EN ISO 17993:2003

Water quality - Determination of 15 polycyclic aromatic hydrocarbons (PAH) in water by HPLC with fluorescence detection after liquid-liquid extraction (ISO 17993:2002)

ISO 17993:2002 specifies a method using high performance liquid chromatography (HPLC) with fluorescence detection for the determination of 15 selected polycyclic aromatic hydrocarbons (PAH) [naphthalene, acenaphthene, phenanthrene, fluoranthene, benzo(a)anthracene, benzo(b)fluoranthene, benzo(a)pyrene, dibenzo(a,h)anthracene, fluorene, anthracene, pyrene, chrysene, benzo(k)fluoranthene, indeno(1,2,3-cd)pyrene, benzo(ghi)perylene] in drinking and ground water in mass concentrations greater than 0,005 microgram/litre (for each single compound) and surface waters in mass concentrations above 0,01 microgram/litre.
This method is, with some modification, also suitable for the analysis of waste water. This method may be applicable to other PAH, provided the method is validated for each case.

Wasserbeschaffenheit - Bestimmung von 15 polycyclischen aromatischen Kohlenwasserstoffen (PAK) in Wasser durch HPLC mit Fluoreszenzdetektion nach Flüssig-Flüssig-Extraktion (ISO 17993:2002)

Diese Internationale Norm legt ein Verfahren zur Bestimmung von 15 ausgewählten PAK (siehe Tabelle 1) mit Hilfe der hochauflösenden Dampfraumnanalyse (HPLC) nach flüssig-flüssig-Extraktion und Fluoreszenzs-pektrometrie fest. Das Verfahren wird angewendet auf Trink- und Grundwasser in Massenkonzentrationen oberhalb 0,005 µg/l (Einzelsubstanz) und auf Oberflächenwasser in Massenkonzentrationen oberhalb 0,01 µg/l fest.
Das Verfahren ist nach Anpassung auch geeignet für die Untersuchung von Abwasser. Das Verfahren darf auch auf andere PAK angewendet werden, vorausgesetzt, es wird in jedem Einzelfall validiert.

Qualité de l'eau - Dosage de 15 hydrocarbures aromatiques polycycliques (HAP) dans l'eau par HPLC avec détection par fluorescence après extraction liquide-liquide (ISO 17993:2002)

La présente Norme internationale spécifie une méthode pour le dosage, par chromatographie en phase liquide à haute performance (HPLC) avec détection par fluorescence, de 15 HAP sélectionnés (voir Tableau 1) dans l'eau potable et dans les eaux souterraines à des concentrations en masse supérieures à 0,005 microgrammes par litre (pour chaque composé individuel), et dans les eaux de surface à des concentrations en masse supérieures à 0,01 microgrammes par litre.
Cette méthode est également appropriée, avec certaines modifications, pour l'analyse des eaux usées. Elle peut être appliquée à d'autres HAP, sous réserve de valider la méthode dans chaque cas.

Kakovost vode – Določevanje 15 policikličnih aromatskih ogljikovodikov (PAH) v vodi s tehniko HPLC s fluorescenčno detekcijo po ekstrakciji tekoče-tekoče (ISO 17993:2002)

General Information

• Status: Published
• Publication Date: 25-Nov-2003
• ICS: 13.060.50 - Examination of water for chemical substances
• Technical Committee: CEN/TC 230 - Water analysis
• Drafting Committee: CEN/TC 230/WG 1 - Physical and biochemical methods
• Current Stage: 9093 - Decision to confirm - Review Enquiry
• Start Date: 21-May-2008
• Completion Date: 21-May-2008
• Directive: 01/990 - Proposal for a EP and Council Decision establishing the list of priority substances in the field of water policy COM(2000)47 New version of 01/990: PE-CONS 3645/01 (2001-09-04) : PE and Council Decision on List of Priority Substances for WFD
• Directive: 2000/60/EC - Directive 2000/60/EC of the European Parliament and of the Council of 23 October 2000 establishing a framework for Community action in the field of water policy (substitutes Directive Reference 01/991 - Common Position on WFD)
• Directive: 2001/990 - Proposal for a EP and Council Decision establishing the list of priority substances in the field of water policy COM(2000)47 New version of 01/990: PE-CONS 3645/01 (2001-09-04) : PE and Council Decision on List of Priority Substances for WFD
• Directive: 98/83/EC - Quality of water intended for human consumption
• Ref Project: SIST EN ISO 17993:2004 - Water quality - Determination of 15 polycyclic aromatic hydrocarbons (PAH) in water by HPLC with fluorescence detection after liquid-liquid extraction (ISO 17993:2002)

Standards Content (Sample)

SLOVENSKI STANDARD
SIST EN ISO 17993:2004
01-februar-2004
.DNRYRVWYRGH±'RORþHYDQMHSROLFLNOLþQLKDURPDWVNLKRJOMLNRYRGLNRY3$+Y
YRGLVWHKQLNR+3/&VIOXRUHVFHQþQRGHWHNFLMRSRHNVWUDNFLMLWHNRþHWHNRþH,62

Water quality - Determination of 15 polycyclic aromatic hydrocarbons (PAH) in water by
HPLC with fluorescence detection after liquid-liquid extraction (ISO 17993:2002)
Wasserbeschaffenheit - Bestimmung von 15 polycyclischen aromatischen
Kohlenwasserstoffen (PAK) in Wasser durch HPLC mit Fluoreszenzdetektion nach
Flüssig-Flüssig-Extraktion (ISO 17993:2002)
Qualité de l'eau - Dosage de 15 hydrocarbures aromatiques polycycliques (HAP) dans
l'eau par HPLC avec détection par fluorescence apres extraction liquide-liquide (ISO
17993:2002)
Ta slovenski standard je istoveten z: EN ISO 17993:2003
ICS:
13.060.50 3UHLVNDYDYRGHQDNHPLþQH Examination of water for
VQRYL chemical substances
SIST EN ISO 17993:2004 en
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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EUROPEAN STANDARD
EN ISO 17993
NORME EUROPÉENNE
EUROPÄISCHE NORM
November 2003
ICS 13.060.50
English version
Water quality - Determination of 15 polycyclic aromatic
hydrocarbons (PAH) in water by HPLC with fluorescence
detection after liquid-liquid extraction (ISO 17993:2002)
Qualité de l'eau - Dosage de 15 hydrocarbures aromatiques Wasserbeschaffenheit - Bestimmung von 15 polycyclischen
polycycliques (HAP) dans l'eau par HPLC avec détection aromatischen Kohlenwasserstoffen (PAK) in Wasser durch
par fluorescence après extraction liquide-liquide (ISO HPLC mit Fluoreszenzdetektion nach Flüssig-Flüssig-
17993:2002) Extraktion (ISO 17993:2002)
This European Standard was approved by CEN on 3 November 2003.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European
Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national
standards may be obtained on application to the Management Centre or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation
under the responsibility of a CEN member into its own language and notified to the Management Centre has the same status as the official
versions.
CEN members are the national standards bodies of Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece,
Hungary, Iceland, Ireland, Italy, Luxembourg, Malta, Netherlands, Norway, Portugal, Slovakia, Spain, Sweden, Switzerland and United
Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
Management Centre: rue de Stassart, 36  B-1050 Brussels
© 2003 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 17993:2003 E
worldwide for CEN national Members.

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EN ISO 17993:2003 (E)
Foreword
The text of ISO 17993:2002 has been prepared by Technical Committee ISO/TC 147 "Water
quality” of the International Organization for Standardization (ISO) and has been taken over as
EN ISO 17993:2003 by Technical Committee CEN/TC 230 "Water analysis", the secretariat of
which is held by DIN.
This European Standard shall be given the status of a national standard, either by publication of
an identical text or by endorsement, at the latest by May 2004, and conflicting national standards
shall be withdrawn at the latest by May 2004.
According to the CEN/CENELEC Internal Regulations, the national standards organizations of
the following countries are bound to implement this European Standard: Austria, Belgium, Czech
Republic, Denmark, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy,
Luxembourg, Malta, Netherlands, Norway, Portugal, Slovakia, Spain, Sweden, Switzerland and
the United Kingdom.
Endorsement notice
The text of ISO 17993:2002 has been approved by CEN as EN ISO 17993:2003 without any
modifications.
NOTE Normative references to International Standards are listed in Annex ZA (normative).
2

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EN ISO 17993:2003 (E)
Annex ZA
(normative)
Normative references to international publications
with their relevant European publications
This European Standard incorporates by dated or undated reference, provisions from other
publications. These normative references are cited at the appropriate places in the text and the
publications are listed hereafter. For dated references, subsequent amendments to or revisions of
any of these publications apply to this European Standard only when incorporated in it by
amendment or revision. For undated references the latest edition of the publication referred to
applies (including amendments).
NOTE Where an International Publication h
...