ASTM E1775-01

Standard Guide for Evaluating Performance of On-Site Extraction and Field-Portable Electrochemical or Spectrophotometric Analysis for Lead

SCOPE
1.1 This standard provides guidelines for determining the performance of field-portable quantitative lead analysis instruments.
1.2 This guide applies to field-portable electroanalytical and spectrophotometric (including reflectance and colorimetric) analyzers.
1.3 Sample matrices of concern herein include paint, dust, soil, and airborne particulate.
1.4 This guide addresses the desired performance characteristics of field-based sample extraction procedures for lead, as well as on-site extraction followed by field-portable analysis.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

• Status: Historical
• Publication Date: 09-Oct-2001
• ICS: 71.040.50 - Physicochemical methods of analysis
• Technical Committee: E06 - Performance of Buildings

Relations

• Replaces: ASTM E1775-96 - Standard Guide for Evaluating Performance of On-Site Extraction and Field-Portable Electrochemical or Spectrophotometric Analysis for Lead
• Effective Date: 10-Oct-2001
• Replaced By: ASTM E1775-07 - Standard Guide for Evaluating Performance of On-Site Extraction and Field-Portable Electrochemical or Spectrophotometric Analysis for Lead
• Effective Date: 01-Aug-2007
• Referred By: ASTM E631-15 - Standard Terminology of Building Constructions
• Effective Date: 10-Oct-2001
• Referred By: ASTM E1979-21 - Standard Practice for Ultrasonic Extraction of Paint, Dust, Soil, and Air Samples for Subsequent Determination of Lead
• Effective Date: 10-Oct-2001

Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:E1775–01
Standard Guide for
Evaluating Performance of On-Site Extraction and Field-
Portable Electrochemical or Spectrophotometric Analysis
1
for Lead
This standard is issued under the fixed designation E 1775; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope E 1645 Practice for Preparation of Dried Paint Samples for
3
Subsequent Lead Analysis by Atomic Spectrometry
1.1 This standard provides guidelines for determining the
E 1726 Practice for Sample Digestion of Soils for Determi-
performance of field-portable quantitative lead analysis instru-
3
nation of Lead by Atomic Spectrometry
ments.
E 1727 Practice for Field Collection of Soil Samples for
1.2 This guide applies to field-portable electroanalytical and
3
Lead Determination by Atomic Spectrometry Techniques
spectrophotometric (including reflectance and colorimetric)
E 1728 Practice for Field Collection of Settled Dust
analyzers.
Samples Using Wipe Sampling Methods for Lead Deter-
1.3 Sample matrices of concern herein include paint, dust,
3
mination by Atomic Spectrometry Techniques
soil, and airborne particulate.
E 1729 Practice for Field Collection of Dried Paint Samples
1.4 This guide addresses the desired performance character-
for Lead Determination by Atomic Spectrometry Tech-
istics of field-based sample extraction procedures for lead, as
3
niques
well as on-site extraction followed by field-portable analysis.
E 1741 Practice for Preparation of Airborne Particulate
1.5 This standard does not purport to address all of the
Lead Samples Collected During Abatement and Construc-
safety concerns, if any, associated with its use. It is the
tion Activities for Subsequent Analysis by Atomic Spec-
responsibility of the user of this standard to establish appro-
3
trometry
priate safety and health practices and determine the applica-
E 1864 Practice for Evaluating Quality Systems of Organi-
bility of regulatory limitations prior to use.
zations Engaged in Conducting Facility and Hazard As-
2. Referenced Documents
sessments to Determine the Presence and Extent of Lead in
3
Paint,Dust, Airborne Particulate, and Soil
2.1 ASTM Standards:
2.2 U.S. EPA Documents:
D 5438 Practice for Collection of Floor Dust for Chemical
2
EPA 600/R-93/200 Standard Operating Procedure for the
Analysis
Field Analysis of Lead in Paint, Bulk Dust, and Soil by
E 1553 Practice for Collection ofAirborne Particulate Lead
3
Ultrasonic,AcidDigestionandColorimetricMeasurement
During Abatement and Construction Activities
4
(1993)
E 1605 Terminology Relating to Abatement of Hazards
EPA 747-R-92-001 Laboratory Accreditation Guidelines:
from Lead-Based Paint in Buildings and Related Struc-
5
3
Measurement of Lead in Paint, Dust, and Soil (1992)
tures
E 1613 Test Method for Analysis of Digested Samples for
3. Terminology
Lead by Inductively Coupled Plasma Atomic Emission
3.1 For definitions of terms not listed here, seeTerminology
Spectrometry (ICP-AES), Flame Atomic Absorption
E 1605.
(FAAS),orGraphiteFurnaceAtomicAbsorption(GFAAS)
3
3.2 anodic stripping voltammetry—an electroanalytical
Techniques
technique in which the concentration of analyte metal species
E 1644 Practice for Hot Plate Digestion of Dust Wipe
dissolved in solution is determined in the following manner.
Samples for Determination of Lead by Atomic Spectrom-
3
The analyte is first deposited (preconcentrated) electrochemi-
etry
cally by reducing the dissolved ion in solution to immobilized
metal species at a mercury electrode surface. The metal is
1
This guide is under the jurisdiction of ASTM Committee E06 on Performance
of Buildings and is the direct responsibility of Subcommittee E06.23 on Lead
Hazards in Buildings.
4
Current edition approved Oct. 10, 2001. Published November 2001. Originally Available from U.S. EPA, Office of Research and Development, Research
published as E 1775–96. Last previous edition E 1775–96. Triangle Park, NC.
2 5
Annual Book of ASTM Standards, Vol 11.03. Available from U.S. EPA, Office of Pollution Prevention andToxic Substances,
3
Annual Book of ASTM Standards, Vol 04.11. Washington, DC.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
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E1775–01
deposited in the form of an amalgam (with Hg) at an applied 5.2 Real-World Materials:
potential (voltage) which is negative of the standard oxidation 5.2.1 Paint, collected using Practice E 1729 (or equivalent).
potential for the metal/ion redox couple. After deposition, the To obtain reference values, determine l
...