oSIST prEN IEC 62321-13:2025
(Main)Determination of certain substances in electrotechnical products - Part 13: Bisphenol A in plastics by liquid chromatography-diode array detection (LC-DAD), liquid chromatography-mass spectrometry (LC-MS) and liquid chromatography-tandem mass spectrometry (LC-MS/MS)
Determination of certain substances in electrotechnical products - Part 13: Bisphenol A in plastics by liquid chromatography-diode array detection (LC-DAD), liquid chromatography-mass spectrometry (LC-MS) and liquid chromatography-tandem mass spectrometry (LC-MS/MS)
Détermination de certaines substances dans les produits électrotechniques - Partie 13: Bisphénol A dans les plastiques par chromatographie en phase liquide avec détection à barrettes de diodes (LC-DAD), par chromatographie en phase liquide avec spectrométrie de masse (LC-MS) et par chromatographie en phase liquide avec spectrométrie de masse en tandem (LC-MS/MS)
Določevanje posameznih snovi v elektrotehničnih izdelkih - 13. del: Določevanje bisfenola A v plastiki s tekočinsko kromatografijo - določevanje s serijo diod (LC-DAD), tekočinsko kromatografijo - masno spektrometrijo (LC-MS) in tekočinsko kromatografijo - tandemsko masno spektrometrijo (LC-MS/MS)
General Information
Standards Content (Sample)
SLOVENSKI STANDARD
01-april-2025
Določevanje posameznih snovi v elektrotehničnih izdelkih - 13. del: Določevanje
bisfenola A v plastiki s tekočinsko kromatografijo - določevanje s serijo diod (LC-
DAD), tekočinsko kromatografijo - masno spektrometrijo (LC-MS) in tekočinsko
kromatografijo - tandemsko masno spektrometrijo (LC-MS/MS)
Determination of certain substances in electrotechnical products - Part 13: Bisphenol A
in plastics by liquid chromatography-diode array detection (LC-DAD), liquid
chromatography-mass spectrometry (LC-MS) and liquid chromatography-tandem mass
spectrometry (LC-MS/MS)
Détermination de certaines substances dans les produits électrotechniques - Partie 13:
Bisphénol A dans les plastiques par chromatographie en phase liquide avec détection à
barrettes de diodes (LC-DAD), par chromatographie en phase liquide avec spectrométrie
de masse (LC-MS) et par chromatographie en phase liquide avec spectrométrie de
masse en tandem (LC-MS/MS)
Ta slovenski standard je istoveten z: prEN IEC 62321-13:2025
ICS:
13.020.01 Okolje in varstvo okolja na Environment and
splošno environmental protection in
general
43.040.10 Električna in elektronska Electrical and electronic
oprema equipment
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.
111/799/CDV
COMMITTEE DRAFT FOR VOTE (CDV)
PROJECT NUMBER:
IEC 62321-13 ED1
DATE OF CIRCULATION: CLOSING DATE FOR VOTING:
2025-01-17 2025-04-11
SUPERSEDES DOCUMENTS:
111/685/CD, 111/790/CC
IEC TC 111 : ENVIRONMENTAL STANDARDIZATION FOR ELECTRICAL AND ELECTRONIC PRODUCTS AND SYSTEMS
SECRETARIAT: SECRETARY:
Italy Mr Alfonso Sturchio
OF INTEREST TO THE FOLLOWING COMMITTEES: HORIZONTAL FUNCTION(S):
TC 2,TC 9,TC 18,TC 20,TC 21,TC 23,TC 34,SC 34D,TC
TC 111 Horizontal Basic Environment - Assessment
59,TC 62,SC 65B,TC 80,TC 82,TC 88,TC 91,TC 100,TC
121,TC 124,TC 125
ASPECTS CONCERNED:
Environment
SUBMITTED FOR CENELEC PARALLEL VOTING NOT SUBMITTED FOR CENELEC PARALLEL VOTING
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clauses to be included should this proposal proceed. Recipients are reminded that the CDV stage is the final stage for
submitting ISC clauses. (SEE AC/22/2007 OR NEW GUIDANCE DOC).
TITLE:
Determination of certain substances in electrotechnical products – Part 13: Bisphenol A in plastics by
liquid chromatography-diode array detection (LC-DAD), liquid chromatography-mass spectrometry (LC-
MS) and liquid chromatography-tandem mass spectrometry (LC-MS/MS)
PROPOSED STABILITY DATE: 2029
NOTE FROM TC/SC OFFICERS:
electronic file, to make a copy and to print out the content for the sole purpose of preparing National Committee positions.
You may not copy or "mirror" the file or printed version of the document, or any part of it, for any other purpose without
permission in writing from IEC.
111/799/CDV -2- IEC CDV 62321-13 © IEC 2025
1 CONTENTS
2 FOREWORD . 3
3 INTRODUCTION . 5
4 1 Scope . 6
5 2 Normative references . 6
6 3 Definitions. 6
7 3.1 Terms and definitions . 6
8 3.2 Abbreviations . 6
9 4 Principle . 7
10 5 Reagents and materials . 7
11 6 Apparatus . 8
12 7 Sampling. 8
13 8 Procedure . 8
14 8.1 General instructions for the analysis. 8
15 8.2 Sample preparation . 9
16 8.2.1 Stock solution . 9
17 8.2.2 Extraction . 9
18 8.3 Instrumental parameters . 9
19 8.3.1 Stationary phase . 9
20 8.3.2 Liquid (mobile) phase . 9
21 8.4 Calibrants. 9
22 8.5 Calibration. 10
23 8.5.1 General . 10
24 8.5.2 Standard solutions . 10
25 9 Calculation of BPA concentration . 11
26 9.1 General . 11
27 9.2 Calculation . 11
28 10 Precision data . 12
29 10.1 LC-DAD Method . 12
30 10.2 LC-MS Method . 13
31 10.3 LC-MS/MS Method . 15
32 11 Quality assurance and quality control . 16
33 11.1 Performance . 16
34 11.2 Internal control samples and blanks . 17
35 11.3 Method detection limit and reporting limit . 17
36 12 Test report . 18
37 Annex A (informative) Conditions of each instrument . 19
38 Annex B (informative) Examples of chromatograms at suggested conditions . 22
39 Annex C (informative) Results of preliminary international Interlaboratory study (Pre-IIS 13)24
40 Annex D (informative) Results of International Interlaboratory study (IIS 13) . 27
111/799/CDV -3- IEC CDV 62321-13 © IEC 2025
42 INTERNATIONAL ELECTROTECHNICAL COMMISSION
43 ____________
45 DETERMINATION OF CERTAIN SUBSTANCES
46 IN ELECTROTECHNICAL PRODUCTS –
48 Part 13: Bisphenol A in plastics by liquid chromatography-diode array detector
49 (LC-DAD), liquid chromatography-mass spectrometry (LC-MS) and liquid
50 chromatography-tandem mass spectrometry (LC/MS-MS)
52 FOREWORD
53 1) The International Electrotechnical Commission (IEC) is a worldwide organization for standardization comprising all national
54 electrotechnical committees (IEC National Committees). The object of IEC is to promote international co-operation on all
55 questions concerning standardization in the electrical and electronic fields. To this end and in addition to other activities,
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79 8) Attention is drawn to the Normative references cited in this publication. Use of the referenced publications is indispensable
80 for the correct application of this publication.
81 9) Attention is drawn to the possibility that some of the elements of this IEC Publication may be the subject of patent rights.
82 IEC shall not be held responsible for identifying any or all such patent rights.
83 IEC 62321 has been prepared by technical committee 111: ENVIRONMENTAL STANDARDIZATION
84 FOR ELECTRICAL AND ELECTRONIC PRODUCTS AND SYSTEMS. It is an International Standard.
85 The text of this International Standard is based on the following documents:
FDIS Report on voting
XX/XX/FDIS XX/XX/RVD
87 Full information on the voting for its approval can be found in the report on voting indicated in the above
88 table.
89 The language used for the development of this International Standard is English.
111/799/CDV -4- IEC CDV 62321-13 © IEC 2025
90 This document was drafted in accordance with ISO/IEC Directives, Part 2, and developed in accordance
91 with ISO/IEC Directives, Part 1 and ISO/IEC Directives, IEC Supplement, available at
92 www.iec.ch/members_experts/refdocs. The main document types developed by IEC are described in
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94 The committee has decided that the contents of this document will remain unchanged until the stability
95 date indicated on the IEC website under "http://webstore.iec.ch" in the data related to the specific
96 document. At this date, the document will be
97 • reconfirmed,
98 • withdrawn,
99 • replaced by a revised edition, or
100 • amended.
111/799/CDV -5- IEC CDV 62321-13 © IEC 2025
101 INTRODUCTION
102 The widespread use of electrotechnical products has drawn increased attention to their impact on the
103 environment. In many countries this has resulted in the adaptation of regulations affecting waste,
104 substances and energy use of electrotechnical products.
105 The use of certain substances (e.g. lead (Pb), cadmium (Cd), mercury (Hg) and polybrominated diphenyl
106 ethers (PBDEs)), phthalates in electronical products is a source of concern in current and proposed
107 regional legislation.
108 The purpose of the IEC 62321 series is therefore to provide test methods that will allow the
109 electrotechnical industry to determine the levels of certain substances of concer
...
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