ASTM D665-14
(Test Method)Standard Test Method for Rust-Preventing Characteristics of Inhibited Mineral Oil in the Presence of Water
Standard Test Method for Rust-Preventing Characteristics of Inhibited Mineral Oil in the Presence of Water
SIGNIFICANCE AND USE
5.1 In many instances, such as in the gears of a steam turbine, water can become mixed with the lubricant, and rusting of ferrous parts can occur. This test indicates how well inhibited mineral oils aid in preventing this type of rusting. This test method is also used for testing hydraulic and circulating oils, including heavier-than-water fluids. It is used for specification of new oils and monitoring of in-service oils.
Note 3: This test method was used as a basis for Test Method D3603. Test Method D3603 is used to test the oil on separate horizontal and vertical test rod surfaces, and can provide a more discriminating evaluation.
SCOPE
1.1 This test method covers the evaluation of the ability of inhibited mineral oils, particularly steam-turbine oils, to aid in preventing the rusting of ferrous parts should water become mixed with the oil. This test method is also used for testing other oils, such as hydraulic oils and circulating oils. Provision is made in the procedure for testing heavier-than-water fluids.
Note 1: For synthetic fluids, such as phosphate ester types, the plastic holder and beaker cover should be made of chemically resistant material suitable for the type of fluid tested.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see 7.4 – 7.6.
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Designation: D665 − 14
Designation:135/06
Standard Test Method for
Rust-Preventing Characteristics of Inhibited Mineral Oil in
1
the Presence of Water
This standard is issued under the fixed designation D665; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope* Vessels and for General Applications
D91 Test Method for Precipitation Number of Lubricating
1.1 This test method covers the evaluation of the ability of
Oils
inhibited mineral oils, particularly steam-turbine oils, to aid in
D1193 Specification for Reagent Water
preventing the rusting of ferrous parts should water become
D2422 Classification of Industrial Fluid Lubricants by Vis-
mixed with the oil. This test method is also used for testing
cosity System
other oils, such as hydraulic oils and circulating oils. Provision
D3603 Test Method for Rust-Preventing Characteristics of
is made in the procedure for testing heavier-than-water fluids.
Steam Turbine Oil in the Presence of Water (Horizontal
NOTE 1—For synthetic fluids, such as phosphate ester types, the plastic
Disk Method)
holder and beaker cover should be made of chemically resistant material
D4057 Practice for Manual Sampling of Petroleum and
suitable for the type of fluid tested.
Petroleum Products
1.2 The values stated in SI units are to be regarded as
E1 Specification for ASTM Liquid-in-Glass Thermometers
standard. No other units of measurement are included in this
2.2 Other Documents:
standard.
Motor Fuels, Section I, Annex A2, Table 32, Reference
3
1.3 This standard does not purport to address all of the
Materials and Blending Accessories
safety concerns, if any, associated with its use. It is the Specifications-IP Standard Thermometers, Vol 2, Appendix
4
responsibility of the user of this standard to establish appro-
A
priate safety and health practices and determine the applica- Specifications for IP Standard Reference Liquids, Appendix
4
bility of regulatory limitations prior to use. For specific B
warning statements, see 7.4 – 7.6.
SAE Standard J405 Chemical Composition of SAEWrought
5
Stainless Steels
4
2. Referenced Documents
BS 871 Specification for abrasive papers and cloths
2
BS 970 Part 1: Carbon and Carbon Manganese Steels
2.1 ASTM Standards:
4
Including Free Cutting Steels
A108 Specification for Steel Bar, Carbon and Alloy, Cold-
Finished
3. Terminology
A240/A240M Specification for Chromium and Chromium-
3.1 Definitions of Terms Specific to This Standard:
Nickel Stainless Steel Plate, Sheet, and Strip for Pressure
3.1.1 rust,n—aspecialcaseofcorrosionthatcanbevisually
observed on the surface of round steel test rods as reddish-
1
This test method is under the jurisdiction of ASTM Committee D02 on
brown discoloration or small black spots.
Petroleum Products, Liquid Fuels, and Lubricants and is the direct responsibility of
Subcommittee D02.C0.02 on Corrosion and Water/Air Separability.
4. Summary of Test Method
Current edition approved Oct. 1, 2014. Published November 2014. Originally
approved in 1942. Last previous edition approved in 2012 as D665 – 12. DOI:
4.1 Amixture of 300 mLof the oil under test is stirred with
10.1520/D0665-14.
30 mL of distilled water or synthetic sea water, as required, at
This standard has been developed through the cooperative effort betweenASTM
International and the Energy Institute, London. The EI and ASTM International
3
logos imply that the ASTM International and EI standards are technically See 1996 Annual Book of ASTM Standards, Vol 05.04.
4
equivalent, but does not imply that both standards are editorially identical. AnnualBookofIPStandardMethodsforAnalysisandTestingofPetroleumand
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or Related Products, Vol 2. Available from Energy Institute, 61 New Cavendish St.,
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM London, WIG 7AR, U.K.
5
Standards volume information, refer to the standard’s Document Summary page on 1995 SAE Handbook, Vol 1. Available from Society of Automotive Engineers
the ASTM website. (SAE), 400 Commonwealth Dr., Warrendale, PA 15096-0001.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
D665 − 14
for the beaker which has been found to be suitable.An optional feature is
a temperature of 60 °C 6 1 °C with a cylindrical steel test rod
shown, consisting of a slot
...
This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D665 − 12 D665 − 14
Designation: 135/06
Standard Test Method for
Rust-Preventing Characteristics of Inhibited Mineral Oil in
1
the Presence of Water
This standard is issued under the fixed designation D665; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope*
1.1 This test method covers the evaluation of the ability of inhibited mineral oils, particularly steam-turbine oils, to aid in
preventing the rusting of ferrous parts should water become mixed with the oil. This test method is also used for testing other oils,
such as hydraulic oils and circulating oils. Provision is made in the procedure for testing heavier-than-water fluids.
NOTE 1—For synthetic fluids, such as phosphate ester types, the plastic holder and beaker cover should be made of a chemically resistant material,
such as polytetrafluoroethylene (PTFE).chemically resistant material suitable for the type of fluid tested.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use. For specific warning statements, see 6.47.4 – 6.67.6.
2. Referenced Documents
2
2.1 ASTM Standards:
A108 Specification for Steel Bar, Carbon and Alloy, Cold-Finished
A240/A240M Specification for Chromium and Chromium-Nickel Stainless Steel Plate, Sheet, and Strip for Pressure Vessels and
for General Applications
D91 Test Method for Precipitation Number of Lubricating Oils
D1193 Specification for Reagent Water
D2422 Classification of Industrial Fluid Lubricants by Viscosity System
D3603 Test Method for Rust-Preventing Characteristics of Steam Turbine Oil in the Presence of Water (Horizontal Disk Method)
D4057 Practice for Manual Sampling of Petroleum and Petroleum Products
E1 Specification for ASTM Liquid-in-Glass Thermometers
2.2 Other Documents:
3
Motor Fuels, Section I, Annex A2, Table 32, Reference Materials and Blending Accessories
4
Specifications-IP Standard Thermometers, Vol 2, Appendix A
4
Specifications for IP Standard Reference Liquids, Appendix B
5
SAE Standard J405 Chemical Composition of SAE Wrought Stainless Steels
4
BS 871 Specification for abrasive papers and cloths
1
This test method is under the jurisdiction of ASTM Committee D02 on Petroleum Products Products, Liquid Fuels, and Lubricants and is the direct responsibility of
Subcommittee D02.C0.02 on Corrosion and Water/Air Separability.
Current edition approved Nov. 1, 2012Oct. 1, 2014. Published March 2013November 2014. Originally approved in 1942. Last previous edition approved in 20062012 as
D665D665 – 12.-06. DOI: 10.1520/D0665-12.10.1520/D0665-14.
This standard has been developed through the cooperative effort between ASTM International and the Energy Institute, London. The EI and ASTM International logos
imply that the ASTM International and EI standards are technically equivalent, but does not imply that both standards are editorially identical.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
3
See 1996 Annual Book of ASTM Standards, Vol 05.04.
4
Annual Book of IP Standard Methods for Analysis and Testing of Petroleum and Related Products, Vol 2. Available from Energy Institute, 61 New Cavendish St., London,
WIG 7AR, U.K.
5
1995 SAE Handbook, Vol 1. Available from Society of Automotive Engineers (SAE), 400 Commonwealth Dr., Warrendale, PA 15096-0001.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
D665 − 14
4
BS 970 Part 1: Carbon and Carbon Manganese Steels Including Free Cutting Steels
3. Terminology
3.1 Definitions of Terms Specific to This Standard:
3.1.1 rust, n—a special case of corrosio
...
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