ASTM D6382/D6382M-99(2022)
(Practice)Standard Practice for Dynamic Mechanical Analysis and Thermogravimetry of Roofing and Waterproofing Membrane Material
Standard Practice for Dynamic Mechanical Analysis and Thermogravimetry of Roofing and Waterproofing Membrane Material
SIGNIFICANCE AND USE
5.1 Dynamic mechanical analysis provides a measure of the rheological properties of roofing and waterproofing membrane materials.
5.2 Thermogravimetry is used to characterize the thermal stability of roofing and waterproofing membrane materials under the specific temperature program and gaseous atmosphere conditions selected for the analysis.
5.3 Both dynamic mechanical analysis and thermogravimetry are used to evaluate the effect of either laboratory-simulated or in-service exposure on roofing and waterproofing membrane materials.
5.4 Both dynamic mechanical analysis and thermogravimetry can be applied to asphalt shingles. However, their application to asphalt shingles is beyond the scope of this practice, which is limited to low-slope membrane materials at this time.
5.5 This practice can be useful in the development of performance criteria for roofing and waterproofing membrane materials.
SCOPE
1.1 This practice covers test procedures and conditions that are applicable when Test Methods D5023, D5024, D5026, D5279, and D5418 are used for conducting dynamic mechanical analysis of roofing and waterproofing membrane material in three-point bending, compression, tension, torsion, and dual cantilever modes, respectively. The specific method is selected by the analyst and depends on the membrane material and the operating principles of the individual instrument used for the analysis.
1.2 This practice covers test procedures and conditions that are applicable when Test Method E1131 is used for conducting thermogravimetry of roofing and waterproofing membrane material.
1.3 Membrane materials include bituminous built-up roofing, polymer-modified bitumen sheets, vulcanized rubbers, non-vulcanized polymeric sheets, and thermoplastics. The membrane materials can be either nonreinforced or reinforced.
1.4 This practice is applicable to new membrane materials received from the supplier, those exposed artificially in the laboratory or outdoors on an exposure rack, and those sampled from field installations.
1.5 This practice contains notes which are explanatory and are not part of the mandatory requirements of this practice.
1.6 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.
1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
General Information
- Status
- Published
- Publication Date
- 31-Oct-2022
- Technical Committee
- D08 - Roofing and Waterproofing
- Drafting Committee
- D08.20 - Roofing Membrane Systems
Relations
- Effective Date
- 01-Oct-2023
- Refers
ASTM D5024-23 - Standard Test Method for Plastics: Dynamic Mechanical Properties: In Compression - Effective Date
- 01-Oct-2023
- Effective Date
- 01-Oct-2023
- Effective Date
- 01-Oct-2023
- Effective Date
- 01-Oct-2023
- Effective Date
- 01-Oct-2023
- Effective Date
- 01-May-2020
- Effective Date
- 15-Mar-2020
- Effective Date
- 15-Dec-2018
- Effective Date
- 15-Dec-2018
- Effective Date
- 01-Feb-2016
- Refers
ASTM D5024-15 - Standard Test Method for Plastics: Dynamic Mechanical Properties: In Compression - Effective Date
- 01-Jul-2015
- Effective Date
- 01-Jul-2015
- Effective Date
- 01-Jul-2015
- Effective Date
- 01-Jul-2015
Overview
ASTM D6382/D6382M-99(2022) is a standard practice developed by ASTM International for the dynamic mechanical analysis and thermogravimetry of roofing and waterproofing membrane materials. This standard outlines key procedures and test conditions for evaluating the performance characteristics and stability of a wide range of membrane materials, including bituminous built-up roofing, polymer-modified bitumen sheets, vulcanized rubbers, non-vulcanized polymeric sheets, and thermoplastics. The practice is applicable to both new and exposed materials, providing valuable data for quality control, research, and product development in the roofing and waterproofing industry.
Key Topics
Dynamic Mechanical Analysis (DMA)
- Measures rheological properties such as modulus, damping, and glass transition of membrane materials.
- Assesses structural integrity and viscoelastic behavior under varying temperatures and stresses.
Thermogravimetry (TGA)
- Evaluates thermal stability and composition by monitoring mass loss as a function of temperature.
- Determines degradation temperatures and residual content under specific atmospheres.
Material Scope
- Covers both reinforced and nonreinforced low-slope membrane materials.
- Suitable for materials sampled from suppliers, laboratory/artificial exposures, or field installations.
Conditions and Reporting
- Prescribes detailed specimen preparation, exposure documentation, and analytical parameters.
- Requires comprehensive reporting on sample history, test methods used, and results obtained.
Applications
The ASTM D6382/D6382M-99(2022) standard is widely used for:
Quality Assurance
- Ensures manufacturers and installers can verify that roofing and waterproofing membranes meet specified mechanical and thermal performance requirements.
Product Development
- Aids in the development of new membrane materials by providing standardized test procedures for benchmarking mechanical behavior and degradation properties.
Performance Evaluation
- Assesses the durability and long-term stability of membranes after accelerated laboratory aging or real-world exposure.
Regulatory Compliance
- Supports product certification and compliance with international standards and specifications for construction materials.
Forensic Analysis
- Used in investigating performance failures or premature aging in roofing systems, helping identify causes such as improper installation or material defects.
Related Standards
Several ASTM and international standards are referenced or related to the practice established in ASTM D6382/D6382M, including:
- ASTM D5023: Test Method for Plastics: Dynamic Mechanical Properties-In Flexure (Three-Point Bending)
- ASTM D5024: Test Method for Plastics: Dynamic Mechanical Properties-In Compression
- ASTM D5026: Test Method for Plastics: Dynamic Mechanical Properties-In Tension
- ASTM D5279: Test Method for Plastics: Dynamic Mechanical Properties-In Torsion
- ASTM D5418: Test Method for Plastics: Dynamic Mechanical Properties-Dual Cantilever Beam
- ASTM E1131: Test Method for Compositional Analysis by Thermogravimetry
- ASTM D1079, D4092, E473, E1142: Terminology standards relevant to roofing, plastics, and thermal analysis
Professionals implementing this standard should consult the full suite of referenced ASTM methods to ensure proper analysis and reporting.
Keywords: dynamic mechanical analysis, thermogravimetry, roofing membrane, waterproofing membrane, ASTM D6382, thermal analysis, mechanical properties, material testing, building materials standards, polymer-modified bitumen, roofing industry, construction materials compliance.
Get Certified
Connect with accredited certification bodies for this standard
ICC Evaluation Service
Building products evaluation and certification.
QAI Laboratories
Building and construction product testing and certification.
Aboma Certification B.V.
Specialized in construction, metal, and transport sectors.
Sponsored listings
Frequently Asked Questions
ASTM D6382/D6382M-99(2022) is a standard published by ASTM International. Its full title is "Standard Practice for Dynamic Mechanical Analysis and Thermogravimetry of Roofing and Waterproofing Membrane Material". This standard covers: SIGNIFICANCE AND USE 5.1 Dynamic mechanical analysis provides a measure of the rheological properties of roofing and waterproofing membrane materials. 5.2 Thermogravimetry is used to characterize the thermal stability of roofing and waterproofing membrane materials under the specific temperature program and gaseous atmosphere conditions selected for the analysis. 5.3 Both dynamic mechanical analysis and thermogravimetry are used to evaluate the effect of either laboratory-simulated or in-service exposure on roofing and waterproofing membrane materials. 5.4 Both dynamic mechanical analysis and thermogravimetry can be applied to asphalt shingles. However, their application to asphalt shingles is beyond the scope of this practice, which is limited to low-slope membrane materials at this time. 5.5 This practice can be useful in the development of performance criteria for roofing and waterproofing membrane materials. SCOPE 1.1 This practice covers test procedures and conditions that are applicable when Test Methods D5023, D5024, D5026, D5279, and D5418 are used for conducting dynamic mechanical analysis of roofing and waterproofing membrane material in three-point bending, compression, tension, torsion, and dual cantilever modes, respectively. The specific method is selected by the analyst and depends on the membrane material and the operating principles of the individual instrument used for the analysis. 1.2 This practice covers test procedures and conditions that are applicable when Test Method E1131 is used for conducting thermogravimetry of roofing and waterproofing membrane material. 1.3 Membrane materials include bituminous built-up roofing, polymer-modified bitumen sheets, vulcanized rubbers, non-vulcanized polymeric sheets, and thermoplastics. The membrane materials can be either nonreinforced or reinforced. 1.4 This practice is applicable to new membrane materials received from the supplier, those exposed artificially in the laboratory or outdoors on an exposure rack, and those sampled from field installations. 1.5 This practice contains notes which are explanatory and are not part of the mandatory requirements of this practice. 1.6 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard. 1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
SIGNIFICANCE AND USE 5.1 Dynamic mechanical analysis provides a measure of the rheological properties of roofing and waterproofing membrane materials. 5.2 Thermogravimetry is used to characterize the thermal stability of roofing and waterproofing membrane materials under the specific temperature program and gaseous atmosphere conditions selected for the analysis. 5.3 Both dynamic mechanical analysis and thermogravimetry are used to evaluate the effect of either laboratory-simulated or in-service exposure on roofing and waterproofing membrane materials. 5.4 Both dynamic mechanical analysis and thermogravimetry can be applied to asphalt shingles. However, their application to asphalt shingles is beyond the scope of this practice, which is limited to low-slope membrane materials at this time. 5.5 This practice can be useful in the development of performance criteria for roofing and waterproofing membrane materials. SCOPE 1.1 This practice covers test procedures and conditions that are applicable when Test Methods D5023, D5024, D5026, D5279, and D5418 are used for conducting dynamic mechanical analysis of roofing and waterproofing membrane material in three-point bending, compression, tension, torsion, and dual cantilever modes, respectively. The specific method is selected by the analyst and depends on the membrane material and the operating principles of the individual instrument used for the analysis. 1.2 This practice covers test procedures and conditions that are applicable when Test Method E1131 is used for conducting thermogravimetry of roofing and waterproofing membrane material. 1.3 Membrane materials include bituminous built-up roofing, polymer-modified bitumen sheets, vulcanized rubbers, non-vulcanized polymeric sheets, and thermoplastics. The membrane materials can be either nonreinforced or reinforced. 1.4 This practice is applicable to new membrane materials received from the supplier, those exposed artificially in the laboratory or outdoors on an exposure rack, and those sampled from field installations. 1.5 This practice contains notes which are explanatory and are not part of the mandatory requirements of this practice. 1.6 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard. 1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
ASTM D6382/D6382M-99(2022) is classified under the following ICS (International Classification for Standards) categories: 19.060 - Mechanical testing; 91.060.20 - Roofs. The ICS classification helps identify the subject area and facilitates finding related standards.
ASTM D6382/D6382M-99(2022) has the following relationships with other standards: It is inter standard links to ASTM E1142-23b, ASTM D5024-23, ASTM D5023-23, ASTM E473-23b, ASTM D5026-23, ASTM D5418-23, ASTM D1079-20, ASTM E1131-20, ASTM D1079-18, ASTM D1079-18e1, ASTM D1079-16, ASTM D5024-15, ASTM D5026-15, ASTM D5418-15, ASTM D5023-15. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.
ASTM D6382/D6382M-99(2022) is available in PDF format for immediate download after purchase. The document can be added to your cart and obtained through the secure checkout process. Digital delivery ensures instant access to the complete standard document.
Standards Content (Sample)
This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D6382/D6382M −99 (Reapproved 2022)
Standard Practice for
Dynamic Mechanical Analysis and Thermogravimetry of
Roofing and Waterproofing Membrane Material
This standard is issued under the fixed designation D6382/D6382M; the number immediately following the designation indicates the
year of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last
reapproval. A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope priate safety, health, and environmental practices and deter-
mine the applicability of regulatory limitations prior to use.
1.1 This practice covers test procedures and conditions that
1.8 This international standard was developed in accor-
are applicable when Test Methods D5023, D5024, D5026,
dance with internationally recognized principles on standard-
D5279, and D5418 are used for conducting dynamic mechani-
ization established in the Decision on Principles for the
calanalysisofroofingandwaterproofingmembranematerialin
Development of International Standards, Guides and Recom-
three-point bending, compression, tension, torsion, and dual
mendations issued by the World Trade Organization Technical
cantilever modes, respectively. The specific method is selected
Barriers to Trade (TBT) Committee.
by the analyst and depends on the membrane material and the
operating principles of the individual instrument used for the
2. Referenced Documents
analysis.
2.1 ASTM Standards:
1.2 This practice covers test procedures and conditions that
D1079Terminology Relating to Roofing and Waterproofing
are applicable whenTest Method E1131 is used for conducting
D4092 Terminology for Plastics: Dynamic Mechanical
thermogravimetry of roofing and waterproofing membrane
Properties
material.
D5023TestMethodforPlastics:DynamicMechanicalProp-
erties: In Flexure (Three-Point Bending)
1.3 Membrane materials include bituminous built-up
D5024TestMethodforPlastics:DynamicMechanicalProp-
roofing, polymer-modified bitumen sheets, vulcanized rubbers,
erties: In Compression
non-vulcanized polymeric sheets, and thermoplastics. The
D5026TestMethodforPlastics:DynamicMechanicalProp-
membrane materials can be either nonreinforced or reinforced.
erties: In Tension
1.4 This practice is applicable to new membrane materials
D5279TestMethodforPlastics:DynamicMechanicalProp-
received from the supplier, those exposed artificially in the
erties: In Torsion
laboratory or outdoors on an exposure rack, and those sampled
D5418TestMethodforPlastics:DynamicMechanicalProp-
from field installations.
erties: In Flexure (Dual Cantilever Beam)
1.5 This practice contains notes which are explanatory and
E473Terminology Relating to Thermal Analysis and Rhe-
are not part of the mandatory requirements of this practice.
ology
E1131Test Method for CompositionalAnalysis by Thermo-
1.6 The values stated in either SI units or inch-pound units
gravimetry
are to be regarded separately as standard. The values stated in
E1142Terminology Relating to Thermophysical Properties
each system may not be exact equivalents; therefore, each
system shall be used independently of the other. Combining
3. Terminology
values from the two systems may result in nonconformance
3.1 Definitions—For definitions of terms used in this
with the standard.
practice, refer to Terminologies E473, D1079, D4092, and
1.7 This standard does not purport to address all of the
E1142.
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appro-
4. Summary of Practice
4.1 In conducting a dynamic mechanical analysis, the roof-
ing or waterproofing membrane specimen is placed in a test
ThispracticeisunderthejurisdictionofASTMCommitteeD08onRoofingand
Waterproofing and is the direct responsibility of Subcommittee D08.20 on Roofing
Membrane Systems. For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Current edition approved Nov. 1, 2022. Published November 2022. Originally contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
approved in 1999. Last previous edition approved in 2017 as D6382/D6382M–99 Standards volume information, refer to the standard’s Document Summary page on
(2017). DOI: 10.1520/D6382_D6382M-99R22. the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
D6382/D6382M − 99 (2022)
chamber and subjected to a controlled, increasing temperature Note 2), taking care to avoid damage to the specimen. Use of
program. The temperature range can be from well below (for solvents other than water is not permissible. If water is used,
example, −80°C) to somewhat (for example, 50°C) above dry the sample overnight at 23 6 2°C [74 6 4°F] before
room temperature. The glass transition temperature, storage analysis.
modulus, loss modulus, and damping factor of the specimen
NOTE 2—In some cases where dirt or bonding adhesive is well adhered
are measured.
to the membrane material, it may not be possible to completely remove it.
In such cases, the decision to conduct the analysis is left to the analyst. If
4.2 In conducting a thermogravimetry analysis, the roofing
the analysis is conducted, the presence of dirt or bonding adhesive on the
or waterproofing membrane specimen is placed in a test
specimen is included in the report.
chamber and subjected to a controlled, increasing temperature
program. The temperature range can be from about room
7. Test Conditions
temperature (for example, 20 to 40°C) to well above room
7.1 Conduct the dynamic mechanical analysis using the
temperature (for example, 900°C), and the atmosphere of the
following conditions and parameters:
chamber is controlled through the use of inert gas such as
7.1.1 Preconditioning—Precondition the specimen in an
nitrogen or reactive gas such as air. The percent mass loss of
oven for1hat80 6 2°C [176 6 4°F] to provide a consistent
the specimen is determined as a function of temperature.
thermal history prior to analysis. Then allow the precondi-
tioned specimen to cool to 23 6 2°C [74 6 4°F] in a
5. Significance and Use
desiccator. Store the preconditioned specimen in the desiccator
5.1 Dynamic mechanical analysis provides a measure of the
at 23 6 2°C [74 6 4°F] until conducting the analysis.
rheological properties of roofing and waterproofing membrane
7.1.2 Temperature Range—The temperature range shall be
materials.
−80 to 50°C [−112 to 122°F], with an allowed variation of
5.2 The
...
Questions, Comments and Discussion
Ask us and Technical Secretary will try to provide an answer. You can facilitate discussion about the standard in here.
Loading comments...