Plastics - Differential scanning calorimetry (DSC) - Part 2: Determination of glass transition temperature and glass transition step height (ISO 11357-2:2013)

EN-ISO 11357-2 specifies methods for the determination of the glass transition temperature and the step height related to the glass transition of amorphous and partially crystalline plastics.

Kunststoffe - Dynamische Differenz-Thermoanalyse (DSC) - Teil 2: Bestimmung der Glasübergangstemperatur und Stufenhöhe (ISO 11357-2:2013)

Dieser Teil von ISO 11357 legt Verfahren für die Bestimmung der Glasübergangstemperatur und der Stufenhöhe des Glasübergangs von amorphen und teilkristallinen Kunststoffen fest.

Plastiques - Analyse calorimétrique différentielle (DSC) - Partie 2: Détermination de la température de transition vitreuse et de la hauteur de palier de transition vitreuse (ISO 11357-2:2013)

L'ISO 11357-2:2013 spécifie des méthodes permettant de déterminer la température de transition vitreuse et la hauteur de palier de transition vitreuse associées à la transition vitreuse des plastiques amorphes et semi-cristallins.

Polimerni materiali - Diferenčna dinamična kalorimetrija (DSC) - 2. del: Ugotavljanje točke posteklenitve in višine stopnje prehoda (ISO 11357-2:2013)

Standard EN-ISO 11357-2 določa metode za ugotavljanje točke posteklenitve in višine stopnje prehoda amorfnih in delno kristaliničnih polimernih materialov.

General Information

Status
Withdrawn
Public Enquiry End Date
09-Feb-2014
Publication Date
01-Apr-2014
Withdrawal Date
31-Mar-2020
Current Stage
9900 - Withdrawal (Adopted Project)
Start Date
01-Apr-2020
Due Date
24-Apr-2020
Completion Date
01-Apr-2020

RELATIONS

Buy Standard

Standard
SIST EN ISO 11357-2:2014
English language
13 pages
sale 10% off
Preview
sale 10% off
Preview

e-Library read for
1 day
Draft
kSIST FprEN ISO 11357-2:2014
English language
13 pages
sale 10% off
Preview
sale 10% off
Preview

e-Library read for
1 day

Standards Content (sample)

SLOVENSKI STANDARD
SIST EN ISO 11357-2:2014
01-maj-2014
3ROLPHUQLPDWHULDOL'LIHUHQþQDGLQDPLþQDNDORULPHWULMD '6& GHO
8JRWDYOMDQMHWRþNHSRVWHNOHQLWYHLQYLãLQHVWRSQMHSUHKRGD ,62

Plastics - Differential scanning calorimetry (DSC) - Part 2: Determination of glass

transition temperature and glass transition step height (ISO 11357-2:2013)
Kunststoffe - Dynamische Differenz-Thermoanalyse (DSC) - Teil 2: Bestimmung der
Glasübergangstemperatur und Stufenhöhe (ISO 11357-2:2013)

Plastiques - Analyse calorimétrique différentielle (DSC) - Partie 2: Détermination de la

température de transition vitreuse et de la hauteur de palier de transition vitreuse (ISO

11357-2:2013)
Ta slovenski standard je istoveten z: EN ISO 11357-2:2014
ICS:
17.200.10 Toplota. Kalorimetrija Heat. Calorimetry
83.080.01 Polimerni materiali na Plastics in general
splošno
SIST EN ISO 11357-2:2014 en,fr,de

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------
SIST EN ISO 11357-2:2014
---------------------- Page: 2 ----------------------
SIST EN ISO 11357-2:2014
EUROPEAN STANDARD
EN ISO 11357-2
NORME EUROPÉENNE
EUROPÄISCHE NORM
March 2014
ICS 83.080.01
English Version
Plastics - Differential scanning calorimetry (DSC) - Part 2:
Determination of glass transition temperature and glass
transition step height (ISO 11357-2:2013)

Plastiques - Analyse calorimétrique différentielle (DSC) - Kunststoffe - Dynamische Differenz-Thermoanalyse (DSC) -

Partie 2: Détermination de la température de transition Teil 2: Bestimmung der Glasübergangstemperatur und

vitreuse et de la hauteur de palier de transition vitreuse Glasübergangsstufenhöhe (ISO 11357-2:2013)

(ISO 11357-2:2013)
This European Standard was approved by CEN on 6 March 2014.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European

Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national

standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member.

This European Standard exists in three official versions (English, French, German). A version in any other language made by translation

under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same

status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,

Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,

Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United

Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels

© 2014 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 11357-2:2014 E

worldwide for CEN national Members.
---------------------- Page: 3 ----------------------
SIST EN ISO 11357-2:2014
EN ISO 11357-2:2014 (E)
Contents Page

Foreword ..............................................................................................................................................................3

---------------------- Page: 4 ----------------------
SIST EN ISO 11357-2:2014
EN ISO 11357-2:2014 (E)
Foreword

The text of ISO 11357-2:2013 has been prepared by Technical Committee ISO/TC 61 “Plastics” of the

International Organization for Standardization (ISO) and has been taken over as EN ISO 11357-2:2014 by

Technical Committee CEN/TC 249 “Plastics” the secretariat of which is held by NBN.

This European Standard shall be given the status of a national standard, either by publication of an identical

text or by endorsement, at the latest by September 2014, and conflicting national standards shall be

withdrawn at the latest by September 2014.

Attention is drawn to the possibility that some of the elements of this document may be the subject of patent

rights. CEN [and/or CENELEC] shall not be held responsible for identifying any or all such patent rights.

According to the CEN-CENELEC Internal Regulations, the national standards organizations of the following

countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech

Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece,

Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,

Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom.

Endorsement notice

The text of ISO 11357-2:2013 has been approved by CEN as EN ISO 11357-2:2014 without any modification.

---------------------- Page: 5 ----------------------
SIST EN ISO 11357-2:2014
---------------------- Page: 6 ----------------------
SIST EN ISO 11357-2:2014
INTERNATIONAL ISO
STANDARD 11357-2
Second edition
2013-05-01
Plastics — Differential scanning
calorimetry (DSC) —
Part 2:
Determination of glass transition
temperature and glass transition step
height
Plastiques — Analyse calorimétrique différentielle (DSC) —
Partie 2: Détermination de la température de transition vitreuse et de
la hauteur de palier de transition vitreuse
Reference number
ISO 11357-2:2013(E)
ISO 2013
---------------------- Page: 7 ----------------------
SIST EN ISO 11357-2:2014
ISO 11357-2:2013(E)
COPYRIGHT PROTECTED DOCUMENT
© ISO 2013

All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized otherwise in any form

or by any means, electronic or mechanical, including photocopying, or posting on the internet or an intranet, without prior

written permission. Permission can be requested from either ISO at the address below or ISO’s member body in the country of

the requester.
ISO copyright office
Case postale 56 • CH-1211 Geneva 20
Tel. + 41 22 749 01 11
Fax + 41 22 749 09 47
E-mail copyright@iso.org
Web www.iso.org
Published in Switzerland
ii © ISO 2013 – All rights reserved
---------------------- Page: 8 ----------------------
SIST EN ISO 11357-2:2014
ISO 11357-2:2013(E)
Contents Page

Foreword ........................................................................................................................................................................................................................................iv

1 Scope ................................................................................................................................................................................................................................. 1

2 Normative references ...................................................................................................................................................................................... 1

3 Terms and definitions ..................................................................................................................................................................................... 1

4 Principle ........................................................................................................................................................................................................................ 2

5 Apparatus and materials.............................................................................................................................................................................. 2

6 Test specimens........................................................................................................................................................................................................ 2

7 Test conditions and specimen conditioning ............................................................................................................................ 2

8 Calibration .................................................................................................................................................................................................................. 2

9 Procedure..................................................................................................................................................................................................................... 2

9.1 Setting up the apparatus................................................................................................................................................................. 2

9.2 Loading the test specimen into the crucible .................................................................................................................. 2

9.3 Insertion of crucibles ......................................................................................................................................................................... 2

9.4 Temperature scan ................................................................................................................................................................................. 2

10 Expression of results ........................................................................................................................................................................................ 3

10.1 Determination of glass transition temperatures ....................................................................................................... 3

10.2 Determination of glass transition step height .............................................................................................................. 5

11 Precision ....................................................................................................................................................................................................................... 5

12 Test report ................................................................................................................................................................................................................... 5

Bibliography ................................................................................................................................................................................................................................ 6

© ISO 2013 – All rights reserved iii
---------------------- Page: 9 ----------------------
SIST EN ISO 11357-2:2014
ISO 11357-2:2013(E)
Foreword

ISO (the International Organization for Standardization) is a worldwide federation of national standards

bodies (ISO member bodies). The work of preparing International Standards is normally carried out

through ISO technical committees. Each member body interested in a subject for which a technical

committee has been established has the right to be represented on that committee. International

organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.

ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of

electrotechnical standardization.

International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2.

The main task of technical committees is to prepare International Standards. Draft International

Standards adopted by the technical committees are circulated to the member bodies for voting.

Publication as an International Standard requires approval by at least 75 % of the member bodies

casting a vote.

Attention is drawn to the possibility that some of the elements of this document may be the subject of

patent rights. ISO shall not be held responsible for identifying any or all such patent rights.

ISO 11357-2 was prepared by Technical Committee ISO/TC 61, Plastics, Subcommittee SC 5, Physical-

chemical properties.

This second edition cancels and replaces the first edition (ISO 11357-2:1999), which has been technically

revised. Significant technical changes are the following:
— deletion of duplicate text contained in ISO 11357-1;
— inclusion of determination of step height;
— description of characteristic glass temperatures moved from 3.3 to 10.1;
— inclusio
...

SLOVENSKI STANDARD
kSIST FprEN ISO 11357-2:2014
01-februar-2014
[Not translated]

Plastics - Differential scanning calorimetry (DSC) - Part 2: Determination of glass

transition temperature and glass transition step height (ISO 11357-2:2013)
Kunststoffe - Dynamische Differenz-Thermoanalyse (DSC) - Teil 2: Bestimmung der
Glasübergangstemperatur und Stufenhöhe (ISO 11357-2:2013)

Plastiques - Analyse calorimétrique différentielle (DSC) - Partie 2: Détermination de la

température de transition vitreuse et de la hauteur de palier de transition vitreuse (ISO

11357-2:2013)
Ta slovenski standard je istoveten z: FprEN ISO 11357-2
ICS:
17.200.10 Toplota. Kalorimetrija Heat. Calorimetry
83.080.01 Polimerni materiali na Plastics in general
splošno
kSIST FprEN ISO 11357-2:2014 en,fr,de

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------
kSIST FprEN ISO 11357-2:2014
---------------------- Page: 2 ----------------------
kSIST FprEN ISO 11357-2:2014
EUROPEAN STANDARD
FINAL DRAFT
FprEN ISO 11357-2
NORME EUROPÉENNE
EUROPÄISCHE NORM
September 2013
ICS 17.200.10; 83.080.01
English Version
Plastics - Differential scanning calorimetry (DSC) - Part 2:
Determination of glass transition temperature and glass
transition step height (ISO 11357-2:2013)

Plastiques - Analyse calorimétrique différentielle (DSC) - Kunststoffe - Dynamische Differenz-Thermoanalyse (DSC)

Partie 2: Détermination de la température de transition - Teil 2: Bestimmung der Glasübergangstemperatur und

vitreuse et de la hauteur de palier de transition vitreuse Stufenhöhe (ISO 11357-2:2013)

(ISO 11357-2:2013)

This draft European Standard is submitted to CEN members for unique acceptance procedure. It has been drawn up by the Technical

Committee CEN/TC 249.

If this draft becomes a European Standard, CEN members are bound to comply with the CEN/CENELEC Internal Regulations which

stipulate the conditions for giving this European Standard the status of a national standard without any alteration.

This draft European Standard was established by CEN in three official versions (English, French, German). A version in any other language

made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management

Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,

Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,

Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United

Kingdom.

Recipients of this draft are invited to submit, with their comments, notification of any relevant patent rights of which they are aware and to

provide supporting documentation.

Warning : This document is not a European Standard. It is distributed for review and comments. It is subject to change without notice and

shall not be referred to as a European Standard.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels

© 2013 CEN All rights of exploitation in any form and by any means reserved Ref. No. FprEN ISO 11357-2:2013: E

worldwide for CEN national Members.
---------------------- Page: 3 ----------------------
kSIST FprEN ISO 11357-2:2014
FprEN ISO 11357-2:2013 (E)
Contents Page

Foreword ..............................................................................................................................................................3

---------------------- Page: 4 ----------------------
kSIST FprEN ISO 11357-2:2014
FprEN ISO 11357-2:2013 (E)
Foreword

The text of ISO 11357-2:2013 has been prepared by Technical Committee ISO/TC 61 “Plastics” of the

International Organization for Standardization (ISO) and has been taken over as FprEN ISO 11357-2:2013 by

Technical Committee CEN/TC 249 “Plastics” the secretariat of which is held by NBN.

This document is currently submitted to the Unique Acceptance Procedure.
Endorsement notice

The text of ISO 11357-2:2013 has been approved by CEN as FprEN ISO 11357-2:2013 without any

modification.
---------------------- Page: 5 ----------------------
kSIST FprEN ISO 11357-2:2014
---------------------- Page: 6 ----------------------
kSIST FprEN ISO 11357-2:2014
INTERNATIONAL ISO
STANDARD 11357-2
Second edition
2013-05-01
Plastics — Differential scanning
calorimetry (DSC) —
Part 2:
Determination of glass transition
temperature and glass transition step
height
Plastiques — Analyse calorimétrique différentielle (DSC) —
Partie 2: Détermination de la température de transition vitreuse et de
la hauteur de palier de transition vitreuse
Reference number
ISO 11357-2:2013(E)
ISO 2013
---------------------- Page: 7 ----------------------
kSIST FprEN ISO 11357-2:2014
ISO 11357-2:2013(E)
COPYRIGHT PROTECTED DOCUMENT
© ISO 2013

All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized otherwise in any form

or by any means, electronic or mechanical, including photocopying, or posting on the internet or an intranet, without prior

written permission. Permission can be requested from either ISO at the address below or ISO’s member body in the country of

the requester.
ISO copyright office
Case postale 56 • CH-1211 Geneva 20
Tel. + 41 22 749 01 11
Fax + 41 22 749 09 47
E-mail copyright@iso.org
Web www.iso.org
Published in Switzerland
ii © ISO 2013 – All rights reserved
---------------------- Page: 8 ----------------------
kSIST FprEN ISO 11357-2:2014
ISO 11357-2:2013(E)
Contents Page

Foreword ........................................................................................................................................................................................................................................iv

1 Scope ................................................................................................................................................................................................................................. 1

2 Normative references ...................................................................................................................................................................................... 1

3 Terms and definitions ..................................................................................................................................................................................... 1

4 Principle ........................................................................................................................................................................................................................ 2

5 Apparatus and materials.............................................................................................................................................................................. 2

6 Test specimens........................................................................................................................................................................................................ 2

7 Test conditions and specimen conditioning ............................................................................................................................ 2

8 Calibration .................................................................................................................................................................................................................. 2

9 Procedure..................................................................................................................................................................................................................... 2

9.1 Setting up the apparatus................................................................................................................................................................. 2

9.2 Loading the test specimen into the crucible .................................................................................................................. 2

9.3 Insertion of crucibles ......................................................................................................................................................................... 2

9.4 Temperature scan ................................................................................................................................................................................. 2

10 Expression of results ........................................................................................................................................................................................ 3

10.1 Determination of glass transition temperatures ....................................................................................................... 3

10.2 Determination of glass transition step height .............................................................................................................. 5

11 Precision ....................................................................................................................................................................................................................... 5

12 Test report ................................................................................................................................................................................................................... 5

Bibliography ................................................................................................................................................................................................................................ 6

© ISO 2013 – All rights reserved iii
---------------------- Page: 9 ----------------------
kSIST FprEN ISO 11357-2:2014
ISO 11357-2:2013(E)
Foreword

ISO (the International Organization for Standardization) is a worldwide federation of national standards

bodies (ISO member bodies). The work of preparing International Standards is normally carried out

through ISO technical committees. Each member body interested in a subject for which a technical

committee has been established has the right to be represented on that committee. International

organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.

ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of

electrotechnical standardization.

International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2.

The main task of technical committees is to prepare International Standards. Draft International

Standards adopted by the technical committees are circulated to the member bodies for voting.

Publication as an International Standard requires approval by at least 75 % of the member bodies

casting a vote.

Attention is drawn to the possibility that some of the elements of this document may be the subject of

patent rights. ISO shall not be held responsible for identifying any or all such patent rights.

ISO 11357-2 was prepared by Technical Committee ISO/TC 61, Plastics, Subcommittee SC 5, Physical-

chemical properties.

This second edition cancels and replaces the first edition (ISO 11357-2:1999), which has been technically

revised. Significant technical changes are the following:
— deletion of duplicate text contained in ISO 11357-1;
— inclusion of determination of step height;
— description of characteristic glass temperatures moved from 3.3 to 10.1;

— inclusion of additional methods of determination of T based on inflection point and equal-areas

calculation.

ISO 11357 consists of the following parts, under the general title Plastics — Differential scanning

calorimetry (DSC):
— Part 1: General principles
— Part 2: Determination of glass transition temperature and glass tra
...

Questions, Comments and Discussion

Ask us and Technical Secretary will try to provide an answer. You can facilitate discussion about the standard in here.