prEN 18082

Foods of animal origin - Multimethod for the determination of pesticide residues using LC-based analysis following acetonitrile extraction/partitioning and clean-up by dispersive SPE

This document specifies a method for the analysis of pesticide residues in foods of animal origin with a fat content of up to approximatively 10 %, such as meat, egg or milk by LC-MS/MS. Because of the low material requirements for miniaturized processing and the few work steps, the process is particularly time and cost-saving with high reliability and effectiveness. The method has been collaboratively studied on a number of commodity/pesticide combinations. Precision data are summarized in Table B.1. Guidelines for calibration are outlined in CEN/TS 17061.

Tierische Lebensmittel - Multiverfahren zur Bestimmung von Pestizidrückständen mit LC nach Acetonitril-Extraktion/Verteilung und Reinigung mit dispersiver SPE

Dieses Dokument legt ein Verfahren für die Analyse von Pestizidrückständen in Lebensmitteln tierischer Herkunft mit einem Fettgehalt von bis zu ca. 10 %, wie z. B. Fleisch, Eier oder Milch, mittels LC-MS/MS fest. Aufgrund der geringen Materialanforderungen für die miniaturisierte Verarbeitung und der wenigen Arbeitsschritte ist das Verfahren besonders zeit- und kostensparend bei hoher Zuverlässigkeit und Effektivität. Das Verfahren wurde im Ringversuch mit einer Reihe an Erzeugnis-/Pestizidkombinationen geprüft. Die Präzisionsdaten sind in Tabelle B.1 zusammengefasst. Eine Anleitung zur Kalibrierung ist in CEN/TS 17061 angegeben.

Aliments d'origine animale - Multiméthode de détermination des résidus de pesticides par analyse CL après extraction/partition avec de l'acétonitrile et purification par SPE dispersive

Le présent document décrit une méthode d'analyse CL-SM/SM des résidus de pesticides dans les aliments d'origine animale dont la teneur en matière grasse est inférieure ou égale à 10 % environ, tels que la viande, les œufs ou le lait. En raison des faibles besoins en produits pour la transformation miniaturisée et du nombre réduit d'étapes de travail, le processus est particulièrement économe en temps et en argent, tout en offrant une fiabilité et une efficacité élevées. La méthode a fait l'objet d'un essai interlaboratoires portant sur plusieurs combinaisons denrée/pesticide. Les données de fidélité sont résumées dans le Tableau B.1. Les lignes directrices relatives à l'étalonnage sont données dans la CEN/TS 17061.

Živila živalskega izvora - Multimetoda za določanje ostankov pesticidov z uporabo LC-analize po acetonitrilni ekstrakciji/delitvi in čiščenju z disperzijsko SPE

General Information

• Status: Not Published
• Publication Date: 21-Jan-2026
• ICS: 67.050 - General methods of tests and analysis for food products
• ICS: 67.120.01 - Animal produce in general
• Technical Committee: CEN/TC 275 - Food analysis - Horizontal methods
• Drafting Committee: CEN/TC 275/WG 3 - Pesticides and PCB's in foods of animal origin
• Current Stage: 4020 - Submission to enquiry - Enquiry
• Start Date: 23-May-2024
• Due Date: 05-Sep-2024
• Completion Date: 23-May-2024
• Ref Project: oSIST prEN 18082:2024 - Foods of animal origin - Multimethod for the determination of pesticide residues using LC-based analysis following acetonitrile extraction/partitioning and clean-up by dispersive SPE

Standards Content (Sample)

SLOVENSKI STANDARD
oSIST prEN 18082:2024
01-julij-2024
Živila živalskega izvora - Multimetoda za določanje ostankov pesticidov z uporabo
LC-analize po acetonitrilni ekstrakciji/delitvi in čiščenju z disperzijsko SPE
Foods of animal origin - Multimethod for the determination of pesticide residues using
LC-based analysis following acetonitrile extraction/partitioning and clean-up by
dispersive SPE
Tierische Lebensmittel - Multiverfahren zur Bestimmung von Pestizidrückständen mit LC
nach Acetonitril-Extraktion/Verteilung und Reinigung mit dispersiver SPE
Ta slovenski standard je istoveten z: prEN 18082
ICS:
67.050 Splošne preskusne in General methods of tests and
analizne metode za živilske analysis for food products
proizvode
67.120.01 Živila živalskega izvora na Animal produce in general
splošno
oSIST prEN 18082:2024 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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oSIST prEN 18082:2024

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oSIST prEN 18082:2024


DRAFT
EUROPEAN STANDARD
prEN 18082
NORME EUROPÉENNE

EUROPÄISCHE NORM

May 2024
ICS 67.050; 67.120.01
English Version

Foods of animal origin - Multimethod for the
determination of pesticide residues using LC-based
analysis following acetonitrile extraction/partitioning and
clean-up by dispersive SPE
 Tierische Lebensmittel - Multiverfahren zur
Bestimmung von Pestizidrückständen mit LC nach
Acetonitril-Extraktion/Verteilung und Reinigung mit
dispersiver SPE
This draft European Standard is submitted to CEN members for enquiry. It has been drawn up by the Technical Committee
CEN/TC 275.

If this draft becomes a European Standard, CEN members are bound to comply with the CEN/CENELEC Internal Regulations
which stipulate the conditions for giving this European Standard the status of a national standard without any alteration.

This draft European Standard was established by CEN in three official versions (English, French, German). A version in any other
language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC
Management Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and
United Kingdom.

Recipients of this draft are invited to submit, with their comments, notification of any relevant patent rights of which they are
aware and to provide supporting documentation.

Warning : This document is not a European Standard. It is distributed for review and comments. It is subject to change without
notice and shall not be referred to as a European Standard.


EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2024 CEN All rights of exploitation in any form and by any means reserved Ref. No. prEN 18082:2024 E
worldwide for CEN national Members.

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oSIST prEN 18082:2024
prEN 18082:2024(E)
Contents Page
European foreword . 4
1 Scope . 5
2 Normative references . 5
3 Terms and definitions . 5
4 Principle . 5
5 Preparation and storage of the samples . 5
5.1 General. 5
5.2 Laboratory sample . 6
5.3 Partly-prepared test sample . 6
5.4 Te
...