Bitumen and bituminous binders - Determination of recovered binder and oil distillate from bitumen emulsions by distillation

This EN specifies a method for determining the tensile properties of a bituminous binder, in particular those of polymer-modified bitumens by means of a force ductility test.

Bitumen und bitumenhaltige Bindemittel - Bestimmung des Destillationsrückstandes und des Őldestillates von Bitumenemulsionen mittels Destillation

Diese Europäische Norm legt ein Verfahren zur quantitativen Bestimmung des verbleibenden Bindemittels und des Öldestillates in Bitumenemulsionen fest.
Das Verfahren kann auch angewendet werden, um den Rückstand und das Destillat für weitere Untersuchungen zu gewinnen.
ANMERKUNG   Die an den mit diesem Verfahren gewonnenen Materialien ermittelten Stoffeigenschaften gleichen nicht unbedingt denen der Ausgangsstoffe, aus denen die Emulsion hergestellt wurde; dies gilt besonders für polymermodifizierte Bitumen.

Bitumes et liants bitumineux - Détermination par distillation du liant résiduel et du distillat d'huile dans les émulsions de bitume

La présente Norme européenne prescrit une méthode de détermination quantitative du liant résiduel et du distillat d'huile dans des émulsions de bitume.
La présente méthode d'essai peut également être utilisée pour obtenir du liant résiduel et du distillat d'huile pour des essais ultérieurs.
NOTE   Les propriétés du matériau récupéré par le présent essai ne sont pas nécessairement les mêmes que celles des matériaux d'origine à partir desquels on a produit l'émulsion, et ce plus particulièrement pour les bitumes modifiés par des polymères.
AVERTISSEMENT - L'utilisation de la présente norme européenne peut impliquer l'intervention de produits, d'opérations et d'équipements à caractère dangereux. La présente norme européenne n’est pas censée aborder tous les problèmes de sécurité associés à son usage. Il est de la responsabilité de l'utilisateur de consulter et d'établir des règles de sécurité et d'hygiène appropriées et de déterminer l'applicabilité des restrictions réglementaires avant utilisation.

Bitumen in bitumenska veziva - Določevanje veziva in oljnega destilata v bitumenskih emulzijah z metodo destilacije

General Information

Status
Withdrawn
Public Enquiry End Date
19-Nov-2007
Publication Date
11-Jun-2009
Withdrawal Date
16-May-2018
Technical Committee
Current Stage
9900 - Withdrawal (Adopted Project)
Start Date
17-May-2018
Due Date
09-Jun-2018
Completion Date
17-May-2018

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2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Bitumes et liants bitumineux - Détermination par distillation du liant résiduel et du distillat d'huile dans les émulsions de bitumeBitumen and bituminous binders - Determination of recovered binder and oil distillate from bitumen emulsions by distillation91.100.50Veziva. Tesnilni materialiBinders. Sealing materials75.140Voski, bitumni in drugi naftni proizvodiWaxes, bituminous materials and other petroleum productsICS:Ta slovenski standard je istoveten z:EN 1431:2009SIST EN 1431:2009en,fr,de01-julij-2009SIST EN 1431:2009SLOVENSKI
STANDARDSIST EN 1431:20001DGRPHãþD



SIST EN 1431:2009



EUROPEAN STANDARDNORME EUROPÉENNEEUROPÄISCHE NORMEN 1431March 2009ICS 75.140; 91.100.50Supersedes EN 1431:1999
English VersionBitumen and bituminous binders - Determination of residualbinder and oil distillate from bitumen emulsions by distillationBitumes et liants bitumineux - Détermination par distillationdu liant résiduel et du distillat d'huile dans les émulsions debitumeBitumen und bitumenhaltige Bindemittel - Bestimmung desDestillationsrückstandes und des Öldestillates vonBitumenemulsionen mittels DestillationThis European Standard was approved by CEN on 17 January 2009.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained on application to the CEN Management Centre or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as theofficial versions.CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland,France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMITÉ EUROPÉEN DE NORMALISATIONEUROPÄISCHES KOMITEE FÜR NORMUNGManagement Centre:
Avenue Marnix 17,
B-1000 Brussels© 2009 CENAll rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN 1431:2009: ESIST EN 1431:2009



EN 1431:2009 (E) 2 Contents Page Foreword .3 1 Scope .4 2 Normative references .4 3 Terms and definitions .4 4 Principle .5 5 Reagents and materials .5 6 Apparatus .5 7 Sampling .6 8 Procedure .6 9 Calculation .7 10 Expression of results .7 11 Precision .8 12 Test report .8 Annex A (normative)
Characteristics of thermometer . 12 Bibliography . 13
SIST EN 1431:2009



EN 1431:2009 (E) 3 Foreword This document (EN 1431:2009) has been prepared by Technical Committee CEN/TC 336 “Bituminous binders”, the secretariat of which is held by AFNOR. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by September 2009, and conflicting national standards shall be withdrawn at the latest by September 2009. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN [and/or CENELEC] shall not be held responsible for identifying any or all such patent rights. This document supersedes EN 1431:1999. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom. SIST EN 1431:2009



EN 1431:2009 (E) 4 1 Scope This European Standard specifies a method for the quantitative determination of residual binder and oil distillate in bituminous emulsions. The method can also be used to obtain residue and oil distillate for further testing. NOTE The properties of the material recovered in the test are not necessarily the same as those of the original materials from which the emulsion was produced, especially for polymer modified bitumens. WARNING — The use of this standard may involve hazardous materials, operations and equipment. This standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 58, Bitumen and bituminous binders – Sampling bituminous binders EN 573-3, Aluminium and aluminium alloys - Chemical composition and form of wrought products - Part 3: Chemical composition and form of products EN 1425, Bitumen and bituminous binders – Characterization of perceptible properties EN 12594, Bitumen and bituminous binders - Preparation of test samples ISO 565, Test sieves - Metal wire cloth, perforated plate and electroformed sheet - Nominal sizes of openings 3 Terms and definitions For the purposes of this document, the following definitions apply. 3.1 oil distillate hydrocarbon fraction which is distilled and collected in the graduated cylinder under conditions specified in this test 3.2 residual binder residue from a bituminous emulsion after distillation of water and oil distillate NOTE Although mentioned as "recovered binder content" in the EN 13808 specification standard, the residual binder by distillation is being considered in that case. The EN 13808 specification standard specifies the "recovered binder content" according to EN 1431, although the appropriate denomination is "residual binder after distillation". Consequently, it is highly recommended that this correction should be considered when revising the EN 13808 standard. SIST EN 1431:2009



EN 1431:2009 (E) 5 4 Principle Water and oil distillate are distilled from the bituminous emulsion, and separated in a graduated cylinder, leaving a residue of residual binder. 5 Reagents and materials 5.1 Cleaning agents, as used conventionally in a laboratory. 5.2 Sodium hydroxide solution, 40 g/l. 6 Apparatus Usual laboratory apparatus and glassware, together with the following: NOTE For details of assembly of the distillation apparatus for the test, see Figure 3. 6.1 Aluminium alloy still (see Figure 1) or iron still, (241+ 5) mm in height by (101 + 1) mm external diameter with a (3,2 + 0,2) mm thickness wall and a (125 + 5) mm inside diameter ring burner, having holes on the inner circumference and having three appropriate spacers or guide pins, to ensure centring of burner around the still (see Figure 2). Lid (see Figure 1) of suitable dimensions to allow two thermome
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