EN 14538:2006

Fat and oil derivatives - Fatty acid methyl ester (FAME) - Determination of Ca, K, Mg and Na content by optical emission spectral analysis with inductively coupled plasma (ICP OES)

This document specifies a procedure for the direct determination of the soap building elements Calcium (Ca), Magnesium (Mg), Sodium (Na) and Potassium (K) in fatty acid methyl esters (FAME) by ICP OES at levels of about 1 mg/kg to 10 mg/kg.

Erzeugnisse aus pflanzlichen und tierischen Fetten und Ölen - Fettsäure-Methylester (FAME) - Bestimmung des Ca-, K-, Mg- und Na-Gehaltes durch optische Emissionsspektralanalyse mit induktiv gekoppeltem Plasma (ICP OES)

Dieses Dokument legt ein Verfahren fest zur direkten Bestimmung der Seifebilder Calcium (Ca), Magnesium (Mg), Natrium (Na) und Kalium (K) in Fettsäure-Methylester (FAME) mittels ICP OES im Bereich von etwa 1 mg/kg bis 10 mg/kg.

Produits dérivés des corps gras - Esters méthyliques d'acides gras (EMAG) - Détermination de la teneur en Ca, K, Mg et Na par spectrométrie d'émission optique avec plasma à couplage inductif (ICP OES)

Le présent document prescrit une méthode de dosage direct du calcium (Ca), du magnésium (Mg), du sodium (Na) et du potassium (K), éléments susceptibles de former des savons, dans les esters méthyliques d'acides gras (EMAG) par ICP OES et s'applique à des teneurs allant d'environ 1 mg/kg à 10 mg/kg.

Derivati maščob in olj – Metil estri maščobnih kislin (FAME) – Določevanje Ca, K, Mg in Na z optično emisijsko spektometrijo z induktivno sklopljeno plazmo (ICP OES)

General Information

• Status: Published
• Publication Date: 06-Jun-2006
• ICS: 67.200.10 - Animal and vegetable fats and oils
• Technical Committee: CEN/TC 19 - Petroleum products, lubricants and related products
• Drafting Committee: CEN/TC 19/WG 27 - Elemental analysis of petroleum and related products
• Current Stage: 9093 - Decision to confirm - Review Enquiry
• Completion Date: 03-Dec-2019
• Ref Project: SIST EN 14538:2006 - Fat and oil derivatives - Fatty acid methyl ester (FAME) - Determination of Ca, K, Mg and Na content by optical emission spectral analysis with inductively coupled plasma (ICP OES)

Relations

• Revised: prEN 14538 - Fat and oil derivatives - Fatty acid methyl ester (FAME) - Determination of Ca, Mg, Na, K and P content by optical emission spectral analysis with inductively coupled plasma (ICP OES)
• Effective Date: 08-Nov-2023

Standards Content (Sample)

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Fat and oil derivatives - Fatty acid methyl ester (FAME) - Determination of Ca, K, Mg and Na content by optical emission spectral analysis with inductively coupled plasma (ICP OES)2(6Produits dérivés des corps gras - Esters méthyliques d'acides gras (EMAG) - Détermination de la teneur en Ca, K, Mg et Na par spectrométrie d'émission optique avec plasma a couplage inductif (ICP OES)Erzeugnisse aus pflanzlichen und tierischen Fetten und Ölen - Fettsäure-Methylester (FAME) - Bestimmung des Ca-, K-, Mg- und Na-Gehaltes durch optische Emissionsspektralanalyse mit induktiv gekoppeltem Plasma (ICP OES)Ta slovenski standard je istoveten z:EN 14538:2006SIST EN 14538:2006en67.200.10ICS:SLOVENSKI
STANDARDSIST EN 14538:200601-september-2006







EUROPEAN STANDARDNORME EUROPÉENNEEUROPÄISCHE NORMEN 14538June 2006ICS 67.200.10 English VersionFat and oil derivatives - Fatty acid methyl ester (FAME) -Determination of Ca, K, Mg and Na content by optical emissionspectral analysis with inductively coupled plasma (ICP OES)Produits dérivés des corps gras - Esters méthyliquesd'acides gras (EMAG) - Détermination de la teneur en Ca,K, Mg et Na par spectrométrie d'émission optique avecplasma à couplage inductif (ICP OES)Erzeugnisse aus pflanzlichen und tierischen Fetten undÖlen - Fettsäure-Methylester (FAME) - Bestimmung vonCa, K, Mg und Na durch optischeEmissionsspektralanalyse mit induktiv gekoppeltemPlasma (ICP OES)This European Standard was approved by CEN on 10 May 2006.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained on application to the Central Secretariat or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its own language and notified to the Central Secretariat has the same status as the officialversions.CEN members are the national standards bodies of Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France,Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania,Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMITÉ EUROPÉEN DE NORMALISATIONEUROPÄISCHES KOMITEE FÜR NORMUNGManagement Centre: rue de Stassart, 36
B-1050 Brussels© 2006 CENAll rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN 14538:2006: E



EN 14538:2006 (E)
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Contents Page Foreword.3 1 Scope.4 2 Normative references.4 3 Principle.4 4 Chemicals.4 5 Apparatus.4 6 Sampling.5 7 Preparation of the calibration solutions and the blank solution.5 7.1 General.5 7.2 Blank solution.6 7.3 Calibration solution with a nominal element content of 0,5 mg/kg.6 7.4 Calibration solution with a nominal element content of 1 mg/kg.6 7.5 Calibration solution with a nominal element content of 5 mg/kg.6 7.6 Calibration solution with a nominal element content of 10 mg/kg.6 8 Calibration.
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