iTeh StandardsiTeh Standards
EURUSD
Your shopping cart is empty.
ASTM

ASTM D6352-15

(Test Method)

Standard Test Method for Boiling Range Distribution of Petroleum Distillates in Boiling Range from 174 °C to 700 °C by Gas Chromatography

Standard Test Method for Boiling Range Distribution of Petroleum Distillates in Boiling Range from 174 °C to 700 °C by Gas Chromatography

SIGNIFICANCE AND USE
5.1 The boiling range distribution of medium and heavy petroleum distillate fractions provides an insight into the composition of feed stocks and products related to petroleum refining processes (for example, hydrocracking, hydrotreating, visbreaking, or deasphalting). The gas chromatographic simulation of this determination can be used to replace conventional distillation methods for control of refining operations. This test method can be used for product specification testing with the mutual agreement of interested parties.  
5.2 This test method extends the scope of boiling range determination by gas chromatography to include medium and heavy petroleum distillate fractions beyond the scope of Test Method D2887 (538 °C).  
5.3 Boiling range distributions obtained by this test method have not been analyzed for correlation to those obtained by low efficiency distillation, such as with Test Method D86 or D1160.
SCOPE
1.1 This test method covers the determination of the boiling range distribution of petroleum distillate fractions. The test method is applicable to petroleum distillate fractions having an initial boiling point greater than 174 °C (345 °F) and a final boiling point of less than 700 °C (1292 °F) (C10 to C90) at atmospheric pressure as measured by this test method.  
1.2 The test method is not applicable for the analysis of petroleum or petroleum products containing low molecular weight components (for example naphthas, reformates, gasolines, crude oils). Materials containing heterogeneous components (for example alcohols, ethers, acids, or esters) or residue are not to be analyzed by this test method. See Test Methods D3710, D2887, or D5307 for possible applicability to analysis of these types of materials.  
1.3 The values stated in SI units are to be regarded as standard. The values stated in inch-pound units are for information only and may be included as parenthetical values.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
30-Jun-2015
ICS
75.080 - Petroleum products in general
Technical Committee
D02 - Petroleum Products, Liquid Fuels, and Lubricants
Drafting Committee
D02.04.0H - Chromatographic Distribution Methods
Current Stage
Ref Project

Relations

Replaced By
ASTM D6352-19 - Standard Test Method for Boiling Range Distribution of Petroleum Distillates in Boiling Range from 174 °C to 700 °C by Gas Chromatography
Effective Date
01-Dec-2019

Buy Standard

ASTM D6352-15 - Standard Test Method for Boiling Range Distribution of Petroleum Distillates in Boiling Range from 174 °C to 700 °C by Gas ChromatographyASTM D6352-15 - Standard Test Method for Boiling Range Distribution of Petroleum Distillates in Boiling Range from 174 °C to 700 °C by Gas Chromatography
PreviousNext
Standard
ASTM D6352-15 - Standard Test Method for Boiling Range Distribution of Petroleum Distillates in Boiling Range from 174 °C to 700 °C by Gas Chromatography
English language
17 pages
sale 15% off
Preview
sale 15% off
Preview
REDLINE ASTM D6352-15 - Standard Test Method for Boiling Range Distribution of Petroleum Distillates in Boiling Range from 174 °C to 700 °C by Gas ChromatographyREDLINE ASTM D6352-15 - Standard Test Method for Boiling Range Distribution of Petroleum Distillates in Boiling Range from 174 °C to 700 °C by Gas Chromatography
PreviousNext
Standard
REDLINE ASTM D6352-15 - Standard Test Method for Boiling Range Distribution of Petroleum Distillates in Boiling Range from 174 °C to 700 °C by Gas Chromatography
English language
17 pages
sale 15% off
Preview
sale 15% off
Preview

Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D6352 − 15
Standard Test Method for
Boiling Range Distribution of Petroleum Distillates in
Boiling Range from 174 °C to 700 °C by Gas
1
Chromatography
This standard is issued under the fixed designation D6352; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope* D2887Test Method for Boiling Range Distribution of Pe-
troleum Fractions by Gas Chromatography
1.1 Thistestmethodcoversthedeterminationoftheboiling
D2892Test Method for Distillation of Crude Petroleum
range distribution of petroleum distillate fractions. The test
(15-Theoretical Plate Column)
methodisapplicabletopetroleumdistillatefractionshavingan
D3710TestMethodforBoilingRangeDistributionofGaso-
initial boiling point greater than 174°C (345°F) and a final
line and Gasoline Fractions by Gas Chromatography
boiling point of less than 700°C (1292°F) (C10 to C90) at
3
(Withdrawn 2014)
atmospheric pressure as measured by this test method.
D4626Practice for Calculation of Gas Chromatographic
1.2 The test method is not applicable for the analysis of
Response Factors
petroleum or petroleum products containing low molecular
D5307Test Method for Determination of Boiling Range
weight components (for example naphthas, reformates,
Distribution of Crude Petroleum by Gas Chromatography
3
gasolines, crude oils). Materials containing heterogeneous
(Withdrawn 2011)
components (for example alcohols, ethers, acids, or esters) or
E355PracticeforGasChromatographyTermsandRelation-
residue are not to be analyzed by this test method. See Test
ships
MethodsD3710,D2887,orD5307forpossibleapplicabilityto
E594Practice for Testing Flame Ionization Detectors Used
analysis of these types of materials.
in Gas or Supercritical Fluid Chromatography
1.3 The values stated in SI units are to be regarded as E1510Practice for Installing Fused Silica Open Tubular
Capillary Columns in Gas Chromatographs
standard. The values stated in inch-pound units are for infor-
mation only and may be included as parenthetical values.
3. Terminology
1.4 This standard does not purport to address all of the
3.1 Definitions—This test method makes reference to many
safety concerns, if any, associated with its use. It is the
common gas chromatographic procedures, terms, and relation-
responsibility of the user of this standard to establish appro-
ships. For definitions of these terms used in this test method,
priate safety and health practices and determine the applica-
refer to Practices E355, E594, and E1510.
bility of regulatory limitations prior to use.
3.2 Definitions of Terms Specific to This Standard:
2. Referenced Documents 3.2.1 areaslice,n—thearearesultingfromtheintegrationof
2
the chromatographic detector signal within a specified reten-
2.1 ASTM Standards:
tiontimeinterval.Inareaslicemode(see6.4.2),peakdetection
D86Test Method for Distillation of Petroleum Products at
parameters are bypassed and the detector signal integral is
Atmospheric Pressure
recorded as area slices of consecutive, fixed duration time
D1160TestMethodforDistillationofPetroleumProductsat
intervals.
Reduced Pressure
3.2.2 corrected area slice, n—an area slice corrected for
baselineoffsetbysubtractionoftheexactlycorrespondingarea
1
This test method is under the jurisdiction of ASTM Committee D02 on slice in a previously recorded blank (non-sample) analysis.
Petroleum Products, Liquid Fuels, and Lubricants and is the direct responsibility of
3.2.3 cumulativecorrectedarea,n—theaccumulatedsumof
Subcommittee D02.04.0H on Chromatographic Distribution Methods.
correctedareaslicesfromthebeginningoftheanalysisthrough
CurrenteditionapprovedJuly1,2015.PublishedJuly2015.Originallyapproved
in 1998. Last previous edition approved in 2014 as D6352–14. DOI: 10.1520/
a given retention time, ignoring any non-sample area (for
D6352-15.
example, solvent).
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
3
Standards volume information, refer to the standard’s Document Summary page on The last approved version of this historical standard is referenced on
the ASTM website. www.astm.org.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D6352 − 15
3.2.4 final boiling point (FBP), n—the temperature (corre- visbreaking, or deasphalting). The gas chromatographic simu-
spondingtotheretentiontime)atwhichacumulativecorrected lationofthisdeterminationcanbeu
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D6352 − 14 D6352 − 15
Standard Test Method for
Boiling Range Distribution of Petroleum Distillates in
Boiling Range from 174 °C to 700 °C by Gas
1
Chromatography
This standard is issued under the fixed designation D6352; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope*
1.1 This test method covers the determination of the boiling range distribution of petroleum distillate fractions. The test method
is applicable to petroleum distillate fractions having an initial boiling point greater than 174 °C (345 °F) and a final boiling point
of less than 700 °C (1292 °F) (C10 to C90) at atmospheric pressure as measured by this test method.
1.2 The test method is not applicable for the analysis of petroleum or petroleum products containing low molecular weight
components (for example naphthas, reformates, gasolines, crude oils). Materials containing heterogeneous components (for
example alcohols, ethers, acids, or esters) or residue are not to be analyzed by this test method. See Test Methods D3710, D2887,
or D5307 for possible applicability to analysis of these types of materials.
1.3 The values stated in SI units are to be regarded as standard. The values stated in inch-pound units are for information only
and may be included as parenthetical values.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
D86 Test Method for Distillation of Petroleum Products at Atmospheric Pressure
D1160 Test Method for Distillation of Petroleum Products at Reduced Pressure
D2887 Test Method for Boiling Range Distribution of Petroleum Fractions by Gas Chromatography
D2892 Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
D3710 Test Method for Boiling Range Distribution of Gasoline and Gasoline Fractions by Gas Chromatography (Withdrawn
3
2014)
D4626 Practice for Calculation of Gas Chromatographic Response Factors
D5307 Test Method for Determination of Boiling Range Distribution of Crude Petroleum by Gas Chromatography (Withdrawn
3
2011)
E355 Practice for Gas Chromatography Terms and Relationships
E594 Practice for Testing Flame Ionization Detectors Used in Gas or Supercritical Fluid Chromatography
E1510 Practice for Installing Fused Silica Open Tubular Capillary Columns in Gas Chromatographs
3. Terminology
3.1 Definitions—This test method makes reference to many common gas chromatographic procedures, terms, and relationships.
For definitions of these terms used in this test method, refer to Practices E355, E594, and E1510.
3.2 Definitions of Terms Specific to This Standard:
1
This test method is under the jurisdiction of ASTM Committee D02 on Petroleum Products, Liquid Fuels, and Lubricants and is the direct responsibility of Subcommittee
D02.04.0H on Chromatographic Distribution Methods.
Current edition approved Oct. 1, 2014July 1, 2015. Published December 2014July 2015. Originally approved in 1998. Last previous edition approved in 20122014 as
D6352 – 12.D6352 – 14. DOI: 10.1520/D6352-14.10.1520/D6352-15.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
3
The last approved version of this historical standard is referenced on www.astm.org.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D6352 − 15
3.2.1 area slice, n—the area resulting from the integration of the chromatographic detector signal within a specified retention
time interval. In area slice mode (see 6.4.2), peak detection parameters are bypassed and the detector signal integral is recorded
as area slices of consecutive, fixed duration time intervals.
3.2.2 corrected area slice, n—an area slice corrected for baseline offset by subtraction of the exactly corresponding area slice
in a previously
...

Questions, Comments and Discussion

Ask us and Technical Secretary will try to provide an answer. You can facilitate discussion about the standard in here.

This May Also Interest You

ASTM
ASTM D2890-23(Test Method)
Standard Test Method for Calculation of Liquid Heat Capacity of Petroleum Distillate Fuels

SIGNIFICANCE AND USE
5.1 Heat capacities obtained by this method are those at atmospheric pressure. However, because the temperature range is low, the calculated values are similar to saturated liquid heat capacities in the temperature-pressure range required for most engineering design.
SCOPE
1.1 This test method covers the calculation of liquid heat capacity, Btu/lb · °F (kJ/kg · K), at atmospheric pressure, of petroleum fuels for which distillation data may be obtained in accordance with Test Method D86 without reaching a decomposition point prior to obtaining 90 % by volume distilled.  
1.2 This test method is not applicable at temperatures less than 0 °F (−18 °C) and greater than 60 °F (16 °C) above the volumetric average boiling point of the fuel.  
1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    3 pages
    English language
    sale 15% off
  • Standard
    3 pages
    English language
    sale 15% off
ASTM
ASTM D7213-23(Test Method)
Standard Test Method for Boiling Range Distribution of Petroleum Distillates in the Boiling Range from 100 °C to 615 °C by Gas Chromatography

SIGNIFICANCE AND USE
5.1 The boiling range distribution of light and medium petroleum distillate fractions provides an insight into the composition of feed stocks and products related to petroleum refining process, This gas chromatographic determination of boiling range can be used to replace conventional distillation methods for control of refining operations. This test method can be used for product specification testing with the mutual agreement of interested parties.  
5.2 This test method extends the scope of boiling range determination by gas chromatography to include light and medium petroleum distillate fractions beyond the scope of Test Method D2887 (538 °C) and below Test Method D6352 (700 °C).  
5.3 Boiling range distributions obtained by this test method are theoretically equivalent to those obtained by true boiling point (TBP) distillation (see Test Method D2892). They are not equivalent to results from low efficiency distillation such as those obtained with Test Method D86 or D1160.
SCOPE
1.1 This test method covers the determination of the boiling range distribution of petroleum products. This test method is applicable to petroleum distillates having an initial boiling point greater than 100 °C and a final boiling point less than 615 °C at atmospheric pressure as measured by this test method.  
1.2 The test method is not applicable for analysis of petroleum distillates containing low molecular weight components (for example, naphthas, reformates, gasolines, crude oils). Materials containing heterogeneous components (for example, alcohols, ethers, acids or esters) or residue are not to be analyzed by this test method. See Test Methods D7096, D2887, D6352, or D7169.  
1.3 This test method uses the principles of simulated distillation methodology.  
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    16 pages
    English language
    sale 15% off
  • Standard
    16 pages
    English language
    sale 15% off
ASTM
ASTM D6792-23c(Practice)
Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories

SIGNIFICANCE AND USE
4.1 A petroleum products, liquid fuels, and lubricants testing laboratory plays a crucial role in product quality management and customer satisfaction. It is essential for a laboratory to provide quality data. This document provides guidance for establishing and maintaining a quality management system in a laboratory.  
4.1.1 The word ‘customer’ can refer to both customers internal and external to the laboratory or organization.
SCOPE
1.1 This practice covers the establishment and maintenance of the essentials of a quality management system in laboratories engaged in the analysis of petroleum products, liquid fuels, and lubricants. It is designed to be used in conjunction with Practice D6299.
Note 1: This practice is based on the quality management concepts and principles advocated in ANSI/ISO/ASQ Q9000 standards, ISO/IEC 17025, ASQ Manual,2 and ASTM standards such as D3244, D4182, D4621, D6299, D6300, D7372, E29, E177, E456, E548, E882, E994, E1301, E1323, STP 15D,3 and STP 1209.4  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory requirements prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    14 pages
    English language
    sale 15% off
  • Standard
    14 pages
    English language
    sale 15% off
ASTM
ASTM D1159-23(Test Method)
Standard Test Method for Bromine Numbers of Petroleum Distillates and Commercial Aliphatic Olefins by Electrometric Titration

SIGNIFICANCE AND USE
5.1 The bromine number is useful as a measure of aliphatic unsaturation in petroleum samples. When used in conjunction with the calculation procedure described in Annex A2, it can be used to estimate the percentage of olefins in petroleum distillates boiling up to approximately 315 °C (600 °F).  
5.2 The bromine number of commercial aliphatic monoolefins provides supporting evidence of their purity and identity.
SCOPE
1.1 This test method3 covers the determination of the bromine number of the following materials:  
1.1.1 Petroleum distillates that are substantially free of material lighter than isobutane and that have 90 % distillation points (by Test Method D86) under 327 °C (626 °F). This test method is generally applicable to gasoline (including leaded, unleaded, and oxygenated fuels), kerosine, and distillates in the gas oil range that fall in the following limits:    
90 % Distillation Point, °C (°F)  
Bromine Number, max3    
Under 205 (400)  
175    
205 to 327 (400 to 626)  
10  
1.1.2 Commercial olefins that are essentially mixtures of aliphatic mono-olefins and that fall within the range of 95 to 165 bromine number (see Note 1). This test method has been found suitable for such materials as commercial propylene trimer and tetramer, butene dimer, and mixed nonenes, octenes, and heptenes. This test method is not satisfactory for normal alpha-olefins.  
Note 1: These limits are imposed since the precision of this test method has been determined only up to or within the range of these bromine numbers.  
1.2 The magnitude of the bromine number is an indication of the quantity of bromine-reactive constituents, not an identification of constituents; therefore, its application as a measure of olefinic unsaturation should not be undertaken without the study given in Annex A1.  
1.3 For petroleum hydrocarbon mixtures of bromine number less than 1.0, a more precise measure for bromine-reactive constituents can be obtained by using Test Method D2710. If the bromine number is less than 0.5, then Test Method D2710 or the comparable bromine index methods for industrial aromatic hydrocarbons, Test Methods D1492 or D5776 must be used in accordance with their respective scopes. The practice of using a factor of 1000 to convert bromine number to bromine index is not applicable for these lower values of bromine number.  
1.4 The values stated in SI units are to be regarded as the standard.  
1.4.1 Exception—The values given in parentheses are for information only.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see Sections 7, 8, and 9.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    10 pages
    English language
    sale 15% off
  • Standard
    10 pages
    English language
    sale 15% off
ASTM
ASTM D445-23(Test Method)
Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)

SIGNIFICANCE AND USE
5.1 Many petroleum products, and some non-petroleum materials, are used as lubricants, and the correct operation of the equipment depends upon the appropriate viscosity of the liquid being used. In addition, the viscosity of many petroleum fuels is important for the estimation of optimum storage, handling, and operational conditions. Thus, the accurate determination of viscosity is essential to many product specifications.
SCOPE
1.1 This test method specifies a procedure for the determination of the kinematic viscosity, ν, of liquid petroleum products, both transparent and opaque, by measuring the time for a volume of liquid to flow under gravity through a calibrated glass capillary viscometer. The dynamic viscosity, η, can be obtained by multiplying the kinematic viscosity, ν, by the density, ρ, of the liquid.  
Note 1: For the measurement of the kinematic viscosity and viscosity of bitumens, see also Test Methods D2170 and D2171.
Note 2: ISO 3104 corresponds to Test Method D445 – 03.  
1.2 The result obtained from this test method is dependent upon the behavior of the sample and is intended for application to liquids for which primarily the shear stress and shear rates are proportional (Newtonian flow behavior). If, however, the viscosity varies significantly with the rate of shear, different results may be obtained from viscometers of different capillary diameters. The procedure and precision values for residual fuel oils, which under some conditions exhibit non-Newtonian behavior, have been included.  
1.3 The range of kinematic viscosities covered by this test method is from 0.2 mm2/s to 300 000 mm2/s (see Table A1.1) at all temperatures (see 6.3 and 6.4). The precision has only been determined for those materials, kinematic viscosity ranges and temperatures as shown in the footnotes to the precision section.  
1.4 The values stated in SI units are to be regarded as standard. The SI unit used in this test method for kinematic viscosity is mm2/s, and the SI unit used in this test method for dynamic viscosity is mPa·s. For user reference, 1 mm2/s = 10-6 m2/s = 1 cSt and 1 mPa·s = 1 cP = 0.001 Pa·s.  
1.5 WARNING—Mercury has been designated by many regulatory agencies as a hazardous substance that can cause serious medical issues. Mercury, or its vapor, has been demonstrated to be hazardous to health and corrosive to materials. Use Caution when handling mercury and mercury-containing products. See the applicable product Safety Data Sheet (SDS) for additional information. The potential exists that selling mercury or mercury-containing products, or both, is prohibited by local or national law. Users must determine legality of sales in their location.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    16 pages
    English language
    sale 15% off
  • Standard
    16 pages
    English language
    sale 15% off
ASTM
ASTM D3235-23(Test Method)
Standard Test Method for Solvent Extractables in Petroleum Waxes

SIGNIFICANCE AND USE
5.1 The solvent extractables in a wax may have significant effects on several of its properties such as strength, hardness, flexibility, scuff resistance, coefficient of friction, coefficient of expansion, melting point, and staining characteristics. Whether these effects are desirable or undesirable depends on the intended use of the wax.
SCOPE
1.1 This test method covers the determination of solvent extractables in petroleum waxes.  
1.2 The values stated in SI units are to be regarded as standard.  
1.2.1 Exception—The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    7 pages
    English language
    sale 15% off
  • Standard
    7 pages
    English language
    sale 15% off
ASTM
ASTM D156-23(Test Method)
Standard Test Method for Saybolt Color of Petroleum Products (Saybolt Chromometer Method)

SIGNIFICANCE AND USE
5.1 Determination of the color of petroleum products is used mainly for manufacturing control purposes and is an important quality characteristic since color is readily observed by the user of the product. In some cases the color may serve as an indication of the degree of refinement of the material. When the color range of a particular product is known, a variation outside the established range can indicate possible contamination with another product. However, color is not always a reliable guide to product quality and should not be used indiscriminately in product specifications.
SCOPE
1.1 This test method covers the determination of the color of refined oils such as undyed motor and aviation gasoline, jet propulsion fuels, naphthas and kerosine, and, in addition, petroleum waxes and pharmaceutical white oils.  
Note 1: For determining the color of petroleum products darker than Saybolt Color − 16, see Test Method D1500.  
1.2 This test method reports results specific to this test method and recorded as, “Saybolt Color units.”  
1.3 The values stated in inch-pound units or in SI units and which are not in parentheses are to be regarded as the standard. The values given in parentheses are for information only.  
Note 2: Oil tubes and apparatus used in this test method have traditionally been marked in inches, (the tube is required to be etched with 1/8 in. divisions.) The Saybolt Color Numbers are aligned with inch, 1/2 in., 1/4 in., and 1/8 in. changes in the depth of oil. These fractional inch changes do not readily correspond to SI equivalents and in view of the preponderance of apparatus already in use and marked in inches, the inch/pound unit is regarded as the standard. However the test method does use SI units of length when the length is not directly related to divisions on the oil tube and Saybolt Color Numbers. The test method uses SI units for temperature.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    6 pages
    English language
    sale 15% off
  • Standard
    6 pages
    English language
    sale 15% off
ASTM
ASTM D7152-23(Practice)
Standard Practice for Calculating Viscosity of a Blend of Petroleum Products

SIGNIFICANCE AND USE
5.1 Predicting the viscosity of a blend of components is a common problem. Both the Wright Blending Method and the ASTM Blending Method, described in this practice, may be used to solve this problem.  
5.2 The inverse problem, predicating the required blend fractions of components to meet a specified viscosity at a given temperature may also be solved using either the Inverse Wright Blending Method or the Inverse ASTM Blending Method.  
5.3 The Wright Blending Methods are generally preferred since they have a firmer basis in theory, and are more accurate. The Wright Blending Methods require component viscosities to be known at two temperatures. The ASTM Blending Methods are mathematically simpler and may be used when viscosities are known at a single temperature.  
5.4 Although this practice was developed using kinematic viscosity and volume fraction of each component, the dynamic viscosity or mass fraction, or both, may be used instead with minimal error if the densities of the components do not differ greatly. For fuel blends, it was found that viscosity blending using mass fractions gave more accurate results. For base stock blends, there was no significant difference between mass fraction and volume fraction calculations.  
5.5 The calculations described in this practice have been computerized as a spreadsheet and are available as an adjunct.3
SCOPE
1.1 This practice covers the procedures for calculating the estimated kinematic viscosity of a blend of two or more petroleum products, such as lubricating oil base stocks, fuel components, residual fuel oil with kerosene, crude oils, and related products, from their kinematic viscosities and blend fractions.  
1.2 This practice allows for the estimation of the fraction of each of two petroleum products needed to prepare a blend meeting a specific viscosity.  
1.3 This practice may not be applicable to other types of products, or to materials which exhibit strong non-Newtonian properties, such as viscosity index improvers, additive packages, and products containing particulates.  
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 Logarithms may be either common logarithms or natural logarithms, as long as the same are used consistently. This practice uses common logarithms. If natural logarithms are used, the inverse function, exp(×), must be used in place of the base 10 exponential function, 10×, used herein.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and to determine the applicability of regulatory limitations prior to use.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    9 pages
    English language
    sale 15% off
  • Standard
    9 pages
    English language
    sale 15% off
ASTM
ASTM D4952-23(Test Method)
Standard Test Method for Qualitative Analysis for Active Sulfur Species in Fuels and Solvents (Doctor Test)

SIGNIFICANCE AND USE
5.1 Sulfur present as mercaptans or as hydrogen sulfide in distillate fuels and solvents can attack many metallic and non-metallic materials in fuel and other distribution systems. A negative result in the doctor test ensures that the concentration of these compounds is insufficient to cause such problems in normal use.
SCOPE
1.1 This test method covers and is intended primarily for the detection of mercaptans in motor fuel, kerosine, and similar petroleum products. This method may also provide information on hydrogen sulfide and elemental sulfur that may be present in these sample types.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  For specific warning statements, see 7.3.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    3 pages
    English language
    sale 15% off
  • Standard
    3 pages
    English language
    sale 15% off
ASTM
ASTM D2887-23(Test Method)
Standard Test Method for Boiling Range Distribution of Petroleum Fractions by Gas Chromatography

SIGNIFICANCE AND USE
5.1 The boiling range distribution of petroleum fractions provides an insight into the composition of feedstocks and products related to petroleum refining processes. The gas chromatographic simulation of this determination can be used to replace conventional distillation methods for control of refining operations. This test method can be used for product specification testing with the mutual agreement of interested parties.  
5.2 Boiling range distributions obtained by this test method are essentially equivalent to those obtained by true boiling point (TBP) distillation (see Test Method D2892). They are not equivalent to results from low efficiency distillations such as those obtained with Test Method D86 or D1160.  
5.3 Procedure B was tested with biodiesel mixtures and reports the Boiling Point Distribution of FAME esters of vegetable and animal origin mixed with ultra low sulfur diesel.
SCOPE
1.1 This test method covers the determination of the boiling range distribution of petroleum products. The test method is applicable to petroleum products and fractions having a final boiling point of 538 °C (1000 °F) or lower at atmospheric pressure as measured by this test method. This test method is limited to samples having a boiling range greater than 55.5 °C (100 °F), and having a vapor pressure sufficiently low to permit sampling at ambient temperature.
Note 1: Since a boiling range is the difference between two temperatures, only the constant of 1.8 °F/°C is used in the conversion of the temperature range from one system of units to another.  
1.1.1 Procedure A (Sections 6 – 14)—Allows a larger selection of columns and analysis conditions such as packed and capillary columns as well as a Thermal Conductivity Detector in addition to the Flame Ionization Detector. Analysis times range from 14 min to 60 min.  
1.1.2 Procedure B (Sections 15 – 23)—Is restricted to only 3 capillary columns and requires no sample dilution. In addition, Procedure B is used not only for the sample types described in Procedure A but also for the analysis of samples containing biodiesel mixtures B5, B10, and B20. The analysis time, when using Procedure B (Accelerated D2887), is reduced to about 8 min.  
1.2 This test method is not to be used for the analysis of gasoline samples or gasoline components. These types of samples must be analyzed by Test Method D7096.  
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    35 pages
    English language
    sale 15% off
  • Standard
    35 pages
    English language
    sale 15% off