Corrosion of metals and alloys - Aqueous corrosion testing of zirconium alloys for use in nuclear power reactors (ISO 10270:2022)

This document specifies:
a) the determination of mass gain;
b) the surface inspection of products of zirconium and its alloys when corrosion is tested in water at 360 °C or in steam at or above 400 °C;
c) the performance of tests in steam at 10,3 MPa.
This document is applicable to wrought products, castings, powder metallurgy products and weld metals.
This method has been widely used in the development of new alloys, heat-treating practices and for the evaluation of welding techniques. It is applicable for use in its entirety to the extent specified for a product acceptance test, rather than merely a means of assessing performance in service.

Korrosion von Metallen und Legierungen - Korrosionsprüfung in wässrigen Lösungen für in Kernreaktoren angewendete Zirkoniumlegierungen (ISO 10270:2022)

Dieses Dokument legt fest:
a) die Bestimmung der Massezunahme;
b) die Untersuchung der Oberflächen von Produkten aus Zirkonium und Zirkoniumlegierungen nach einer Korrosionsprüfung in Wasser bei 360 °C oder in Dampf bei oder über 400 °C;
c) die Durchführung der Prüfungen in Dampf unter einem Druck von 10,3 MPa.
Dieses Dokument ist auf Schmiedeprodukte, Gussteile, pulvermetallurgische Produkte und Schweißgut anwendbar.
Das Verfahren wurde bereits vielfach zur Entwicklung neuer Legierungen und Wärmebehandlungsverfahren sowie zur Bewertung von Schweißverfahren genutzt. Es ist nicht nur zur Beurteilung des Betriebsverhaltens anwendbar, sondern stattdessen als Ganzes in dem Umfang, der zur Abnahmeprüfung des jeweiligen Produkts festgelegt ist.
WARNUNG - Dieses Dokuments kann die Anwendung von gefährlichen Materialien, Arbeitsgängen und Einrichtungen zur Folge haben (siehe Abschnitt 9). Die Anwender dieses Dokuments sind dafür verantwortlich, vor Anwendung geeignete Maßnahmen zur Einhaltung der Sicherheit und zum Schutz der Gesundheit zu ergreifen und die zutreffenden gesetzlichen Einschränkungen zu beachten.

Corrosion des métaux et alliages - Essais de corrosion aqueuse des alliages de zirconium utilisés dans les réacteurs nucléaires (ISO 10270:2022)

Le présent document décrit :
a) la détermination du gain en masse ;
b) le contrôle superficiel des produits en zirconium et en alliages de zirconium après essai de corrosion dans l'eau à 360 °C et dans la vapeur à 400 °C ou plus ;
c) les performances des essais dans la vapeur à 10,3 MPa.
Le présent document est applicable aux produits corroyés, moulés, aux produits de la métallurgie des poudres et aux métaux d'apport pour le soudage.
La méthode a été beaucoup utilisée pour mettre au point de nouveaux alliages et de nouvelles techniques de traitement thermique et à évaluer les techniques de soudage Elle peut être utilisée dans sa totalité comme moyen de réception des produits plutôt que comme moyen d'évaluation de leurs propriétés en service.

Korozija kovin in zlitin - Preskušanje vodne korozije cirkonijevih zlitin za uporabo v jedrskih reaktorjih (ISO 10270:2022)

Ta dokument določa: a) določevanje povečanja mase; b) pregledovanje površine proizvodov iz cirkonija in njegovih zlitin pri preskušanju korozije v vodi pri temperaturi 360 °C ali v pari pri temperaturi 400 °C ali več; c) izvajanje preskusov v pari pri tlaku 10,3 MPa. Ta dokument se uporablja za gnetene zlitine, ulitke, proizvode, izdelane z metalurgijo prahu, in zvarne kovine. Ta metoda se pogosto uporablja pri razvoju novih zlitin, v postopkih toplotne obdelave in za vrednotenje tehnik varjenja. V obsegu, določenem za preskus sprejemljivosti proizvoda, se lahko uporablja v celoti in ne zgolj kot sredstvo za ocenjevanje učinkovitosti delovanja.

General Information

Status
Published
Publication Date
22-Feb-2022
Withdrawal Date
30-Aug-2022
Current Stage
6060 - Definitive text made available (DAV) - Publishing
Start Date
23-Feb-2022
Completion Date
23-Feb-2022

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SLOVENSKI STANDARD
01-april-2022
Nadomešča:
SIST EN ISO 10270:2008
Korozija kovin in zlitin - Preskušanje vodne korozije cirkonijevih zlitin za uporabo
v jedrskih reaktorjih (ISO 10270:2022)
Corrosion of metals and alloys - Aqueous corrosion testing of zirconium alloys for use in
nuclear power reactors (ISO 10270:2022)
Korrosion von Metallen und Legierungen - Korrosionsprüfung in wässrigen Lösungen für
in Kernreaktoren angewendete Zirkoniumlegierungen (ISO 10270:2022)
Corrosion des métaux et alliages - Essais de corrosion aqueuse des alliages de
zirconium utilisés dans les réacteurs nucléaires (ISO 10270:2022)
Ta slovenski standard je istoveten z: EN ISO 10270:2022
ICS:
27.120.99 Drugi standardi v zvezi z Other standards related to
jedrsko energijo nuclear energy
77.060 Korozija kovin Corrosion of metals
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

EN ISO 10270
EUROPEAN STANDARD
NORME EUROPÉENNE
February 2022
EUROPÄISCHE NORM
ICS 27.120.10; 77.060 Supersedes EN ISO 10270:2008
English Version
Corrosion of metals and alloys - Aqueous corrosion testing
of zirconium alloys for use in nuclear power reactors (ISO
10270:2022)
Corrosion des métaux et alliages - Essais de corrosion Korrosion von Metallen und Legierungen -
aqueuse des alliages de zirconium utilisés dans les Korrosionsprüfung in wässrigen Lösungen für in
réacteurs nucléaires (ISO 10270:2022) Kernreaktoren angewendete Zirkoniumlegierungen
(ISO 10270:2022)
This European Standard was approved by CEN on 26 December 2021.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and
United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2022 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 10270:2022 E
worldwide for CEN national Members.

Contents Page
European foreword . 3

European foreword
This document (EN ISO 10270:2022) has been prepared by Technical Committee ISO/TC 156
"Corrosion of metals and alloys" in collaboration with Technical Committee CEN/TC 262 “Metallic and
other inorganic coatings, including for corrosion protection and corrosion testing of metals and alloys”
the secretariat of which is held by BSI.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by August 2022, and conflicting national standards shall
be withdrawn at the latest by August 2022.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
This document supersedes EN ISO 10270:2008.
Any feedback and questions on this document should be directed to the users’ national standards
body/national committee. A complete listing of these bodies can be found on the CEN website.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland,
Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Republic of
North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the
United Kingdom.
Endorsement notice
The text of ISO 10270:2022 has been approved by CEN as EN ISO 10270:2022 without any modification.

INTERNATIONAL ISO
STANDARD 10270
Second edition
2022-02
Corrosion of metals and alloys —
Aqueous corrosion testing of
zirconium alloys for use in nuclear
power reactors
Corrosion des métaux et alliages — Essais de corrosion aqueuse des
alliages de zirconium utilisés dans les réacteurs nucléaires
Reference number
ISO 10270:2022(E)
ISO 10270:2022(E)
© ISO 2022
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting on
the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address below
or ISO’s member body in the country of the requester.
ISO copyright office
CP 401 • Ch. de Blandonnet 8
CH-1214 Vernier, Geneva
Phone: +41 22 749 01 11
Email: copyright@iso.org
Website: www.iso.org
Published in Switzerland
ii
ISO 10270:2022(E)
Contents Page
Foreword .iv
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Principle . 2
5 Significance . 2
6 Interference. 2
7 Reagents and materials . 2
8 Apparatus . 3
9 Hazards . 3
10 Sampling, test specimens and test units . 3
11 Preparation of apparatus .4
12 Calibration and standardization .4
12.1 High mass gain coupon preparation . 4
12.2 Autoclaves . 4
12.3 Use of control coupons. 7
12.4 Calibration . 7
13 Conditioning .7
13.1 Test water quality . 7
13.2 Autoclave load restrictions . 8
13.3 Test conditions . 8
13.3.1 Temperature . 8
13.3.2 Pressure . 8
13.3.3 Time . 8
13.3.4 Tests . 8
13.4 Specimen preparation . 8
13.4.1 Etched specimens . 8
13.4.2 As-manufacturer specimens . 8
14 Procedure .8
14.1 Inspection of specimens . . 8
14.2 Dimensions, weight and inspection . 9
14.3 Autoclaving . 9
14.3.1 Placing of test specimens . 9
14.3.2 Venting method A . 9
14.3.3 Venting method B . 10
14.3.4 Closed system method C . 10
14.3.5 Refreshed autoclaving, method D . 11
14.4 Post-test measurements and inspection . 11
15 Calculation or interpretation of results .11
15.1 Calculation of mass gain . 11
15.2 Visual interpretation of surface appearance .12
15.3 Invalid tests .
...

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