Metallic and oxide coatings - Measurement of coating thickness - Microscopical method (ISO 1463:2021)

This document specifies a method for the measurement of the local thickness of metallic coatings, oxide layers, and porcelain or vitreous enamel coatings, by the microscopical examination of cross-sections using an optical microscope.

Metall- und Oxidschichten - Schichtdickenmessung - Mikroskopisches Verfahren (ISO 1463:2021)

Dieses Dokument legt ein Verfahren zur Messung der örtlichen Schichtdicke von metallischen Überzügen, Oxidschichten und Emailschichten durch Untersuchung der Querschnittflächen mit einem Lichtmikroskop fest.
WARNUNG - Die Anwendung dieses Dokumentes kann den Einsatz gefährlicher Stoffe, Arbeitsgänge und Ausrüstungen mit sich bringen. Dieses Dokument erhebt nicht den Anspruch, auf alle Sicherheitsprobleme hinzuweisen, die mit ihrer Anwendung verbunden sind. Es liegt in der Verantwortung des Anwenders dieses Dokumentes, vor ihrer Anwendung geeignete Maßnahmen für die Sicherheit und den Gesundheitsschutz des Personals zu ergreifen.

Revêtements métalliques et couches d'oxyde - Mesurage de l'épaisseur de revêtement - Méthode par coupe micrographique (ISO 1463:2021)

Le présent document spécifie une méthode de mesure de l'épaisseur locale des revêtements métalliques, des couches d'oxyde, et des revêtements de porcelaine ou d'émail vitrifié, par examen de coupes transversales à l'aide d'un microscope optique.

Kovinske in oksidne prevleke - Merjenje debeline prevleke - Mikroskopska metoda (ISO 1463:2021)

General Information

Status
Published
Publication Date
25-May-2021
Withdrawal Date
29-Nov-2021
Current Stage
6060 - Definitive text made available (DAV) - Publishing
Start Date
26-May-2021
Completion Date
26-May-2021

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SLOVENSKI STANDARD
01-julij-2021
Nadomešča:
SIST EN ISO 1463:2004
Kovinske in oksidne prevleke - Merjenje debeline prevleke - Mikroskopska metoda
(ISO 1463:2021)
Metallic and oxide coatings - Measurement of coating thickness - Microscopical method
(ISO 1463:2021)
Metall- und Oxidschichten - Schichtdickenmessung - Mikroskopisches Verfahren (ISO
1463:2021)
Revêtements métalliques et couches d'oxyde - Mesurage de l'épaisseur de revêtement -
Méthode par coupe micrographique (ISO 1463:2021)
Ta slovenski standard je istoveten z: EN ISO 1463:2021
ICS:
25.220.20 Površinska obdelava Surface treatment
25.220.40 Kovinske prevleke Metallic coatings
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

EN ISO 1463
EUROPEAN STANDARD
NORME EUROPÉENNE
May 2021
EUROPÄISCHE NORM
ICS 25.220.20; 25.220.40 Supersedes EN ISO 1463:2004
English Version
Metallic and oxide coatings - Measurement of coating
thickness - Microscopical method (ISO 1463:2021)
Revêtements métalliques et couches d'oxyde - Metall- und Oxidschichten - Schichtdickenmessung -
Mesurage de l'épaisseur de revêtement - Méthode par Mikroskopisches Verfahren (ISO 1463:2021)
coupe micrographique (ISO 1463:2021)
This European Standard was approved by CEN on 17 April 2021.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and
United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2021 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 1463:2021 E
worldwide for CEN national Members.

Contents Page
European foreword . 3

European foreword
This document (EN ISO 1463:2021) has been prepared by Technical Committee ISO/TC 107 "Metallic
and other inorganic coatings" in collaboration with Technical Committee CEN/TC 262 “Metallic and
other inorganic coatings, including for corrosion protection and corrosion testing of metals and alloys”
the secretariat of which is held by BSI.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by November 2021, and conflicting national standards
shall be withdrawn at the latest by November 2021.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
This document supersedes EN ISO 1463:2004.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland,
Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Republic of
North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the
United Kingdom.
Endorsement notice
The text of ISO 1463:2021 has been approved by CEN as EN ISO 1463:2021 without any modification.

INTERNATIONAL ISO
STANDARD 1463
Fourth edition
2021-05
Metallic and oxide coatings —
Measurement of coating thickness —
Microscopical method
Revêtements métalliques et couches d'oxyde — Mesurage de
l'épaisseur de revêtement — Méthode par coupe micrographique
Reference number
ISO 1463:2021(E)
©
ISO 2021
ISO 1463:2021(E)
© ISO 2021
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting
on the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address
below or ISO’s member body in the country of the requester.
ISO copyright office
CP 401 • Ch. de Blandonnet 8
CH-1214 Vernier, Geneva
Phone: +41 22 749 01 11
Email: copyright@iso.org
Website: www.iso.org
Published in Switzerland
ii © ISO 2021 – All rights reserved

ISO 1463:2021(E)
Contents Page
Foreword .iv
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Principle . 1
5 Factors relating to measurement uncertainty . 1
5.1 Surface roughness . 1
5.2 Taper of cross-section . 2
5.3 Deformation of coating . 2
5.4 Rounding of edge of coating . 2
5.5 Overplating . 2
5.6 Etching . 2
5.7 Smearing . 2
5.8 Magnification . 2
5.9 Calibration of stage micrometer . 2
5.10 Calibration of the microscope’s length measuring device . 2
5.10.1 Micrometer eyepiece . 2
5.10.2 Digital image processing . 3
5.11 Uniformity of magnification . 3
5.12 Lens quality . 3
5.13 Orientation of measuring lines . 3
5.14 Tube length . 3
6 Preparation of cross-sections . 4
7 Measurement . 4
8 Measurement uncertainty . 4
9 Test report . 4
Annex A (informative) Guidance on the preparation and measurement of cross-sections .6
Annex B (informative) Taper of cross-section and measurement of tooth-constructed coatings .9
Annex C (informative) Some typical etchants for use at room temperature .12
Bibliography .13
ISO 1463:2021(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.
ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular, the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see www .iso .org/ directives).
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of
any patent rights identified during the development of the document will be in the Introduction and/or
on the ISO list of patent declarations received (see www .iso .org/ patents).
Any trade name used in this document is information given for the convenience of users and does not
constitute an endorsement.
For an explanation of the voluntary nature of standards, the meaning of ISO specific terms and
expressions related to conformity assessment, as well as information about ISO's adherence to the
World Trade Organization (WTO) principles in the Technical Barriers to Trade (TBT), see www .iso .org/
iso/ foreword .html.
This document was prepared by Technical Committee ISO/TC 107, Metallic and other inorganic coatings,
in collaboration with the European Committee for Standardization (CEN) Technical Committee CEN/
TC 262, Metallic and other inorganic coatings, including for corrosion protection and corrosion testing of
metals and alloys, in accordance with the Agreement on technical cooperation between ISO and CEN
(Vienna Agreement).
This fourth edition cancels and replaces the third edition (ISO 1463:2003), which has been technically
revised.
The main changes compared with the previous edition are as follows:
— digital image processing for light microscopes has been added;
— further hints and methods for the preparation of microsections have been added;
— one hazardous etching recipe has been removed from Annex C.
Any feedback or questions on this document should be directed to the user’s national standards body. A
complete listing of these
...

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