Plastics - Determination of the molecular mass and molecular mass distribution of polymer species by matrix-assisted laser desorption/ionization time-of-flight mass spectrometry (MALDI-TOF-MS) (ISO 10927:2018)

This document specifies a general method for determining the average molecular mass and molecular mass distribution of polymers (see Reference [1]) from 2 000 g ⋅ mol−1 to 20 000 g ⋅ mol−1 by matrix-assisted laser desorption/ionization time-of-flight mass spectrometry (MALDI-TOF-MS).
The average molecular masses and molecular mass distributions are calculated from a calibration curve constructed using synthetic-polymer and/or biopolymer standards. This method is therefore classified as a relative method.
The method is not applicable to polyolefins or to polymers with a polydispersity >1,2.

Kunststoffe - Bestimmung der Molmasse und Molmassenverteilung von polymeren Species durch matrixunterstütze Laser-Desorptions/Ionisations-Flugzeit-Massenspektrometrie (MALDI-TOF-MS) (ISO 10927:2018)

Dieses Dokument legt ein allgemeines Verfahren zum Bestimmen der mittleren Molmasse und der
Molmassenverteilung von Polymeren (siehe Literaturhinweis [1]) in einem Molmassenbereich von
2 000 g ⋅ mol−1 bis 20 000 g ⋅ mol−1 durch die matrixunterstützte Laser-Desorptions/Ionisations-Flugzeit-
Massenspektrometrie (MALDI-TOF-MS) fest.
Die mittleren Molmassen und Molmassenverteilungen werden über eine Kalibrierkurve berechnet, die mit
Hilfe von synthetischen und/oder Biopolymerstandards erstellt wird. Daher handelt es sich um eine relative
Methode.
Das Verfahren ist nicht für Polyolefine oder Polymere mit einer Polydispersität > 1,2 anwendbar.

Plastiques - Détermination de la masse moléculaire et de la distribution des masses moléculaires des polymères par spectrométrie de masse, à temps de vol, après désorption/ionisation laser assistée par matrice (SM-MALDI-TOF) (ISO 10927:2018)

Le présent document spécifie une méthode générale permettant de déterminer la masse moléculaire moyenne et la distribution des masses moléculaires moyennes de polymères (voir Référence [1]) comprises entre 2 000 g ⋅ mol−1 et 20 000 g ⋅ mol−1 par spectrométrie de masse, à temps de vol, après désorption/ionisation laser assistée par matrice (SM-MALDI-TOF).
Les masses moléculaires et les distributions des masses moléculaires moyennes sont calculées à partir d'une courbe d'étalonnage établie à l'aide d'étalons de polymères synthétiques et/ou de biopolymères. Par conséquent, la présente méthode est classée comme méthode relative.
La présente méthode n'est pas applicable aux polyoléfines et aux polymères ayant une polydispersité > 1,2.

Polimerni materiali - Ugotavljanje molekulske mase in porazdelitve molekulske mase polimerov z masno spektrometrijo po laserski desorpciji/ionizaciji v nosilcu (matriksu) (MALDI-TOF-MS) (ISO 10927:2018)

Ta dokument določa splošno metodo za ugotavljanje povprečne molekulske mase in porazdelitve molekulske mase polimerov (glej sklic [1]) od 2000 g ⋅ mol−1 do 20.000 g ⋅ mol−1 z masno spektrometrijo po laserski desorpciji/ionizaciji v nosilcu (matriksu) (MALDI-TOF-MS).
Povprečne molekulske mase in porazdelitve molekulskih mas se izračunajo na podlagi kalibracijske krivulje, izdelane z uporabo standardov za sintetični polimer in/ali biopolimer. Ta metoda je zato klasificirana kot relativna metoda.
Metoda se ne uporablja za poliolefine oziroma polimere s polidisperzijo > 1,2.

General Information

Status
Published
Publication Date
10-Jul-2018
Withdrawal Date
30-Jan-2019
Current Stage
6060 - Definitive text made available (DAV) - Publishing
Start Date
11-Jul-2018
Completion Date
11-Jul-2018

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SLOVENSKI STANDARD
SIST EN ISO 10927:2018
01-december-2018
1DGRPHãþD
SIST EN ISO 10927:2011
Polimerni materiali - Ugotavljanje molekulske mase in porazdelitve molekulske
mase polimerov z masno spektrometrijo po laserski desorpciji/ionizaciji v nosilcu
(matriksu) (MALDI-TOF-MS) (ISO 10927:2018)
Plastics - Determination of the molecular mass and molecular mass distribution of
polymer species by matrix-assisted laser desorption/ionization time-of-flight mass
spectrometry (MALDI-TOF-MS) (ISO 10927:2018)
Kunststoffe - Bestimmung der Molmasse und Molmassenverteilung von polymeren
Species durch matrixunterstütze Laser-Desorptions/Ionisations-Flugzeit-
Massenspektrometrie (MALDI-TOF-MS) (ISO 10927:2018)
Plastiques - Détermination de la masse moléculaire et de la distribution des masses
moléculaires des polymères par spectrométrie de masse, à temps de vol, après
désorption/ionisation laser assistée par matrice (SM-MALDI-TOF) (ISO 10927:2018)
Ta slovenski standard je istoveten z: EN ISO 10927:2018
ICS:
71.040.50 Fizikalnokemijske analitske Physicochemical methods of
metode analysis
83.080.01 Polimerni materiali na Plastics in general
splošno
SIST EN ISO 10927:2018 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------

SIST EN ISO 10927:2018

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SIST EN ISO 10927:2018


EN ISO 10927
EUROPEAN STANDARD

NORME EUROPÉENNE

July 2018
EUROPÄISCHE NORM
ICS 83.080.01 Supersedes EN ISO 10927:2011
English Version

Plastics - Determination of the molecular mass and
molecular mass distribution of polymer species by matrix-
assisted laser desorption/ionization time-of-flight mass
spectrometry (MALDI-TOF-MS) (ISO 10927:2018)
Plastiques - Détermination de la masse moléculaire et Kunststoffe - Bestimmung der Molmasse und
de la distribution des masses moléculaires des Molmassenverteilung von polymeren Species durch
polymères par spectrométrie de masse, à temps de vol, matrixunterstütze Laser-Desorptions/Ionisations-
après désorption/ionisation laser assistée par matrice Flugzeit-Massenspektrometrie (MALDI-TOF-MS) (ISO
(SM-MALDI-TOF) (ISO 10927:2018) 10927:2018)
This European Standard was approved by CEN on 28 June 2018.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.

This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and United Kingdom.





EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2018 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 10927:2018 E
worldwide for CEN national Members.

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SIST EN ISO 10927:2018
EN ISO 10927:2018 (E)
Contents Page
European foreword . 3

2

---------------------- Page: 4 ----------------------

SIST EN ISO 10927:2018
EN ISO 10927:2018 (E)
European foreword
This document (EN ISO 10927:2018) has been prepared by Technical Committee ISO/TC 61 "Plastics"
in collaboration with Technical Committee CEN/TC 139 “Paints and varnishes” the secretariat of which
is held by DIN.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by January 2019, and conflicting national standards shall
be withdrawn at the latest by January 2019.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
This document supersedes EN ISO 10927:2011.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the
...

SLOVENSKI STANDARD
oSIST prEN ISO 10927:2017
01-april-2017
Polimerni materiali - Ugotavljanje molekularne mase in porazdelitev molekularne
mase z masno spektrometrijo po laserski desorpciji/ionizaciji i(MALDI-TOF-MS)
(ISO/DIS 10927:2017)
Plastics - Determination of the molecular mass and molecular mass distribution of
polymer species by matrix-assisted laser desorption/ionization time-of-flight mass
spectrometry (MALDI-TOF-MS) (ISO/DIS 10927:2017)
Kunststoffe - Bestimmung der Molmasse und Molmassenverteilung von polymeren
Species durch matrixunterstütze Laser-Desorptions/Ionisations-Flugzeit-
Massenspektrometrie (MALDI-TOF-MS) (ISO/DIS 10927:2017)
Plastiques - Détermination de la masse moléculaire et de la distribution des masses
moléculaires des polymères par spectrométrie de masse, à temps de vol, après
désorption/ionisation laser assistée par matrice (SM-MALDI-TOF) (ISO/DIS 10927:2017)
Ta slovenski standard je istoveten z: prEN ISO 10927
ICS:
83.080.01 Polimerni materiali na Plastics in general
splošno
oSIST prEN ISO 10927:2017 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------
oSIST prEN ISO 10927:2017

---------------------- Page: 2 ----------------------
oSIST prEN ISO 10927:2017
DRAFT INTERNATIONAL STANDARD
ISO/DIS 10927
ISO/TC 61/SC 5 Secretariat: DIN
Voting begins on: Voting terminates on:
2017-02-01 2017-04-25
Plastics — Determination of the molecular mass and
molecular mass distribution of polymer species by matrix-
assisted laser desorption/ionization time-of-flight mass
spectrometry (MALDI-TOF-MS)
Plastiques — Détermination de la masse moléculaire et de la distribution des masses moléculaires des
polymères par spectrométrie de masse, à temps de vol, après désorption/ionisation laser assistée par
matrice (SM-MALDI-TOF)
ICS: 83.080.01
THIS DOCUMENT IS A DRAFT CIRCULATED
This document is circulated as received from the committee secretariat.
FOR COMMENT AND APPROVAL. IT IS
THEREFORE SUBJECT TO CHANGE AND MAY
NOT BE REFERRED TO AS AN INTERNATIONAL
STANDARD UNTIL PUBLISHED AS SUCH.
IN ADDITION TO THEIR EVALUATION AS
ISO/CEN PARALLEL PROCESSING
BEING ACCEPTABLE FOR INDUSTRIAL,
TECHNOLOGICAL, COMMERCIAL AND
USER PURPOSES, DRAFT INTERNATIONAL
STANDARDS MAY ON OCCASION HAVE TO
BE CONSIDERED IN THE LIGHT OF THEIR
POTENTIAL TO BECOME STANDARDS TO
WHICH REFERENCE MAY BE MADE IN
Reference number
NATIONAL REGULATIONS.
ISO/DIS 10927:2017(E)
RECIPIENTS OF THIS DRAFT ARE INVITED
TO SUBMIT, WITH THEIR COMMENTS,
NOTIFICATION OF ANY RELEVANT PATENT
RIGHTS OF WHICH THEY ARE AWARE AND TO
©
PROVIDE SUPPORTING DOCUMENTATION. ISO 2017

---------------------- Page: 3 ----------------------
oSIST prEN ISO 10927:2017
ISO/DIS 10927:2017(E)

COPYRIGHT PROTECTED DOCUMENT
© ISO 2017, Published in Switzerland
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized otherwise in any form
or by any means, electronic or mechanical, including photocopying, or posting on the internet or an intranet, without prior
written permission. Permission can be requested from either ISO at the address below or ISO’s member body in the country of
the requester.
ISO copyright office
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CH-1214 Vernier, Geneva, Switzerland
Tel. +41 22 749 01 11
Fax +41 22 749 09 47
copyright@iso.org
www.iso.org
ii © ISO 2017 – All rights reserved

---------------------- Page: 4 ----------------------
oSIST prEN ISO 10927:2017
ISO/DIS 10927:2017(E)

Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Principle . 2
5 Reagents .
...

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