Vinegar - Isotopic analysis of acetic acid and water - Part 1: 2H-NMR analysis of acetic acid

This European Standard specifies an isotopic method to control the authenticity of vinegar. This method is applicable on acetic acid of vinegar (from wine, cider, agricultural alcohol, etc.) in order to characterise the botanical origin of acetic acid and to detect adulterations of vinegar using synthetic acetic acid or acetic acid from a non-allowed origin (together with the method described in FprEN 16466-2).
The isotopic analysis of the extracted acetic acid by 2H-NMR is based on a similar method already normalised for wine analysis [2].
The application to complex matrices made with vinegar as an ingredient, such as balsamic vinegar, is out of the scope of the inter-laboratory validation performed.

Essig - Isotopenanalyse von Essigsäure und Wasser - Teil 1: 2H-NMR-Analyse von Essigsäure

Diese Europäische Norm legt ein isotopenanalytisches Verfahren zur Überprüfung der Authentizität von Essig fest. Dieses Verfahren ist anwendbar auf Essigsäure aus Essig (aus Wein, Apfelwein, Agraralkohol usw.), um den botanischen Ursprung der Essigsäure zu charakterisieren und um Verfälschungen von Essig durch Verwendung synthetischer Essigsäure oder Essigsäure aus einem nicht zulässigen Ursprung nachzuweisen (in Kombination mit dem in EN 16466 2 beschriebenen Verfahren).
Die Isotopenanalyse der extrahierten Essigsäure durch 2H NMR Spektroskopie beruht auf einem ähnlichen Verfahren, das bereits für die Weinanalyse genormt wurde [2].
Diese Europäische Norm ist auf komplexe Matrices, die unter Verwendung von Essig als Zutat hergestellt wurden, z. B. Balsamessig, nicht anwendbar.

Vinaigre - Analyse isotopique de l'acide acétique et de l'eau - Partie 1: Analyse RMN-2H de l'acide acétique

La présente Norme européenne spécifie une méthode isotopique de contrôle de l’authenticité du vinaigre. La présente méthode s’applique à l’acide acétique de vinaigre (de vin, de cidre, d’alcool agricole, etc.) afin de caractériser l’origine botanique de l’acide acétique et de détecter des adultérations du vinaigre utilisant de l’acide acétique synthétique ou de l’acide acétique d’une origine non autorisée (en complément de la méthode décrite dans l’EN 16466-2).
L’analyse isotopique par RMN-2H de l’acide acétique extrait est fondée sur une méthode similaire à celle de l’analyse du vin, déjà normalisée [2].
La présente Norme européenne ne s’applique pas aux matrices complexes réalisées avec du vinaigre comme ingrédient, par exemple le vinaigre balsamique.

Kis - Izotopska analiza ocetne kisline in vode - 1. del: 2H-NMR-analiza ocetne kisline

Ta evropski standard določa izotopsko metodo za nadzorovanje pristnosti kisa. Ta metoda se uporablja za ocetno kislino v kisu (iz vina, mošta, kmetijskega alkohola itd.), da se opredelijo značilnosti botaničnega izvora ocetne kisline in zazna ponarejanje kisa z uporabo sintetične ocetne kisline ali ocetne kisline nedovoljenega izvora (skupaj z metodo iz standarda EN 16466-2). Izotopska analiza ekstrahirane ocetne kisline z 2H-NMR temelji na podobni metodi, ki je že normalizirana za analizo vina. Ta evropski standard se ne uporablja za kompleksne matrice, katerih sestavina je kis, npr. balzamični kis.

General Information

Status
Published
Publication Date
08-Jan-2013
Current Stage
9093 - Decision to confirm - Review Enquiry
Completion Date
11-Sep-2019

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2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Kis - Izotopska analiza ocetne kisline in vode - 1. del: 2H-NMR-analiza ocetne kislineEssig - Isotopenanalyse von Essigsäure und Wasser - Teil 1: 2H-NMR-Analyse von EssigsäureVinaigre - Analyse isotopique de l'acide acétique et de l'eau - Partie 1: Analyse RMN-2H de l'acide acétiqueVinegar - Isotopic analysis of acetic acid and water - Part 1: 2H-NMR analysis of acetic acid67.220.20Dodatki jedemFood additivesICS:Ta slovenski standard je istoveten z:EN 16466-1:2013SIST EN 16466-1:2013en,fr,de01-junij-2013SIST EN 16466-1:2013SLOVENSKI
STANDARD



SIST EN 16466-1:2013



EUROPEAN STANDARD NORME EUROPÉENNE EUROPÄISCHE NORM
EN 16466-1
January 2013 ICS 67.220.10
English Version
Vinegar - Isotopic analysis of acetic acid and water - Part 1:
2H-NMR analysis of acetic acid
Vinaigre - Analyse isotopique de l'acide acétique et de l'eau - Partie 1: Analyse RMN-2H de l'acide acétique
Essig - Isotopenanalyse von Essigsäure und Wasser - Teil 1: 2H-NMR-Analyse von Essigsäure This European Standard was approved by CEN on 3 November 2012.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
Management Centre:
Avenue Marnix 17,
B-1000 Brussels © 2013 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN 16466-1:2013: E SIST EN 16466-1:2013



EN 16466-1:2013 (E) 2 Contents Page Foreword . 3 Introduction . 4 1 Scope . 5 2 Normative references . 5 3 Principle. 5 4 Reagents . 5 5 Apparatus . 6 6 Procedure . 6 7 Precision . 8 8 Test report . 9 Annex A (informative)
Results of the collaborative study (2009) . 10 Bibliography. 11
SIST EN 16466-1:2013



EN 16466-1:2013 (E) 3 Foreword This document (EN 16466-1:2013) has been based on an international collaborative study of the methods published in Analytica Chimica Acta 649 (2009) 98-105, and organised under the auspices of the Permanent International Vinegar Committee (CPIV, Brussels). This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by July 2013, and conflicting national standards shall be withdrawn at the latest by July 2013. Attention is drawn to the possibility that some
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