Bituminous mixtures - Test methods - Part 7: Determination of the bulk density of bituminous specimens by gamma rays

This document specifies a method for measuring the bulk density of pavement mixtures using a transmission-type gamma radiation test bench.
This method applies to cylindrical specimens or blocks, prepared in a laboratory or cut from a pavement, the thickness and the mass absorption coefficient which is a function of the chemical composition are known. The thickness of the specimen body traversed by the radiation shall be between 30 mm and 300 mm.
The method cannot be applied to materials containing slags, with variable metal content or chemical composition.
NOTE   Material containing metal or chemical compositions can affect the absorption of gamma rays.

Asphalt - Prüfverfahren - Teil 7: Bestimmung der Raumdichte von Asphalt-Probekörpern mit Gammastrahlen

Dieses Dokument beschreibt ein Verfahren, mit dem die Raumdichte von Asphaltgemischen für Fahrbahnbeläge gemessen wird, wenn eine Durchstrahlungseinrichtung mit Gammastrahlung verwendet wird.
Dieses Verfahren gilt für zylindrische oder blockförmige, im Labor hergestellte oder einem Fahrbahnbelag entnommene Probekörper, deren Dicke und von der chemischen Zusammensetzung abhängiger Massenabsorptionskoeffizient bekannt sind. Die Dicke des Probekörpers, der bei der Messung von Gammastrahlen durchdrungen wird, muss zwischen 30 mm und 300 mm betragen.
Dieses Verfahren kann nicht auf Materialien angewendet werden, die Schlacken enthalten oder über unterschiedliche Metallgehalte oder unterschiedliche chemische Zusammensetzungen verfügen.
ANMERKUNG   Materialien mit Metallgehalten oder mit chemischer Zusammensetzung können die Absorption der Gammastrahlen verändern.

Mélanges bitumineux - Méthodes d’essai - Partie 7 : Détermination de la masse volumique apparente des éprouvettes bitumineuses par les rayons gamma

Le présent document décrit une méthode de mesure de la masse volumique apparente des matériaux de chaussée au moyen d’un banc d’essai à rayons gamma par transmission.
Cette méthode s’applique à des éprouvettes cylindriques ou blocs parallélépipédiques, préparés en laboratoire ou découpés dans une chaussée. L’épaisseur et le coefficient d’absorption massique qui est fonction de la composition chimique sont connus. L’épaisseur du corps d’éprouvette traversé par le rayonnement doit être comprise entre 30 mm et 300 mm.
La méthode ne peut être appliquée à des matériaux contenant des laitiers présentant une teneur en métal ou une composition chimique variable.
NOTE Les matériaux contenant du métal ou présentant des compositions chimiques variables peuvent affecter l’absorption des rayons gamma.

Bitumenske zmesi - Preskusne metode - 7. del: Ugotavljanje gostote bitumenskih preskušancev z žarki gama

Ta dokument določa metodo za merjenje gostote vozišč s preskusno mizo za oddajanje žarkov gama.
Ta metoda se uporablja za valjaste preskušance ali bloke, pripravljene v laboratoriju ali izrezane iz vozišč, katerih debelina in koeficient absorpcije mase, kar je funkcija kemične sestave, sta znana. Debelina vzorca telesa, skozi katerega poteka sevanje, mora biti med 30 mm in 300 mm.
Metode ni mogoče uporabljati za snovi, ki vsebujejo žlindre ali s spremenljivo vsebnostjo kovin ali kemijsko sestavo.
OPOMBA:   Snovi z vsebnostjo kovin ali kemijsko sestavo lahko vplivajo na absorpcijo žarkov gama.

General Information

Status
Published
Public Enquiry End Date
19-Jan-2021
Publication Date
14-Mar-2022
Technical Committee
Current Stage
6060 - National Implementation/Publication (Adopted Project)
Start Date
03-Mar-2022
Due Date
08-May-2022
Completion Date
15-Mar-2022

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SLOVENSKI STANDARD
SIST EN 12697-7:2022
01-april-2022
Nadomešča:
SIST EN 12697-7:2014
Bitumenske zmesi - Preskusne metode - 7. del: Ugotavljanje gostote bitumenskih
preskušancev z žarki gama
Bituminous mixtures - Test methods - Part 7: Determination of the bulk density of
bituminous specimens by gamma rays
Asphalt - Prüfverfahren - Teil 7: Bestimmung der Raumdichte von Asphalt-Probekörpern
mit Gammastrahlen
Mélanges bitumineux - Méthodes d’essai - Partie 7 : Détermination de la masse
volumique apparente des éprouvettes bitumineuses par les rayons gamma
Ta slovenski standard je istoveten z: EN 12697-7:2022
ICS:
93.080.20 Materiali za gradnjo cest Road construction materials
SIST EN 12697-7:2022 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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SIST EN 12697-7:2022

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SIST EN 12697-7:2022


EN 12697-7
EUROPEAN STANDARD

NORME EUROPÉENNE

February 2022
EUROPÄISCHE NORM
ICS 93.080.20 Supersedes EN 12697-7:2014
English Version

Bituminous mixtures - Test methods - Part 7:
Determination of the bulk density of bituminous
specimens by gamma rays
Mélanges bitumineux - Méthodes d'essai - Partie 7 : Asphalt - Prüfverfahren - Teil 7: Bestimmung der
Détermination de la masse volumique apparente des Raumdichte von Asphalt-Probekörpern mit Gamma-
éprouvettes bitumineuses par les rayons gamma Strahlen
This European Standard was approved by CEN on 26 December 2021.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.

This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and
United Kingdom.





EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2022 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN 12697-7:2022 E
worldwide for CEN national Members.

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SIST EN 12697-7:2022
EN 12697-7:2022 (E)
Contents Page
European foreword . 3
Introduction . 4
1 Scope . 5
2 Normative references . 5
3 Terms and definitions . 5
4 Principle . 5
5 Apparatus . 5
6 Preparation of specimens . 6
7 Procedure. 6
7.1 Prior adjustments . 6
7.2 Choice of beam diameter . 7
7.3 Measurement procedure . 7
7.3.1 Measurement mode . 7
7.3.2 Continuous measurements . 7
7.3.3 Localized or point measurements . 8
8 Expression of results . 8
9 Test report . 10
10 Precision . 10
Bibliography . 11

2

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SIST EN 12697-7:2022
EN 12697-7:2022 (E)
European foreword
This document (EN 12697-7:2022) has been prepared by Technical Committee CEN/TC 227 “Road
materials”, the secretariat of which is held by BSI.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by August 2022, and conflicting national standards shall be
withdrawn at the latest by August 2022.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
This document supersedes EN 12697-7:2014.
The main changes compared to the previous edition are listed below:
— the title no longer refers to hot mix asphalt;
— [ge] editorial update according to current standard template;
— Clause 1, scope clarified according the CEN/CENELEC Internal Regulations Part 3:2019, 14.5;
— Clause 4, deletion of the exponential law including equation. Added reference to Clause 8;
1)
— (5.1), footnote amended to NOTE. Existing NOTE amended to normal text;
— Clause 6, NOTE 1: The period for when specimens are considered to be dry amended to 4 h in line
with other parts;
2)
— Clause 6, Footnote amended to NOTE 2. Existing NOTE amended to NOTE 1;
— Clause 6, measurement of the thickness of specimen replaced by “shall be known”;
— (7.3.3), formula for consistency test deleted and replaced with reference to Formula (1);
— Clause 8, editorial adjustments, renumbered formulas and addition of references to formulas;
— Clause 9, revision of data to be reported;
— Clause 10, completion of standard edition to read ISO 5725-2;
— [ge] bibliography added.
A list of all parts in the EN 12697 series can be found on the CEN website.
Any feedback and questions on this document should be directed to the users’ national standards body.
A complete listing of these bodies can be found on the CEN website.
According to the CEN-CENELEC Internal Regulations, the national standards organisations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia,
Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland,
Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Republic of North
Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United
Kingdom.
3

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SIST EN 12697-7:2022
EN 12697-7:2022 (E)
Introduction
Bulk density measurement in the laboratory using gamma rays is a method which does not affect the
properties of the material. It can be included in a series of tests carried out on a given sample. It allows
the plotting of a density chart or gradient.
4

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SIST EN 12697-7:2022
EN 12697-7:2022 (E)
1 Scope
This document specifies a method for measuring the bulk density of pavement mixtures using a
transmission-type gamma radiation test bench.
This method applies to cylindrical specimens or parallelepipedal blocks, prepared in a laboratory or cut
from a pavement. The thickness and the mass absorption coefficient, which is a function of the chemical
composition, are known. The thickness of the specimen body traversed by the radiation is between
30 mm and 300 mm.
The method cannot be applied to materials containing slags, with variable metal content or chemical
composition.
NOTE Material containing metal or chemical compositions can affect the absorption of gamma rays.
2 Normative references
The following documents are referred to in the text in such a way that some or all of their content
constitutes requirements of this document. For dated references, only the edition cited applies. For
undated references, the latest edition of the referenced document (including any amendments) applies.
EN 12697-6, Bituminous mixtures - Test methods - Part 6: Determination of bulk density of bituminous
specimens
3 Terms and definitions
For the purposes of this document, the following terms and definitions apply.
ISO and IEC maintain terminological databases for use in standardization at the following addresses:
— IEC Electropedia: available at https://www.electropedia.org/
— ISO Online browsing platform: available at https://www.iso.org/obp
4 Principle
The method is based upon the absorption of gamma radiation by the material under the conditions of the
test described in this document and for materials such as bituminous mixtures. The method follows an
exponential law according to Clause 8, Formulae (2) and (3).
The specimen is placed in the path of a gamma ray b
...

SLOVENSKI STANDARD
oSIST prEN 12697-7:2021
01-januar-2021
Bitumenske zmesi - Preskusne metode - 7. del: Ugotavljanje gostote bitumenskih
preskušancev z žarki gama
Bituminous mixtures - Test methods - Part 7: Determination of the bulk density of
bituminous specimens by gamma rays
Asphalt - Prüfverfahren - Teil 7: Bestimmung der Raumdichte von Asphalt-Probekörpern
mit Gamma-Strahlen
Mélanges bitumineux - Méthodes d'essai pour mélange hydrocarboné à chaud - Partie 7:
Détermination de la masse volumique apparente des éprouvettes bitumineuses par les
rayons gamma
Ta slovenski standard je istoveten z: prEN 12697-7
ICS:
93.080.20 Materiali za gradnjo cest Road construction materials
oSIST prEN 12697-7:2021 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------
oSIST prEN 12697-7:2021

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oSIST prEN 12697-7:2021


DRAFT
EUROPEAN STANDARD
prEN 12697-7
NORME EUROPÉENNE

EUROPÄISCHE NORM

November 2020
ICS 93.080.20 Will supersede EN 12697-7:2014
English Version

Bituminous mixtures - Test methods - Part 7:
Determination of the bulk density of bituminous
specimens by gamma rays
Mélanges bitumineux - Méthodes d'essai pour mélange Asphalt - Prüfverfahren - Teil 7: Bestimmung der
hydrocarboné à chaud - Partie 7: Détermination de la Raumdichte von Asphalt-Probekörpern mit Gamma-
masse volumique apparente des éprouvettes Strahlen
bitumineuses par les rayons gamma
This draft European Standard is submitted to CEN members for enquiry. It has been drawn up by the Technical Committee
CEN/TC 227.

If this draft becomes a European Standard, CEN members are bound to comply with the CEN/CENELEC Internal Regulations
which stipulate the conditions for giving this European Standard the status of a national standard without any alteration.

This draft European Standard was established by CEN in three official versions (English, French, German). A version in any other
language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC
Management Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and
United Kingdom.

Recipients of this draft are invited to submit, with their comments, notification of any relevant patent rights of which they are
aware and to provide supporting documentation.

Warning : This document is not a European Standard. It is distributed for review and comments. It is subject to change without
notice and shall not be referred to as a European Standard.


EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2020 CEN All rights of exploitation in any form and by any means reserved Ref. No. prEN 12697-7:2020 E
worldwide for CEN national Members.

---------------------- Page: 3 ----------------------
oSIST prEN 12697-7:2021
prEN 12697-7:2020 (E)
Contents Page
European foreword . 3
Introduction . 4
1 Scope . 5
2 Normative references . 5
3 Terms and definitions . 5
4 Principle . 6
5 Apparatus . 6
6 Preparation of specimens . 7
7 Procedure. 7
7.1 Prior adjustments . 7
7.2 Choice of beam diameter . 7
7.3 Measurement procedure . 7
8 Expression of results . 9
9 Test report . 10
10 Precision . 10
Bibliography . 11


2

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oSIST prEN 12697-7:2021
prEN 12697-7:2020 (E)
European foreword
This document (prEN 12697-7:2020) has been prepared by Technical Committee CEN/TC 227 “Road
materials”, the secretariat of which is held by BSI.
This document is currently submitted to the CEN Enquiry.
This document will supersede EN 12697-7:2014.
The main changes compared to the previous edition are listed below:
— the title no longer refers to hot mix asphalt;
— [ge] editorial update according to current standard template;
— [1] scope clarified according the CEN/CENELEC Internal Regulations Part 3:2019, 14.5;
— [4] the exponential law including equation deleted. Added reference to Clause 8;
— [5.1] footnote 1) amended to NOTE. Existing NOTE amended to normal text;
— [6] NOTE 1: The period for when specimens are considered to be dry amended to 4h in line with
other parts;
— [6] footnote 2) amended to NOTE 2. Existing NOTE amended to NOTE 1;
— [7.3.3] formula for consistency test deleted and replaced with reference to Formula (1);
— [8] editorial adjustments, renumbered formulas and addition of references to formulas.
A list of all parts in the EN 12697 series can be found on the CEN website
3

---------------------- Page: 5 ----------------------
oSIST prEN 12697-7:2021
prEN 12697-7:2020 (E)
Introduction
Bulk density measurement in the laboratory using gamma rays is a method which does not affect the
properties of the material. It can be included in a series of tests carried out on a given sample. It allows
the plotting of a density chart or gradient.
The safety regulations applicable to the use of gamma rays should be applied.
4

---------------------- Page: 6 ----------------------
oSIST prEN 12697-7:2021
prEN 12697-7:2020 (E)
1 Scope
This document specifies a method for measuring the bulk density of pavement mixtures using a
transmission-type gamma radiation test bench.
This method applies to cylindrical specimens or blocks, prepared in a laboratory or cut from a pavement,
the thickness and the mass absorption coefficient which is a function of the chemical composition are
known. The thickness of the specimen body traversed by the radiation shall be between 30 mm and
300 mm.
The method cannot be applied to materials containing slags, with variable metal content or chemical
composition.
NOTE Material containing metal or chemical compositions can affect the absorption of gamma rays.
2 Normative references
The following documents are referred to in the text in such a way that some or all of their content
constitutes requirements of this document. For dated references, only the edition cited applies. For
undated references, the latest edition of the referenced document (including any amendments) applies.
EN 12697-6, Bituminous mixtures - Test methods - Part 6: Determination of bulk density of bituminous
specimens
3 Terms and definitions
For the purposes of this document, the following terms and definitions apply.
ISO and IEC maintain terminological databases for use in standardization at the following addresses:
— IEC Electropedia: available at http://www.electropedia.org/
— ISO Online browsing platform: available at https://www.iso.org/obp
3.1
precision
closeness of agreement between independent test results obtained under stipulated conditions
Note 1 to entry: Precision depends only on the distribution of random errors and does not relate to the true value
or the specified value.
Note 2 to entry: The measure of precision is usually expressed in terms of imprecision and computed as a
standard deviation of the test results. Less precision is indicated by a larger standard deviation.
Note 3 to entry: “Independent test results” means results obtained in a manner not influenced by any previous
result on the same or similar test sample. Quantitative measures of precision depend critically on the stipulated
conditions. Repeatability and reproducibility conditions are particular sets of extreme conditions.
3.2
repeatability
precision under repeatability conditions
5

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oSIST prEN 12697-7:2021
prEN 12697-7:2020 (E)
3.3
repeatability conditions
conditions where independent tests results are obtained with the same method on identical test items in
the same laboratory by the same operator using the same equipment within short intervals of time
3.4
reproducibility
precision under reproducibility conditions
3.5
reproducibility conditions
conditions where test results are obtained with the same method on identical test items in different
laboratories with different operators using different equipment
4 Principle
The method is based upon the absorption of gamma radiation by the material. Under the conditions of
the test descri
...

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