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ASTM E1727-04

(Practice)

Standard Practice for Field Collection of Soil Samples for Lead Determination by Atomic Spectrometry Techniques

Standard Practice for Field Collection of Soil Samples for Lead Determination by Atomic Spectrometry Techniques

SCOPE
1.1 This practice covers the collection of soil samples using coring and scooping methods. Soil samples are collected in a manner that will permit subsequent digestion and determination of lead using laboratory analysis techniques such as Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES), Flame Atomic Absorption Spectrometry (FAAS), and Graphite Furnace Atomic Absorption Spectrometry (GFAAS).  
1.2 This practice is not suitable for collection of soil samples from areas that are paved.  
1.3 This practice does not address the sampling design criteria (that is, sampling plan that includes the number and location of samples) that are used for risk assessment and other purposes. To provide for valid conclusions, sufficient numbers of samples must be obtained as directed by a sampling plan.  
1.4 This practice contains notes that are explanatory and are not part of the mandatory requirements of this practice.  
1.5 The values stated in SI units are to be regarded as the standard. The inch-pound units given in parentheses are for information only.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
31-Jul-2004
ICS
71.040.50 - Physicochemical methods of analysis
Technical Committee
E06 - Performance of Buildings
Current Stage
Ref Project

Relations

Replaces
ASTM E1727-99 - Standard Practice for Field Collection of Soil Samples for Lead Determination by Atomic Spectrometry Techniques
Effective Date
01-Aug-2004
Replaced By
ASTM E1727-05 - Standard Practice for Field Collection of Soil Samples for Subsequent Lead Determination (Withdrawn 2014)
Effective Date
01-May-2005
Referred By
ASTM E3074/E3074M-20 - Standard Practice for Clearance Examinations Following Lead Hazard Reduction Activities in Single Family Dwellings, in Individual Units of Multifamily Dwellings, and in Other Child-Occupied Facilities
Effective Date
01-Aug-2004
Referred By
ASTM E3193-21 - Standard Test Method for Measurement of Lead (Pb) in Dust by Wipe, Paint, and Soil by Flame Atomic Absorption Spectrophotometry (FAAS)
Effective Date
01-Aug-2004
Referred By
ASTM E3203-21 - Standard Test Method for Determination of Lead in Dried Paint, Soil, and Wipe Samples by Inductively Coupled Plasma-Optical Emission Spectroscopy (ICP-OES)
Effective Date
01-Aug-2004
Referred By
ASTM E1979-21 - Standard Practice for Ultrasonic Extraction of Paint, Dust, Soil, and Air Samples for Subsequent Determination of Lead
Effective Date
01-Aug-2004
Referred By
ASTM E2115-22 - Standard Guide for Conducting Lead Hazard Assessments of Dwellings and of Other Child-Occupied Facilities
Effective Date
01-Aug-2004
Referred By
ASTM D8404-21 - Standard Practice for Preparation of Soil Samples by Ammonium Bifluoride-Nitric Acid Digestion for Subsequent Analysis for Metals and Metalloids
Effective Date
01-Aug-2004
Referred By
ASTM E2271/E2271M-22 - Standard Practice for Clearance Examinations Following Lead Hazard Reduction Activities in Multifamily Dwellings
Effective Date
01-Aug-2004
Referred By
ASTM D8064-16 - Standard Test Method for Elemental Analysis of Soil and Solid Waste by Monochromatic Energy Dispersive X-ray Fluorescence Spectrometry Using Multiple Monochromatic Excitation Beams
Effective Date
01-Aug-2004
Referred By
ASTM E1775-20 - Standard Guide for Evaluating Performance of On-Site Extraction and Field-Portable Electrochemical or Spectrophotometric Analysis for Lead
Effective Date
01-Aug-2004
Referred By
ASTM E1605-22 - Standard Terminology Relating to Lead in Buildings
Effective Date
01-Aug-2004
Referred By
ASTM E631-15 - Standard Terminology of Building Constructions
Effective Date
01-Aug-2004

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ASTM E1727-04 - Standard Practice for Field Collection of Soil Samples for Lead Determination by Atomic Spectrometry TechniquesASTM E1727-04 - Standard Practice for Field Collection of Soil Samples for Lead Determination by Atomic Spectrometry Techniques
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ASTM E1727-04 - Standard Practice for Field Collection of Soil Samples for Lead Determination by Atomic Spectrometry Techniques
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
An American National Standard
Designation:E1727–04
Standard Practice for
Field Collection of Soil Samples for Subsequent Lead
1
Determination
This standard is issued under the fixed designation E 1727; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope 3. Terminology
1.1 This practice covers the collection of soil samples from 3.1 Definitions—For definitions of terms not appearing
areas in and around buildings and related structures using here, see Terminology E 1605.
coring and scooping methods. 3.2 Definitions of Terms Specific to This Standard:
1.2 This practice is not suitable for collection of soil 3.2.1 soil collection container—a sealable rigid walled
samples from areas that are paved. container or a resealable plastic bag for holding and transport-
1.3 This practice does not address the sampling design ing the soil sample from the field to the laboratory.
criteria (that is, sampling plan that includes the number and 3.2.1.1 Discussion—The volume must be sufficient to hold
location of samples) that are used for risk assessment and other the entire collected subsample or sample and double bagging
lead hazard activities. may be needed to achieve resealability of a plastic bag.
1.4 This practice contains notes that are explanatory and are
4. Summary of Practice
not part of the mandatory requirements of this practice.
4.1 Soil samples are collected using coring or scooping
1.5 The values stated in SI units are to be regarded as the
standard. The inch-pound units given in parentheses are for methods.
information only.
5. Significance and Use
1.6 This standard does not purport to address all of the
5.1 Although this practice is intended for the collection of
safety concerns, if any, associated with its use. It is the
soil samples from areas in and around buildings, this practice
responsibility of the user of this standard to establish appro-
may also be used to collect soil samples from other areas and
priate safety and health practices and determine the applica-
environments.
bility of regulatory limitations prior to use.
5.2 This practice limits soil collection to approximately the
2. Referenced Documents
top 1.5 cm of soil surface.
2
5.3 These samples are collected in a manner that will permit
2.1 ASTM Standards:
E 1605 Terminology Relating to Lead in Buildings subsequent digestion and determination of lead using labora-
tory analysis techniques such as Inductively Coupled Plasma
E 1613 Test Method for Determination of Lead by Induc-
tively Coupled Plasma Atomic Emission Spectrometry Atomic Emission Spectrometry (ICP-AES) and Flame Atomic
Absorption Spectrometry (FAAS) (see Test Method E 1613).
(ICP-AES), Flame Atomic Absorption Spectrometry
(FAAS), or Graphite Furnace Atomic Absorption Spec-
6. Materials and Equipment
trometry (GFAAS) Techniques
6.1 Soil Coring Tool, minimum diameter of 2.5 cm, or as
E 1792 Specification for Wire Sampling Materials for Lead
agreed upon by the parties requesting and collecting the
in Surface Dust
samples, lead-free, for use in coring.
E 2239 Practice for Record Keeping and Record Preserva-
6.1.1 The coring tool shall be capable of being forced into
tion for Lead Hazard Activities
hard ground without damage to a depth of at least 5 cm (2 in.)
and have a mechanism to remove the soil sample from the tool
1
This practice is under the jurisdiction of ASTM Committee E06 on Perfor-
to permit discarding all but the top 1.5 cm (0.6 in.) of the soil
manceofBuildingsandisthedirectresponsibilityofSubcommitteeE06.23onLead
core (see Note 1).
Hazards Associated with Buildings.
Current edition approved August 1, 2004. Published August 2004. Originally
NOTE 1—A number of devices can be used or modified for use as soil
approved in 1994. Last previous edition approved in 1999 as E 1727 – 99.
coring tools. For example: professional stainless steel coring tools
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
equipped with plastic liners, steel pipe, plastic pipe, or small sapling (tree)
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
planters. Removal of the soil core is generally performed using a pair of
Standards volume information, refer to the standard’s Document Summary page on
plungers cut to fit the inside diameter of the coring device. One plunger is
the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
E1727–04
equipped with a stop that limits extension of the plunger to within 1.5 cm
...

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4.4.1 In the 1940s, industrial processes to co...
SCOPE
1.1 Per- and polyfluoroalkyl substances (PFAS) are a group of over 7,000 manmade compounds consisting of polymeric chains of carbon bonded to fluorine atoms, usually with a polar functional group at the head. This guide recognizes that PFAS can be categorized as polymeric or nonpolymeric, collectively amounting to more than 4,700 Chemical Abstracts Service (CAS)-registered substances. Environmental concerns pertaining to PFAS are centered primarily on the perfluoroalkyl acids (PFAA), a subclass of per-and polyfluoroalkyl substances, which display extreme persistence and chain-length dependent bioaccumulation and adverse effects in biota.  
1.2 The regulatory framework for PFAS continues to evolve, both domestically and internationally. The United States Environmental Protection Agency (EPA) is proceeding with a wide-ranging set of PFAS regulatory actions (EPA, 2021). While the Comprehensive Environmental Response, Compensation, and Liability Act (CERCLA) does not currently recognize PFAS as hazardous substances, the statute does require actions to protect public health and the environment from contaminants and pollutants released to the environment. Other federal regulatory programs, such as the Safe Drinking Water Act are being used to address drinking water supplies adversely impacted by releases of PFAS. The Clean Water Act’s National Pollutant Discharge Elimination System (NPDES) permitting program is tool that both federal and state regulators are using to regulate the inflows of PFAS-impacted wastewaters at both publicly-owned treatment works (POTW) and federally-owned wastewater treatment plants and the concentration of PFAS in permitted effluent. EPA continues to add additional per-and polyfluoroalkyl substances to the list of substances reportable under the federal Toxic Release Inventory (TRI) reporting program. International efforts to address per-and polyfluoroalkyl substances include Australia’s PFAS Nation...

  • Guide
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  • Guide
    23 pages
    English language
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ASTM
ASTM G136-03(2023)e1(Practice)
Standard Practice for Determination of Soluble Residual Contaminants in Materials by Ultrasonic Extraction

SIGNIFICANCE AND USE
5.1 This practice is suitable for the determination of extractable substances that may be found in materials used in systems or components requiring a high level of cleanliness, such as oxygen systems. Soft goods, such as seals and valve seats, may be tested as received. Gloves and wipes, or samples thereof, to be used in cleaning operations may be evaluated prior to use to ensure that the proposed extracting agent does not extract or deposit chemicals, or both, on the surface to be cleaned.  
5.2 Wipes or other cleaning equipment may be tested after use to determine the amount of contaminant removed from a surface.
Note 1: The amount of material extracted may be dependent upon the frequency and power density of the ultrasonic unit.  
5.3 The extraction efficiency has been shown to vary with the frequency and power density of the ultrasonic unit. The unit, therefore, must be carefully evaluated to optimize the extraction conditions.
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1.1 This practice may be used to extract nonvolatile and semivolatile residues from materials such as new and used gloves, new and used wipes, component soft goods, and so forth. When used with proposed cleaning materials (wipes, gloves, and so forth), this practice may be used to determine the potential of the proposed solvent or other fluids to extract contaminants (plasticizers, residual detergents, brighteners, and so forth) and deposit them on the surface being cleaned.  
1.2 This practice is not suitable for the evaluation of particulate contamination.  
1.3 The values stated in SI units are to be regarded standard. No other units of measurement are included in this standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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