RORþDQMHHNDSURODNWDPDLQZODXURODNWDPDV
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Plastics - Polyamides - Determination of e-caprolactam and w-laurolactam by gas
chromatography (ISO 11337:2010)
Kunststoffe - Polyamide - Gaschromatographische Bestimmung von  -
Caprolactam und -Laurolactam (ISO 11337:2010)
Plastiques - Polyamides - Détermination du e-caprolactame et du w-laurolactame par
chromatographie en phase gazeuse (ISO 11337:2010)
Ta slovenski standard je istoveten z: EN ISO 11337:2010
ICS:
83.080.20 Plastomeri Thermoplastic materials
SIST EN ISO 11337:2011 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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SIST EN ISO 11337:2011

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SIST EN ISO 11337:2011


EUROPEAN STANDARD
EN ISO 11337

NORME EUROPÉENNE

EUROPÄISCHE NORM
December 2010
ICS 83.080.20 Supersedes EN ISO 11337:2004
English Version
Plastics - Polyamides - Determination of e-caprolactam and w-
laurolactam by gas chromatography (ISO 11337:2010)
Plastiques - Polyamides - Détermination du e-caprolactame Kunststoffe - Polyamide - Gaschromatographische
et du w-laurolactame par chromatographie en phase Bestimmung von e-Caprolactam und w-Laurolactam (ISO
gazeuse (ISO 11337:2010) 11337:2010)
This European Standard was approved by CEN on 10 December 2010.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European
Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national
standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member.

This European Standard exists in three official versions (English, French, German). A version in any other language made by translation
under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same
status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland,
Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.





EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

Management Centre: Avenue Marnix 17, B-1000 Brussels
© 2010 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 11337:2010: E
worldwide for CEN national Members.

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SIST EN ISO 11337:2011
EN ISO 11337:2010 (E)
Contents Page
Foreword .3

2

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SIST EN ISO 11337:2011
EN ISO 11337:2010 (E)
Foreword
This document (EN ISO 11337:2010) has been prepared by Technical Committee ISO/TC 61 “Plastics” in
collaboration with Technical Committee CEN/TC 249 “Plastics” the secretariat of which is held by NBN.
This European Standard shall be given the status of a national standard, either by publication of an identical
text or by endorsement, at the latest by June 2011, and conflicting national standards shall be withdrawn at
the latest by June 2011.
Attention is drawn to the possibility that some of the elements of this document may be the subject of patent
rights. CEN [and/or CENELEC] shall not be held responsible for identifying any or all such patent rights.
This document supersedes EN ISO 11337:2004.
According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following
countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech
Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia,
Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain,
Sweden, Switzerland and the United Kingdom.
Endorsement notice
The text of ISO 11337:2010 has been approved by CEN as a EN ISO 11337:2010 without any modification.

3

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SIST EN ISO 11337:2011

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SIST EN ISO 11337:2011

INTERNATIONAL ISO
STANDARD 11337
Second edition
2010-12-15

Plastics — Polyamides — Determination
of ε-caprolactam and ω-laurolactam by
ga
...

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