Crude petroleum - Determination of water - Distillation method (ISO 9029:1990)

The precision data of this procedure have only been determined for water contents up to 1 % (V/V). Includes principle, apparatus, solvent, calibration and recovery test, sampling, procedure, expression of results, precision and test report. The distillation apparatus is shown in figures 1 and 2. The precision of the method is shown in figure 3. The sample handling is described in annex A.

Rohöl - Bestimmung des Wassergehaltes - Destillationsverfahren (ISO 9029:1990)

Pétrole brut - Détermination de la teneur en eau - Méthode de distillation (ISO 9029:1990)

La présente Norme internationale prescrit une méthode de détermination de la teneur en eau des pétroles bruts par distillation. Les valeurs de fidélité n'ont été déterminées que pour des teneurs en eau allant jusqu'à 1 % (V/V).

Surova nafta - Določevanje vode - Destilacijska metoda (ISO 9029:1990)

General Information

Status
Published
Publication Date
08-Aug-1995
Current Stage
9093 - Decision to confirm - Review Enquiry
Start Date
17-Mar-2012
Completion Date
17-Mar-2012

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Standards Content (Sample)

SLOVENSKI STANDARD
SIST EN ISO 9029:1998
01-maj-1998
6XURYDQDIWD'RORþHYDQMHYRGH'HVWLODFLMVNDPHWRGD ,62
Crude petroleum - Determination of water - Distillation method (ISO 9029:1990)
Rohöl - Bestimmung des Wassergehaltes - Destillationsverfahren (ISO 9029:1990)
Pétrole brut - Détermination de la teneur en eau - Méthode de distillation (ISO
9029:1990)
Ta slovenski standard je istoveten z: EN ISO 9029:1995
ICS:
75.040 Surova nafta Crude petroleum
SIST EN ISO 9029:1998 en
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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SIST EN ISO 9029:1998

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SIST EN ISO 9029:1998

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SIST EN ISO 9029:1998

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SIST EN ISO 9029:1998
INTERNATIONAL
STANDARD
First edition
1990-l 2-l 5
Crude petroleum - Determination of water -
Distillation method
- CWermination de ia feneur en eau - M6thode de
P&hole brut
dis tilla fion
Reference number
is0 9029: 1990(E)

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SIST EN ISO 9029:1998
IS0 90293 990(E)
Foreword
IS0 (the International Organization for Standardization) is a worldwide
federation of national standards bodies (IS0 member bodies). The work
of preparing International Standards is normally carried out through IS0
technical committees. Each member body interested in a subject for
which a technical committee has been established has the right to be
represented on that committee. International organizations, govern-
mental and non-governmental, in liaison with ISO, also take part in the
work. IS0 collaborates closely with the International Electrotechnical
Commission (IEC) on all matters of electrotechnical standardization.
Draft International Standards adopted by the technical committees are
circulated to the member bodies for voting. Publication as an lnter-
national Standard requires approval by at least 75 % of the member
bodies casting a vote.
International Standard IS0 9029 was prepared by Technical Committee
ISO/TC 28, Petroleum products and lubricants.
Annex A forms an integral part of this International Standard.
0 IS0 1990
All rights reserved. No part of this publication may be reproduced or utilized in any form
or by any means, electronic or mechanical, including photocopying and microfilm, without
permission in writing from the publisher.
International Organization for Standardization
Case Postale 56 l Cl-I-121 1 Genkve 20 l Switzerland
Printed in Switzerland
ii

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SIST EN ISO 9029:1998
_-- ~- -
INTERNATIONAL STANDARD IS0 9029:1990(E)
Determination of water - Distillation
Crude petroleum -
met hod
WARNlNG - The use of this International Standard may involve hazardous materials, operations and
equipment. This standard does not purport to address all of the safety problems associated with its use.
It is the responsibility of the user of this standard to establish appropriate safety and health practices
and determine the applicability of regulatory limitations prior to use.
3 Significance
1 Scope
A knowledge of the water content of crude oil is im-
This International Standard specifies a method for
portant in the refining, purchase, sale and transfer
determining water in crude oil by distillation. The
precision data have only been determined for water of products.
contents up to I % (V/v).
The amount of water as determined by this method
is used to correct the volume involved in the custody
transfer of oil.
2 Normative references
4 Principle
The following standards contain provisions which,
through reference in this text, constitute provisions A test portion is heated under reflux conditions with
of this International Standard. At the time of publi-
a water-immiscible solvent which co-distills with the
cation, the editions indicated were valid. All stan- water in the sample. Condensed solvent and water
dards are subject to revision, and parties to are continuously separated in a trap. The water set-
agreements based on this International Standard tles in the graduated section of the trap, and the
are encouraged to investigate the possibility of ap-
solvent returns to the distillation flask.
plying the most recent editions of the standards in-
dicated below. Members of IEC and IS0 maintain
registers of currently valid International Standards.
5 Apparatus
IS0 383:1976, Laboratory glassware - Interchange-
able conical ground joints. Usual laboratory apparatus, together with the fol-
lowing:
IS0 3170:1988, Petroleum liquids -- Manual
sampling.
5.1 General.
IS0 3171:1988, Petroleum liquids - Automatic pipe-
The recommended apparatus, shown in figure I,
line sampling.
consists of a glass distillation flask, a condenser, a
graduated
...

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