Solid biofuels - Determination of ash content (ISO 18122:2022)

This document specifies a method for the determination of ash content of all solid biofuels.

Biogene Festbrennstoffe - Bestimmung des Aschegehaltes (ISO 18122:2022)

Dieses Dokument legt ein Verfahren zur Bestimmung des Aschegehaltes sämtlicher biogener Festbrennstoffe fest.

Biocombustibles solides - Détermination de la teneur en cendres (ISO 18122:2022)

Le présent document spécifie une méthode de détermination de la teneur en cendres de tous les biocombustibles solides.

Trdna biogoriva - Določevanje vsebnosti pepela (ISO 18122:2022)

Ta dokument opisuje metodo za določevanje vsebnosti pepela v vseh trdnih biogorivih.

General Information

Status
Published
Publication Date
15-Nov-2022
Technical Committee
Drafting Committee
Current Stage
6060 - Definitive text made available (DAV) - Publishing
Start Date
16-Nov-2022
Completion Date
16-Nov-2022

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SLOVENSKI STANDARD
SIST EN ISO 18122:2023
01-januar-2023
Nadomešča:
SIST EN ISO 18122:2016
Trdna biogoriva - Določevanje vsebnosti pepela (ISO 18122:2022)
Solid biofuels - Determination of ash content (ISO 18122:2022)
Biogene Festbrennstoffe - Bestimmung des Aschegehaltes (ISO 18122:2022)
Biocombustibles solides - Détermination de la teneur en cendres (ISO 18122:2022)
Ta slovenski standard je istoveten z: EN ISO 18122:2022
ICS:
75.160.40 Biogoriva Biofuels
SIST EN ISO 18122:2023 en,fr,de

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------
SIST EN ISO 18122:2023
---------------------- Page: 2 ----------------------
SIST EN ISO 18122:2023
EN ISO 18122
EUROPEAN STANDARD
NORME EUROPÉENNE
November 2022
EUROPÄISCHE NORM
ICS 27.190 Supersedes EN ISO 18122:2015
English Version
Solid biofuels - Determination of ash content (ISO
18122:2022)

Biocombustibles solides - Détermination de la teneur Biogene Festbrennstoffe - Bestimmung des

en cendres (ISO 18122:2022) Aschegehaltes (ISO 18122:2022)
This European Standard was approved by CEN on 30 October 2022.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this

European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references

concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN

member.

This European Standard exists in three official versions (English, French, German). A version in any other language made by

translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management

Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,

Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,

Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and

United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels

© 2022 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 18122:2022 E

worldwide for CEN national Members.
---------------------- Page: 3 ----------------------
SIST EN ISO 18122:2023
EN ISO 18122:2022 (E)
Contents Page

European foreword ....................................................................................................................................................... 3

---------------------- Page: 4 ----------------------
SIST EN ISO 18122:2023
EN ISO 18122:2022 (E)
European foreword

This document (EN ISO 18122:2022) has been prepared by Technical Committee ISO/TC 238 "Solid

biofuels" in collaboration with Technical Committee CEN/TC 335 “Solid biofuels” the secretariat of

which is held by SIS.

This European Standard shall be given the status of a national standard, either by publication of an

identical text or by endorsement, at the latest by May 2023, and conflicting national standards shall be

withdrawn at the latest by May 2023.

Attention is drawn to the possibility that some of the elements of this document may be the subject of

patent rights. CEN shall not be held responsible for identifying any or all such patent rights.

This document supersedes EN ISO 18122:2015.

Any feedback and questions on this document should be directed to the users’ national standards

body/national committee. A complete listing of these bodies can be found on the CEN website.

According to the CEN-CENELEC Internal Regulations, the national standards organizations of the

following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,

Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland,

Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Republic of

North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and the

United Kingdom.
Endorsement notice

The text of ISO 18122:2022 has been approved by CEN as EN ISO 18122:2022 without any modification.

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SIST EN ISO 18122:2023
---------------------- Page: 6 ----------------------
SIST EN ISO 18122:2023
INTERNATIONAL ISO
STANDARD 18122
Second edition
2022-11
Solid biofuels — Determination of ash
content
Biocombustibles solides — Détermination de la teneur en cendres
Reference number
ISO 18122:2022(E)
© ISO 2022
---------------------- Page: 7 ----------------------
SIST EN ISO 18122:2023
ISO 18122:2022(E)
COPYRIGHT PROTECTED DOCUMENT
© ISO 2022

All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may

be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting on

the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address below

or ISO’s member body in the country of the requester.
ISO copyright office
CP 401 • Ch. de Blandonnet 8
CH-1214 Vernier, Geneva
Phone: +41 22 749 01 11
Email: copyright@iso.org
Website: www.iso.org
Published in Switzerland
© ISO 2022 – All rights reserved
---------------------- Page: 8 ----------------------
SIST EN ISO 18122:2023
ISO 18122:2022(E)
Contents Page

Foreword ........................................................................................................................................................................................................................................iv

Introduction .................................................................................................................................................................................................................................v

1 S c op e ................................................................................................................................................................................................................................. 1

2 Nor m at i ve r ef er enc e s ..................................................................................................................................................................................... 1

3 Terms and definitions .................................................................................................................................................................................... 1

4 P r i nc iple ........................................................................................................................................................................................................................ 1

5 A pp a r at u s .................................................................................................................................................................................................................... 2

6 S a mple pr ep a r at ion ..........................................................................................................................................................................................2

6.1 General ........................................................................................................................................................................................................... 2

6.2 S ample conditioning .......................................................................................................................................................................... 2

7 P r o c e du re ....................................................................................................................................................................................................................3

7.1 G eneral ........................................................................................................................................................................................................... 3

7.2 C onditioning of dish ........................................................................................................................................................................... 3

7.3 C onditioning of the general analysis sample ............................................................................................................... 3

7.4 A shing of test portion ....................................................................................................................................................................... 3

7.5 Weighing ...................................................................................................................................................................................................... 3

7.6 C ompletion of ashing ......................................................................................................................................................................... 4

8 C a lc u l at ion .................................................................................................................................................................................................................. 4

9 Per f or m a nc e c h a r ac t er i s t ic s .................................................................................................................................................................. 4

10 Te s t r ep or t .................................................................................................................................................................................................................. 4

Annex A (informative) Performance data ...................................................................................................................................................... 5

Bibliography ................................................................................................................................................................................................................................ 7

iii
© ISO 2022 – All rights reserved
---------------------- Page: 9 ----------------------
SIST EN ISO 18122:2023
ISO 18122:2022(E)
Foreword

ISO (the International Organization for Standardization) is a worldwide federation of national standards

bodies (ISO member bodies). The work of preparing International Standards is normally carried out

through ISO technical committees. Each member body interested in a subject for which a technical

committee has been established has the right to be represented on that committee. International

organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.

ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of

electrotechnical standardization.

The procedures used to develop this document and those intended for its further maintenance are

described in the ISO/IEC Directives, Part 1. In particular, the different approval criteria needed for the

different types of ISO documents should be noted. This document was drafted in accordance with the

editorial rules of the ISO/IEC Directives, Part 2 (see www.iso.org/directives).

Attention is drawn to the possibility that some of the elements of this document may be the subject of

patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of

any patent rights identified during the development of the document will be in the Introduction and/or

on the ISO list of patent declarations received (see www.iso.org/patents).

Any trade name used in this document is information given for the convenience of users and does not

constitute an endorsement.

For an explanation of the voluntary nature of standards, the meaning of ISO specific terms and

expressions related to conformity assessment, as well as information about ISO's adherence to

the World Trade Organization (WTO) principles in the Technical Barriers to Trade (TBT), see

www.iso.org/iso/foreword.html.

This document was prepared by Technical Committee ISO/TC 238, Solid biofuels, in collaboration with

the European Committee for Standardization (CEN) Technical Committee CEN/TC 335, Solid biofuels, in

accordance with the Agreement on technical cooperation between ISO and CEN (Vienna Agreement).

This second edition cancels and replaces the first edition (ISO 18122:2015), which has been technically

revised.
The main changes are as follows:
— more detailed descriptions of the ashing furnace and ashing procedure;
— repeatability and reproducibility performance data updated;
— several references updated;
— minor editorial corrections.

Any feedback or questions on this document should be directed to the user’s national standards body. A

complete listing of these bodies can be found at www.iso.org/members.html.
© ISO 2022 – All rights reserved
---------------------- Page: 10 ----------------------
SIST EN ISO 18122:2023
ISO 18122:2022(E)
Introduction

Ash content is an important parameter for fuel deliveries since ash is a by-product of combustion and

ends up as bottom ash or fly-ash and needs to be removed. Depending on the jurisdiction, ash may be

deposited or used for production of other products or as fertilizer. Knowing how much ash comes with a

fuel can have economic consequences. Since the chemical composition of ash contributes to slagging and

corrosion in the combustion equipment, it is therefore important to know the amount of ash contained

in a fuel. Other testing standards are used for determining the chemical composition of ash.

© ISO 2022 – All rights reserved
---------------------- Page: 11 ----------------------
SIST EN ISO 18122:2023
---------------------- Page: 12 ----------------------
SIST EN ISO 18122:2023
INTERNATIONAL STANDARD ISO 18122:2022(E)
Solid biofuels — Determination of ash content
...

SLOVENSKI STANDARD
oSIST prEN ISO 18122:2021
01-december-2021
Trdna biogoriva - Določevanje vsebnosti pepela (ISO/DIS 18122:2021)
Solid biofuels - Determination of ash content (ISO/DIS 18122:2021)
Biogene Festbrennstoffe - Bestimmung des Aschegehaltes (ISO/DIS 18122:2021)

Biocombustibles solides - Détermination de la teneur en cendres (ISO/DIS 18122:2021)

Ta slovenski standard je istoveten z: prEN ISO 18122
ICS:
75.160.40 Biogoriva Biofuels
oSIST prEN ISO 18122:2021 en,fr,de

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------
oSIST prEN ISO 18122:2021
---------------------- Page: 2 ----------------------
oSIST prEN ISO 18122:2021
DRAFT INTERNATIONAL STANDARD
ISO/DIS 18122
ISO/TC 238 Secretariat: SIS
Voting begins on: Voting terminates on:
2021-10-01 2021-12-24
Solid biofuels — Determination of ash content
Biocombustibles solides — Méthode de détermination de la teneur en cendres
ICS: 27.190; 75.160.40
THIS DOCUMENT IS A DRAFT CIRCULATED
This document is circulated as received from the committee secretariat.
FOR COMMENT AND APPROVAL. IT IS
THEREFORE SUBJECT TO CHANGE AND MAY
NOT BE REFERRED TO AS AN INTERNATIONAL
STANDARD UNTIL PUBLISHED AS SUCH.
IN ADDITION TO THEIR EVALUATION AS
ISO/CEN PARALLEL PROCESSING
BEING ACCEPTABLE FOR INDUSTRIAL,
TECHNOLOGICAL, COMMERCIAL AND
USER PURPOSES, DRAFT INTERNATIONAL
STANDARDS MAY ON OCCASION HAVE TO
BE CONSIDERED IN THE LIGHT OF THEIR
POTENTIAL TO BECOME STANDARDS TO
WHICH REFERENCE MAY BE MADE IN
Reference number
NATIONAL REGULATIONS.
ISO/DIS 18122:2021(E)
RECIPIENTS OF THIS DRAFT ARE INVITED
TO SUBMIT, WITH THEIR COMMENTS,
NOTIFICATION OF ANY RELEVANT PATENT
RIGHTS OF WHICH THEY ARE AWARE AND TO
PROVIDE SUPPORTING DOCUMENTATION. ISO 2021
---------------------- Page: 3 ----------------------
oSIST prEN ISO 18122:2021
ISO/DIS 18122:2021(E)
COPYRIGHT PROTECTED DOCUMENT
© ISO 2021

All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may

be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting

on the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address

below or ISO’s member body in the country of the requester.
ISO copyright office
CP 401 • Ch. de Blandonnet 8
CH-1214 Vernier, Geneva
Phone: +41 22 749 01 11
Email: copyright@iso.org
Website: www.iso.org
Published in Switzerland
ii © ISO 2021 – All rights reserved
---------------------- Page: 4 ----------------------
oSIST prEN ISO 18122:2021
ISO/DIS 18122:2021(E)
Contents Page

Foreword ........................................................................................................................................................................................................................................iv

Introduction ..................................................................................................................................................................................................................................v

1 Scope ................................................................................................................................................................................................................................. 1

2 Normative references ...................................................................................................................................................................................... 1

3 Terms and definitions ..................................................................................................................................................................................... 1

4 Principle ........................................................................................................................................................................................................................ 1

5 Apparatus ..................................................................................................................................................................................................................... 2

5.1 Dish ................................................................................................................................................................................................................... 2

5.2 Furnace .......................................................................................................................................................................................................... 2

5.3 Balance ........................................................................................................................................................................................................... 2

5.4 Desiccator and desiccant ................................................................................................................................................................ 2

6 Sample preparation ........................................................................................................................................................................................... 2

6.1 Sample size ................................................................................................................................................................................................. 2

6.2 Sample conditioning........................................................................................................................................................................... 2

7 Procedure..................................................................................................................................................................................................................... 3

7.1 Conditioning of dish ........................................................................................................................................................................... 3

7.2 Conditioning of the general analysis sample ................................................................................................................ 3

7.3 Ashing of test portion ........................................................................................................................................................................ 3

7.4 Weighing ....................................................................................................................................................................................................... 3

7.5 Completion of ashing ......................................................................................................................................................................... 3

8 Calculation .................................................................................................................................................................................................................. 4

9 Performance characteristics .................................................................................................................................................................... 4

9.1 Repeatability ............................................................................................................................................................................................. 4

9.2 Reproducibility ....................................................................................................................................................................................... 4

10 Test Report .................................................................................................................................................................................................................. 4

Bibliography ................................................................................................................................................................................................................................ 6

© ISO 2021 – All rights reserved iii
---------------------- Page: 5 ----------------------
oSIST prEN ISO 18122:2021
ISO/DIS 18122:2021(E)
Foreword

ISO (the International Organization for Standardization) is a worldwide federation of national standards

bodies (ISO member bodies). The work of preparing International Standards is normally carried out

through ISO technical committees. Each member body interested in a subject for which a technical

committee has been established has the right to be represented on that committee. International

organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.

ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of

electrotechnical standardization.

The procedures used to develop this document and those intended for its further maintenance are

described in the ISO/IEC Directives, Part 1. In particular, the different approval criteria needed for the

different types of ISO documents should be noted. This document was drafted in accordance with the

editorial rules of the ISO/IEC Directives, Part 2 (see www .iso .org/ directives).

Attention is drawn to the possibility that some of the elements of this document may be the subject of

patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of

any patent rights identified during the development of the document will be in the Introduction and/or

on the ISO list of patent declarations received (see www .iso .org/ patents).

Any trade name used in this document is information given for the convenience of users and does not

constitute an endorsement.

For an explanation of the voluntary nature of standards, the meaning of ISO specific terms and

expressions related to conformity assessment, as well as information about ISO's adherence to the

World Trade Organization (WTO) principles in the Technical Barriers to Trade (TBT), see www .iso .org/

iso/ foreword .html.
This document was prepared by Technical Committee ISO/TC 238, Solid biofuels.

This second edition cancels and replaces the first edition (ISO 18122:2015), which has been technically

revised.
The main changes compared to the previous edition are as follows:

— The revision is required in order to provide more detailed descriptions of the ashing furnace and

ashing procedure, update the repeatability and reproducibility performance data, update several

references, and make other minor editorial corrections.

Any feedback or questions on this document should be directed to the user’s national standards body. A

complete listing of these bodies can be found at www .iso .org/ members .html.
iv © ISO 2021 – All rights reserved
---------------------- Page: 6 ----------------------
oSIST prEN ISO 18122:2021
ISO/DIS 18122:2021(E)
Introduction

Ash content is an important parameter for fuel deliveries since ash is a by-product of combustion and

ends up as bottom ash or fly-ash and needs to be removed. Depending on the jurisdiction, ash may

be deposited or used for production of other products and knowing how much ash comes with a fuel

may have economic consequences. In addition, the chemical composition of ash contributes to slagging

and corrosion in the combustion equipment and it is therefore important to know the amount of ash

contained in a fuel. Other testing standards are used for determining the chemical composition of ash.

© ISO 2021 – All rights reserved v
---------------------- Page: 7 ---
...

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