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EN ISO 17294-1:2024

(Main)

Water quality - Application of inductively coupled plasma mass spectrometry (ICP-MS) - Part 1: General requirements (ISO 17294-1:2024)

Water quality - Application of inductively coupled plasma mass spectrometry (ICP-MS) - Part 1: General requirements (ISO 17294-1:2024)

This document specifies the principles of inductively coupled plasma mass spectrometry (ICP-MS) and provides general requirements for the use of this technique to determine elements in water, digests of sludges and sediments (e.g. digests of water as described in ISO 15587-1 or ISO 15587-2). Generally, the measurement is carried out in water, but gases, vapours or fine particulate matter can be introduced too. This document applies to the use of ICP-MS for aqueous solution analysis.
The ultimate determination of the elements is described in a separate International Standard for each series of elements and matrix. The individual clauses of this document refer the user to these guidelines for the basic principles of the method and the configuration of the instrument.

Wasserbeschaffenheit - Anwendung der induktiv gekoppelten Plasma-Massenspektrometrie (ICP-MS) - Teil 1: Allgemeine Anforderungen (ISO 17294-1:2024)

Dieses Dokument legt die Grundlagen der induktiv gekoppelten Plasma-Massenspektrometrie (ICP MS) fest und gibt allgemeine Anforderungen für die Anwendung dieser Technik zur Bestimmung von Elementen in Wasser, Aufschlüsse von Schlämmen und Sedimenten (z. B. Aufschlüsse von Wasserproben nach ISO 15587 1 oder ISO 15587 2). Im Allgemeinen wird die Messung in Wasser durchgeführt, kann aber auch auf Gase, Dämpfe oder feine partikuläre Substanzen angewendet werden. Dieses Dokument gilt für die Anwendung der ICP-MS für die Analytik von wässrigen Lösungen.
Die eigentliche Durchführung der Elementbestimmung für spezifische Elemente und Matrizes wird jeweils in separaten Internationalen Normen beschrieben. Die individuellen Abschnitte von diesem Dokument verweisen den Anwender auf diese Anleitungen für die grundlegenden Prinzipien des Verfahrens und Gerätekonfigurationen.

Qualité de l’eau - Application de la spectrométrie de masse avec plasma à couplage inductif (ICP- MS) - Partie 1: Exigences générales (ISO 17294-1:2024)

Le présent document spécifie les principes de la spectrométrie de masse avec plasma à couplage inductif (ICP-MS) et fournit des exigences générales sur l’utilisation de cette technique pour déterminer des éléments présents dans l’eau, les minéralisats de boues et de sédiments (par exemple, les minéralisats d’eau décrits dans l’ISO 15587-1 ou l’ISO 15587-2). En règle générale, le mesurage est effectué dans l’eau, mais des gaz, des vapeurs ou de fines matières particulaires peuvent également être introduits. Le présent document est axé sur l’application de l’ICP-MS à l’analyse de solutions aqueuses.
La détermination finale des éléments est décrite dans une Norme internationale distincte pour chaque série d’éléments et chaque matrice. Les articles individuels du présent document renvoient l’utilisateur à ce cadre directeur pour les principes fondamentaux de la méthode et la configuration de l’instrument.

Kakovost vode - Uporaba masne spektrometrije z induktivno sklopljeno plazmo (ICP-MS) - 1. del: Splošne smernice (ISO 17294-1:2024)

Ta dokument določa načela masne spektrometrije z induktivno sklopljeno plazmo (ICP-MS) in podaja splošne smernice glede uporabe te tehnike za določevanje elementov v vodi, razklopih blata in usedlinah (npr. v razklopih vode, kot je opisano v standardu ISO 15587-1 ali ISO 15587-2). Meritve se na splošno izvajajo v vodi, vendar je mogoče dodati tudi pline, hlape ali drobne delce. Ta dokument se uporablja za uporabo masne spektrometrije z induktivno sklopljeno plazmo za analizo vodne raztopine.
Končna določitev elementov je opisana v ločenem mednarodnem standardu za vsako serijo elementov in matriko. Posamezne točke tega dokumenta napotijo uporabnika k tem smernicam za osnovna načela metode in konfiguracijo instrumenta.

General Information

Status
Published
Publication Date
02-Apr-2024
ICS
13.060.50 - Examination of water for chemical substances
Technical Committee
CEN/TC 230 - Water analysis
Drafting Committee
CEN/TC 230 - Water analysis
Current Stage
6060 - Definitive text made available (DAV) - Publishing
Start Date
03-Apr-2024
Completion Date
03-Apr-2024
Ref Project
SIST EN ISO 17294-1:2024 - Water quality - Application of inductively coupled plasma mass spectrometry (ICP-MS) - Part 1: General requirements (ISO 17294-1:2024)

Relations

Replaces
EN ISO 17294-1:2006 - Water quality - Application of inductively coupled plasma mass spectrometry (ICP-MS) - Part 1: General guidelines (ISO 17294-1:2004)
Effective Date
14-Oct-2020

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SLOVENSKI STANDARD
01-julij-2024
Nadomešča:
SIST EN ISO 17294-1:2007
Kakovost vode - Uporaba masne spektrometrije z induktivno sklopljeno plazmo
(ICP-MS) - 1. del: Splošne smernice (ISO 17294-1:2024)
Water quality - Application of inductively coupled plasma mass spectrometry (ICP-MS) -
Part 1: General requirements (ISO 17294-1:2024)
Wasserbeschaffenheit - Anwendung der induktiv gekoppelten Plasma-
Massenspektrometrie (ICP-MS) - Teil 1: Allgemeine Anforderungen (ISO 17294-1:2024)
Qualité de l’eau - Application de la spectrométrie de masse avec plasma à couplage
inductif (ICP- MS) - Partie 1: Exigences générales (ISO 17294-1:2024)
Ta slovenski standard je istoveten z: EN ISO 17294-1:2024
ICS:
13.060.50 Preiskava vode na kemične Examination of water for
snovi chemical substances
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

EN ISO 17294-1
EUROPEAN STANDARD
NORME EUROPÉENNE
April 2024
EUROPÄISCHE NORM
ICS 13.060.50 Supersedes EN ISO 17294-1:2006
English Version
Water quality - Application of inductively coupled plasma
mass spectrometry (ICP-MS) - Part 1: General
requirements (ISO 17294-1:2024)
Qualité de l'eau - Application de la spectrométrie de Wasserbeschaffenheit - Anwendung der induktiv
masse avec plasma à couplage inductif (ICP- MS) - gekoppelten Plasma-Massenspektrometrie (ICP-MS) -
Partie 1: Exigences générales (ISO 17294-1:2024) Teil 1: Allgemeine Anforderungen (ISO 17294-1:2024)
This European Standard was approved by CEN on 20 January 2024.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and
United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2024 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 17294-1:2024 E
worldwide for CEN national Members.

Contents Page
European foreword . 3

European foreword
This document (EN ISO 17294-1:2024) has been prepared by Technical Committee ISO/TC 147 "Water
quality" in collaboration with Technical Committee CEN/TC 230 “Water analysis” the secretariat of
which is held by DIN.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by October 2024, and conflicting national standards shall
be withdrawn at the latest by October 2024.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
This document supersedes EN ISO 17294-1:2006.
Any feedback and questions on this document should be directed to the users’ national standards
body/national committee. A complete listing of these bodies can be found on the CEN website.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland,
Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Republic of
North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and the
United Kingdom.
Endorsement notice
The text of ISO 17294-1:2024 has been approved by CEN as EN ISO 17294-1:2024 without any
modification.
International
Standard
ISO 17294-1
Second edition
Water quality — Application of
2024-03
inductively coupled plasma mass
spectrometry (ICP-MS) —
Part 1:
General requirements
Qualité de l’eau — Application de la spectrométrie de masse avec
plasma à couplage inductif (ICP-MS) —
Partie 1: Exigences générales
Reference number
ISO 17294-1:2024(en) © ISO 2024

ISO 17294-1:2024(en)
© ISO 2024
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting on
the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address below
or ISO’s member body in the country of the requester.
ISO copyright office
CP 401 • Ch. de Blandonnet 8
CH-1214 Vernier, Geneva
Phone: +41 22 749 01 11
Email: copyright@iso.org
Website: www.iso.org
Published in Switzerland
ii
ISO 17294-1:2024(en)
Contents Page
Foreword .v
Introduction .vi
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Principle . 3
5 Apparatus . 4
5.1 General .4
5.2 Sample introduction .4
5.2.1 General .4
5.2.2 Pump .5
5.2.3 Nebulizer .5
5.2.4 Spray chamber .6
5.2.5 Other systems .6
5.3 Torch and plasma .6
5.4 Gas and gas control .7
5.5 Generator .7
5.6 Transfer of the ions to the mass spectrometer .7
5.7 Mass spectrometer .8
5.7.1 General .8
5.7.2 Lens system .8
5.7.3 Collision or reaction cell .8
5.7.4 Analyser .8
5.7.5 Detector .9
5.7.6 Alternative mass spectrometers and types of instruments .10
5.8 Signal processing and instrument control.11
6 Interferences by concomitant elements .11
6.1 General .11
6.2 Spectral interferences .11
6.2.1 General .11
6.2.2 Possible elimination strategies for polyatomic ion interferences . 12
6.3 Non-spectral interferences . 13
6.3.1 General . 13
6.3.2 Interferences in the nebulization process . 13
6.3.3 Interferences in the plasma . 13
6.3.4 Interferences in the interface or lens area .14
6.3.5 Possible elimination strategies for non-spectral interferences (matrix effects) .14
7 Adjustment of the apparatus . 17
7.1 General .17
7.2 Tuning the apparatus .17
7.2.1 General .17
7.2.2 Alig
...

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