Advanced technical ceramics - Methods of test for ceramic coatings - Part 6: Determination of the abrasion resistance of coatings by a micro-abrasion wear test

This part of EN 1071 specifies a method for measuring the abrasive wear rate of ceramic coatings by means of a micro-scale abrasion wear test, based on the well known crater grinding technique used for film thickness determination (see EN 1071-2).
This method can provide data on both film and substrate wear rates, either by performing two separate tests or by careful analysis of data from a single test series.
The test method can be applied to samples with planar or non-planar surfaces but the analysis described in clause 9 applies only to flat samples. For non-planar samples, a more complicated analysis, possibly requiring the use of numerical methods, is required.

Hochleistungskeramik - Verfahren zur Prüfung keramischer Schichten - Teil 6: Bestimmung der Beständigkeit gegen Abriebverschleiß von Schichten mittels Mikroabriebprüfung

Dieser Teil von EN 1071 legt ein Verfahren zur Messung der Abriebverschleißrate keramischer Schichten durch eine Mikroabriebprüfung fest, die auf dem von der Bestimmung der Schichtdicke bekannten Kalottenschleifverfahren basiert (siehe EN 1071 2).
Nach diesem Verfahren können Daten zur Bestimmung der Abriebverschleißraten sowohl der Schicht als auch des Grundwerkstoffs ermittelt werden, indem entweder eine Prüfung für die Schicht und eine Prüfung für den Grundwerkstoff oder aber eine Analyse durchgeführt wird, bei der eine sorgfältige Auswertung der aus nur einer einzigen Prüfserie gewonnenen Daten erfolgt.
Das Prüfverfahren kann auf Proben mit ebenen oder nicht ebenen Flächen angewendet werden, während die im Abschnitt 9 beschriebene Analyse nur auf flache Proben anwendbar ist. Für nicht ebene Proben ist eine komplexere Analyse erforderlich, möglicherweise unter Anwendung numerischer Verfahren.

Céramiques techniques avancées - Méthodes d'essai pour revêtements céramiques - Partie 6 : Détermination de la résistance à l'abrasion des revêtements par essai de micro-usure

Sodobna tehnična keramika - Metode za preskušanje keramičnih prevlek - 6. del: Ugotavljanje odpornosti prevlek proti obrabi z mikroabrazivnim preskusom

General Information

Status
Withdrawn
Publication Date
06-Nov-2007
Withdrawal Date
19-Apr-2016
Current Stage
9960 - Withdrawal effective - Withdrawal
Completion Date
20-Apr-2016

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2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.HVNXVRPHochleistungskeramik - Verfahren zur Prüfung keramischer Schichten - Teil 6: Bestimmung der Beständigkeit gegen Abriebverschleiß von Schichten mittels MikroabriebprüfungCéramiques techniques avancées - Méthodes d'essai pour revêtements céramiques - Partie 6 : Détermination de la résistance à l'abrasion des revêtements par essai de micro-usureAdvanced technical ceramics - Methods of test for ceramic coatings - Part 6: Determination of the abrasion resistance of coatings by a micro-abrasion wear test81.060.30Sodobna keramikaAdvanced ceramics25.220.99Druge obdelave in prevlekeOther treatments and coatingsICS:Ta slovenski standard je istoveten z:EN 1071-6:2007SIST EN 1071-6:2009en,fr,de01-januar-2009SIST EN 1071-6:2009SLOVENSKI
STANDARDSIST ENV 1071-6:20071DGRPHãþD

EUROPEAN STANDARDNORME EUROPÉENNEEUROPÄISCHE NORMEN 1071-6November 2007ICS 81.060.30; 25.220.99; 17.040.20Supersedes ENV 1071-6:2002
English VersionAdvanced technical ceramics - Methods of test for ceramiccoatings - Part 6: Determination of the abrasion resistance ofcoatings by a micro-abrasion wear testCéramiques techniques avancées - Méthodes d'essai pourrevêtements céramiques - Partie 6 : Détermination de larésistance à l'abrasion des revêtements par essai de micro-usureHochleistungskeramik - Verfahren zur Prüfung keramischerSchichten - Teil 6: Bestimmung der Beständigkeit gegenAbriebverschleiß von Schichten mittels MikroabriebprüfungThis European Standard was approved by CEN on 30 September 2007.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained on application to the CEN Management Centre or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as theofficial versions.CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland,France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMITÉ EUROPÉEN DE NORMALISATIONEUROPÄISCHES KOMITEE FÜR NORMUNGManagement Centre: rue de Stassart, 36
B-1050 Brussels© 2007 CENAll rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN 1071-6:2007: ESIST EN 1071-6:2009

Measurement of coating thickness.19 Bibliography.20
Rockwell indentation test for evaluation of adhesion Part 9: Determination of fracture strain Part 10: Determination of coating thickness by cross sectioning Part 11: Determination of internal stress by the Stoney formula Part 5, a European pre-standard, was withdrawn in 2007. Part 7, a Technical Specification, was withdrawn in 2007, following publication of EN ISO 14577-4. At the time of publication of this document, Parts 8 to 11 were Technical Specifications. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom.
EN ISO 17025, General requirements for the competence of testing and calibration laboratories (ISO/IEC 17025:2005) ISO 3290, Rolling bearings — Balls — Dimensions and tolerances 3 Terms and definitions For the purposes of this European Standard, the following term and definition applies. 3.1 abrasive wear rate, K abrasive wear coefficient volume of material removed in unit sliding distance under a normal contact load of 1 N 4 Significance and use Although few protective coatings are subject to single wear processes, the abrasive wear resistance of such coatings can play a decisive role in their performance. Hence knowledge of the abrasive wear resistance of ceramic coatings can help in the proper selection of coatings for applications where abrasion plays a major role in their degradation. Although techniques exist to measure the abrasive wear behaviour of bulk materials and thick films (see [1 – 3]), these techniques are not easily applied to thin films and are difficult to interpret when used on curved surfaces.
The purpose of this European Standard is to provide a method for measuring the abrasion resistance of both thin and thick coatings and of bulk materials. The test can be performed on flat surfaces or surfaces with a known radius of curvature, and requires only a few mm2 of sample. However, the analysis described in clause 9 applies only to flat samples, and is applicable to homogeneous single layer coatings only; errors may occur if the test is used on in-homogeneous coatings. [4] and [5] give details of analytical treatments for determining the wear rate for coatings on curved surfaces.
By proper treatment of the results, as indicated in 9.2, where the test produces penetration of the coating it can provide abrasive wear coefficients for both the coating and substrate from a single test series.
(a)(b)1245343125 Key for a) 1
ball 2
sample 3
drive shaft 4
sample support 5
load cell Key for b) 1
ball 2
sample 3
weight 4
pivot point 5
lever
Figure 1 — Two different types of a ball cratering system: a) free-ball, b) fixed-ball
The recommended conditioning treatment consists of running the new test ball for at least 300 revolutions on a non-critical part of the sample, or other suitable surface, under normal test conditions and repeating this for at least 5 different orientations of the ball before starting the test programme. NOTE 2 A flat, ground steel coupon with a hardness of between 200 and 800 HV 30 has been found to be suitable for conditioning the ball. NOTE 3 Following conditioning, balls have been found to be usable for around 50 individual craters, depending on the precise conditions used.
The performance of balls shall be subject to regular performance checks to ensure that they continue to produce a
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