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ASTM D6300-07

(Practice)

Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants

Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants

SCOPE
1.1 This practice covers the necessary preparations and planning for the conduct of interlaboratory programs for the development of estimates of precision (determinability, repeatability, and reproducibility) and of bias (absolute and relative), and further presents the standard phraseology for incorporating such information into standard test methods.
1.2 This practice is generally limited to homogeneous products with which serious sampling problems do not normally arise.
1.3 This practice may not be suitable for solid or semisolid products such as petroleum coke, industrial pitches, paraffin waxes, greases, or solid lubricants when the heterogeneous properties of the substances create sampling problems. In such instances, use Practice E 691 or consult a trained statistician.
1.4 A software program (ADJD6300) performs the necessary computations prescribed by this practice.

General Information

Status
Historical
Publication Date
30-Jun-2007
ICS
03.120.20 - Product and company certification. Conformity assessment
75.080 - Petroleum products in general
Technical Committee
D02 - Petroleum Products, Liquid Fuels, and Lubricants
Drafting Committee
D02.94 - Coordinating Subcommittee on Quality Assurance and Statistics
Current Stage
Ref Project

Relations

Replaces
ASTM D6300-06 - Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
Effective Date
01-Jul-2007
Replaced By
ASTM D6300-08 - Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
Effective Date
15-Dec-2008
Referred By
ASTM D8304-19 - Standard Test Method for Determination of Compounded Forms of Iron in In-service Fluids
Effective Date
01-Jul-2007
Referred By
ASTM D7797-23 - Standard Test Method for Determination of the Fatty Acid Methyl Esters Content of Aviation Turbine Fuel Using Flow Analysis by Fourier Transform Infrared Spectroscopy—Rapid Screening Method
Effective Date
01-Jul-2007
Referred By
ASTM D8126-21 - Standard Test Method for Efficient Basicity Determination by Potentiometric Hydrochloric Acid Titration
Effective Date
01-Jul-2007
Referred By
ASTM D8073-22 - Standard Test Method for Determination of Water Separation Characteristics of Aviation Turbine Fuel by Small Scale Water Separation Instrument
Effective Date
01-Jul-2007
Referred By
ASTM D4929-22 - Standard Test Method for Determination of Organic Chloride Content in Crude Oil
Effective Date
01-Jul-2007
Referred By
ASTM D5800-21 - Standard Test Method for Evaporation Loss of Lubricating Oils by the Noack Method
Effective Date
01-Jul-2007
Referred By
ASTM D7668-17 - Standard Test Method for Determination of Derived Cetane Number (DCN) of Diesel Fuel Oils—Ignition Delay and Combustion Delay Using a Constant Volume Combustion Chamber Method
Effective Date
01-Jul-2007
Referred By
ASTM D7220-22 - Standard Test Method for Sulfur in Automotive, Heating, and Jet Fuels by Monochromatic Energy Dispersive X-ray Fluorescence Spectrometry
Effective Date
01-Jul-2007
Referred By
ASTM D7060-20 - Standard Test Method for Determination of the Maximum Flocculation Ratio and Peptizing Power in Residual and Heavy Fuel Oils (Optical Detection Method)
Effective Date
01-Jul-2007
Referred By
ASTM D8519-23 - Standard Test Method for Determination of Hydrocarbon Types in Waste Plastic Process Oil Using Gas Chromatography with Vacuum Ultraviolet Absorption Spectroscopy Detection (GC-VUV)
Effective Date
01-Jul-2007
Referred By
ASTM D2887-22e1 - Standard Test Method for Boiling Range Distribution of Petroleum Fractions by Gas Chromatography
Effective Date
01-Jul-2007
Referred By
ASTM D8351-22 - Standard Test Method for Determination of Trace Elements in Biodiesel and Biodiesel Blends by Microwave Plasma Atomic Emission Spectrometry (MP-AES)
Effective Date
01-Jul-2007
Referred By
ASTM D3831-22 - Standard Test Method for Manganese in Gasoline By Atomic Absorption Spectroscopy
Effective Date
01-Jul-2007

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ASTM D6300-07 - Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and LubricantsASTM D6300-07 - Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
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ASTM D6300-07 - Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
An American National Standard
Designation:D6300–07
Standard Practice for
Determination of Precision and Bias Data for Use in Test
1
Methods for Petroleum Products and Lubricants
This standard is issued under the fixed designation D 6300; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
INTRODUCTION
2
Both Research Report RR:D02–1007, Manual on Determining Precision Data for ASTM Methods
2
on Petroleum Products and Lubricants and the ISO 4259, benefitted greatly from more than 50 years
of collaboration betweenASTM and the Institute of Petroleum (IP) in the UK. The more recent work
was documented by the IP and has become ISO 4259.
ISO 4259 encompasses both the determination of precision and the application of such precision
2
data. In effect, it combines the type of information in RR:D02–1007 regarding the determination of
the precision estimates and the type of information in Practice D 3244 for the utilization of test data.
2
The following practice, intended to replace RR:D02–1007, differs slightly from related portions of
the ISO standard. This new practice is consistent with the computer software, ADJD6300 D2PP,
Version 4.43, Determination of Precision and Bias Data for Use in Test Methods for Petroleum
3
Products.
1. Scope 2. Referenced Documents
4
1.1 This practice covers the necessary preparations and 2.1 ASTM Standards:
planning for the conduct of interlaboratory programs for the D 123 Terminology Relating to Textiles
development of estimates of precision (determinability, repeat- D 3244 Practice for Utilization of Test Data to Determine
ability, and reproducibility) and of bias (absolute and relative), Conformance with Specifications
and further presents the standard phraseology for incorporating E29 Practice for Using Significant Digits in Test Data to
such information into standard test methods. Determine Conformance with Specifications
1.2 This practice is generally limited to homogeneous prod- E 456 Terminology Relating to Quality and Statistics
ucts with which serious sampling problems do not normally E 691 Practice for Conducting an Interlaboratory Study to
arise. Determine the Precision of a Test Method
1.3 This practice may not be suitable for solid or semisolid 2.2 ISO Standards:
products such as petroleum coke, industrial pitches, paraffin ISO 4259 Petroleum Products-Determination and Applica-
5
waxes, greases, or solid lubricants when the heterogeneous tion of Precision Data in Relation to Methods of Test
properties of the substances create sampling problems. In such 2.3 ASTM Adjuncts:
instances, use Practice E 691 or consult a trained statistician. ADJD6300 D2PP, Version 4.43, Determination of Preci-
1.4 A software program (ADJD6300) performs the neces- sion and Bias Data for Use in Test Methods for Petroleum
3
sary computations prescribed by this practice. Products
3. Terminology
1
This practice is under the jurisdiction of ASTM Committee D02 on Petroleum
3.1 Definitions:
Products and Lubricants and is the direct responsibility of Subcommittee D02.94 on
Coordinating Subcommittee on Quality Assurance and Statistics.
4
Current edition approved July 1, 2007. Published September 2007. Originally For referenced ASTM standards, visit the ASTM website, www.astm.org, or
approved in 1998. Last previous edition approved in 2006 as D 6300–06. contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
2
Supporting data have been filed at ASTM International Headquarters and may Standards volume information, refer to the standard’s Document Summary page on
be obtained by requesting Research Report RR:D02–1007. the ASTM website.
3 5
Available from ASTM International Headquarters. Order Adjunct No. Available from International Organization for Standardization, 1 rue de
ADJD6300. Varembé, Case postale 56, CH-1211 Geneva 20, Switzerland.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D6300–07
3.1.1 analysis of variance (ANOVA), n—a procedure for to the definitions of each of these terms for greater detail.
2
dividing the total variation of a set of data into two or more RR:D02–1007
parts, one of which estimates the error due to selecting and
3.1.10 random error, n—the chance variation encountered
testing specimens and the other part(s) possible sources of
in all test work despite the closest control of variables.
2
added variation. D 123
RR:D02–1007
3.1.2 bias, n—the difference between the population mean
3.1.11 repeatability, n—the quantitative expression of t
...

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1.1 These test methods cover the physical properties associated with preformed expansion joint fillers. The test methods include:    
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Note 1: Specific test methods are applicable only to certain types of joint fillers, as stated herein.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
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