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SIST EN 12766-1:2000

(Main)

Petroleum products and used oils - Determination of PCBs and related products - Part 1: Separation and determination of selected PCB congeners by gas chromatography (GC) using an electron capture detector (ECD)

Petroleum products and used oils - Determination of PCBs and related products - Part 1: Separation and determination of selected PCB congeners by gas chromatography (GC) using an electron capture detector (ECD)

This European Standard specifies a method to determine the concentration of up to 12 individual or defined unresolved small groups of polychlorinated biphenyl (PCB) congeners in petroleum products and related materials by means of a specified gaschromatographic separation procedure. The gas chromatographic separation is valid for the different quantification procedures described in Part 2 of this European Standard.

Mineralölerzeugnisse und Gebrauchtöle - Bestimmung von PCBs und verwandten Produkten - Teil 1: Trennung und Bestimmung von ausgewählten PCB Congeneren mittels Gaschromatographie (GC) unter Verwendung eines Elektroneneinfang-Detektors (ECD)

Diese Europäische Norm legt ein Verfahren zur Bestimmung des Gehaltes von bis zu 12 PCB Congenere oder definierte unaufgelöste Gruppen polychlorierter Biphenyle in Minerlalölerzeugnissen und verwandten Stoffgemischen durch ein standardisiertes gaschromatographisches Trennverfahren fest. Das gaschromatographische Trennverfahren ist Basis für die unterschiedlichen Quantifizierungsmethoden, die im Teil 2 dieser Norm beschrieben werden.

Produits pétroliers et huiles usagées - Détermination des PCBs et produits connexes - Partie 1: Séparation et dosage d'une sélection de congéneres de PCB par chromatographie en phase gazeuse (CG) avec utilisation d'un détecteur a capture d'électrons (ECD)

La présente norme européenne prescrit une méthode de détermination de la concentration de 12 congéneres individuels ou de petits groupes définis de congéneres de polychlorobiphényles (PCB) dans les produits pétroliers et produits connexes, basée sur une séparation par chromatographie en phase gazeuse. Cette séparation chromatographique est valable pour l'application des différentes méthodes de quantification décrites dans la seconde partie de la présente norme européenne.

Naftni derivati in rabljena olja - Določevanje PCB in sorodnih proizvodov - 1. del: Ločitev in določevanje izbranih PCB spojin s plinsko kromatografijo (GC) z uporabo detektorja na zajetje elektronov (ECD)

General Information

Status
Published
Publication Date
30-Jun-2000
ICS
75.080 - Petroleum products in general
75.100 - Lubricants, industrial oils and related products
Technical Committee
NAD - Petroleum products, lubricants and related products
Current Stage
6060 - National Implementation/Publication (Adopted Project)
Start Date
01-Jul-2000
Due Date
01-Jul-2000
Completion Date
01-Jul-2000
Ref Project
EN 12766-1:2000 - Petroleum products and used oils - Determination of PCBs and related products - Part 1: Separation and determination of selected PCB congeners by gas chromatography (GC) using an electron capture detector (ECD)

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2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Mineralölerzeugnisse und Gebrauchtöle - Bestimmung von PCBs und verwandten Produkten - Teil 1: Trennung und Bestimmung von ausgewählten PCB Congeneren mittels Gaschromatographie (GC) unter Verwendung eines Elektroneneinfang-Detektors (ECD)Produits pétroliers et huiles usagées - Détermination des PCBs et produits connexes - Partie 1: Séparation et dosage d'une sélection de congéneres de PCB par chromatographie en phase gazeuse (CG) avec utilisation d'un détecteur a capture d'électrons (ECD)Petroleum products and used oils - Determination of PCBs and related products - Part 1: Separation and determination of selected PCB congeners by gas chromatography (GC) using an electron capture detector (ECD)75.100MazivaLubricants, industrial oils and related products75.080Naftni proizvodi na splošnoPetroleum products in
...

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a This value is only a best estimate. Real field conditions may, depending on the concentrations in the three different classes, result in other, more limited or more improved application ranges. It is the user's responsibility to demonstrate that the analysis has been performed in a valid calibrated concentration range.

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This standard specifies two calculation procedures ("method A" and "method B") for PCB content. The basis for this quantification is taken from the chromatographic results of EN 12766-1:2000 in which all necessary experimental procedures are described for the specific analysis of unused, used and treated (e.g. dechlorinated) petroleum products including synthetic lubricating oils and mixtures of vegetable oils. The method is also applicable to petroleum products and synthetic lubricating oils suitably recovered from other materials, e.g. from waste materials. Both methods have different strengths and weaknesses which are described in the next paragraphs and which must be considered before use in a specific application. Proper application of either method A or method B needs to be carefully considered before use in a specific application.
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