Standard Practice for Determination of Volatile Organic Compounds (Excluding Formaldehyde) Emissions from Wood-Based Panels Using Small Environmental Chambers Under Defined Test Conditions

SIGNIFICANCE AND USE
The effects of VOC sources on the indoor air quality in buildings have not been well established. One basic requirement that has emerged from indoor air quality studies is the need for well-characterized test data on the emission factors of VOCs from building materials. Standard test method and procedure are a requirement for the comparison of emission factor data from different products.
This practice describes a procedure for using a small environmental test chamber to determine the emission factors of VOCs from wood-based panels over a specified period of time. A pre-screening analysis procedure is also provided to identify the VOCs emitted from the products, to determine the appropriate GC/MS or GC/FID analytical procedure, and to estimate required sampling volume for the subsequent environmental chamber testing.
Test results obtained using this practice provide a basis for comparing the VOC emission characteristics of different wood-based panel products. The emission data can be used to inform manufacturers of the VOC emissions from their products. The data can also be used to identify building materials with reduced VOC emissions over the time interval of the test.
While emission factors determined by using this practice can be used to compare different products, the concentrations measured in the chamber shall not be considered as the resultant concentrations in an actual indoor environment.
SCOPE
1.1 The practice measures the volatile organic compounds (VOC), excluding formaldehyde, emitted from manufactured wood-based panels. A pre-screening analysis is used to identify the VOCs emitted from the panel. Emission factors (that is, emission rates per unit surface area) for the VOCs of interest are then determined by measuring the concentrations in a small environmental test chamber containing a specimen. The test chamber is ventilated at a constant air change rate under the standard environmental conditions. For formaldehyde determination, see Test Method D 6007.
1.2 This practice describes a test method that is specific to the measurement of VOC emissions from newly manufactured individual wood-based panels, such as particleboard, plywood, and oriented strand board (OSB), for the purpose of comparing the emission characteristics of different products under the standard test condition. For general guidance on conducting small environmental chamber tests, see Guide D 5116.
1.3 VOC concentrations in the environmental test chamber are determined by adsorption on an appropriate single adsorbent tube or multi-adsorbent tube, followed by thermal desorption and combined gas chromatograph/mass spectrometry (GC/MS) or gas chromatograph/flame ionization detection (GC/FID). The air sampling procedure and the analytical method recommended in this practice are generally valid for the identification and quantification of VOCs with saturation vapor pressure between 500 and 0.01 kPa at 25°C, depending on the selection of adsorbent(s).
Note 1—VOCs being captured by an adsorbent tube depend on the adsorbent(s) and sampling procedure selected (see Practice D 6196). The user should have a thorough understanding of the limitations of each adsorbent used.
1.4 The emission factors determined using the above procedure describe the emission characteristics of the specimen under the standard test condition. These data can be used directly to compare the emission characteristics of different products and to estimate the emission rates up to one month after the production. They shall not be used to predict the emission rates over longer periods of time (that is, more than one month) or under different environmental conditions.
1.5 Emission data from chamber tests can be used for predicting the impact of wood-based panels on the VOC concentrations in buildings by using an appropriate indoor air quality model, which is beyond the scope of this practice.
1.6 The values stated in SI units shall be ...

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31-Jul-2008
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ASTM D6330-98(2008) - Standard Practice for Determination of Volatile Organic Compounds (Excluding Formaldehyde) Emissions from Wood-Based Panels Using Small Environmental Chambers Under Defined Test Conditions
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D6330 −98(Reapproved 2008)
Standard Practice for
Determination of Volatile Organic Compounds (Excluding
Formaldehyde) Emissions from Wood-Based Panels Using
Small Environmental Chambers Under Defined Test
1
Conditions
This standard is issued under the fixed designation D6330; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 1.4 The emission factors determined using the above pro-
cedure describe the emission characteristics of the specimen
1.1 The practice measures the volatile organic compounds
under the standard test condition. These data can be used
(VOC), excluding formaldehyde, emitted from manufactured
directly to compare the emission characteristics of different
wood-basedpanels.Apre-screeninganalysisisusedtoidentify
products and to estimate the emission rates up to one month
the VOCs emitted from the panel. Emission factors (that is,
after the production. They shall not be used to predict the
emission rates per unit surface area) for the VOCs of interest
emission rates over longer periods of time (that is, more than
arethendeterminedbymeasuringtheconcentrationsinasmall
one month) or under different environmental conditions.
environmental test chamber containing a specimen. The test
1.5 Emission data from chamber tests can be used for
chamber is ventilated at a constant air change rate under the
predicting the impact of wood-based panels on the VOC
standard environmental conditions. For formaldehyde
concentrations in buildings by using an appropriate indoor air
determination, see Test Method D6007.
quality model, which is beyond the scope of this practice.
1.2 This practice describes a test method that is specific to
1.6 The values stated in SI units shall be regarded as the
the measurement ofVOC emissions from newly manufactured
standard (see IEEE/ASTM SI-10).
individualwood-basedpanels,suchasparticleboard,plywood,
andorientedstrandboard(OSB),forthepurposeofcomparing 1.7 This practice does not purport to address all of the
safety concerns, if any, associated with its use. It is the
the emission characteristics of different products under the
standard test condition. For general guidance on conducting responsibility of the user of the standard to consult and
establish appropriate safety and health practices and deter-
small environmental chamber tests, see Guide D5116.
mine the applicability of regulatory limitations prior to use.
1.3 VOC concentrations in the environmental test chamber
For specified hazard statements see Section 6.
are determined by adsorption on an appropriate single adsor-
benttubeormulti-adsorbenttube,followedbythermaldesorp-
2. Referenced Documents
tionandcombinedgaschromatograph/massspectrometry(GC/
2
2.1 ASTM Standards:
MS) or gas chromatograph/flame ionization detection (GC/
D1356Terminology Relating to Sampling and Analysis of
FID). The air sampling procedure and the analytical method
Atmospheres
recommended in this practice are generally valid for the
D1914PracticeforConversionUnitsandFactorsRelatingto
identificationandquantificationofVOCswithsaturationvapor
Sampling and Analysis of Atmospheres
pressure between 500 and 0.01 kPa at 25°C, depending on the
D5116Guide for Small-Scale Environmental Chamber De-
selection of adsorbent(s).
terminationsofOrganicEmissionsfromIndoorMaterials/
Products
NOTE 1—VOCs being captured by an adsorbent tube depend on the
adsorbent(s) and sampling procedure selected (see Practice D6196). The
D6007TestMethodforDeterminingFormaldehydeConcen-
user should have a thorough understanding of the limitations of each
trations in Air from Wood Products Using a Small-Scale
adsorbent used.
Chamber
D6196Practice for Selection of Sorbents, Sampling, and
1
This practice is under the jurisdiction of ASTM Committee D22 on Air
2
Qualityand is the direct responsibility of Subcommittee D22.05 on Indoor Air. For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Current edition approved Aug. 1, 2008. Published September 2008. Originally contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
approved in 1998. Last previous edition approved in 2003 as D6330-98 (2003). Standards volume information, refer to the standard’s Document Summary page on
DOI: 10.1520/D6330-98R08. the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
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D6330−98 (2008)
Thermal Desorption Analysis Procedures for Volatile Or- depend on the collection and desorption efficiency of the
ganic Compounds in Air
...

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