EN 14185-1:2003

Non-fatty food - Determination of N-methylcarbamate residues - Part 1: HPLC-method with SPE clean-up

This En describes a method for the determination of N-methyl-carbamate residues in foodstuffs.

Fettarme Lebensmittel - Bestimmung von N-Methylcarbamat-Rückständen - Teil 1: HPLC-Verfahren mit Reinigung durch Festphasenextraktion

Aliments non gras - Dosages des N-méthylcarbamates - Partie 1: Méthode CLHP avec purification par SPE

Le présent projet de norme européenne spécifie une méthode par chromatographie liquide haute performance (CLHP) pour la détermination des produits phytosanitaires de la famille des N-méthylcarbamates présents dans les céréales, les fruits et les végétaux.
La méthode a été validée par une étude inter-laboratoires du carbaryl, carbofuran, méthiocarbe, méthomyl, oxamyl et des composés parents du propoxur ainsi que du méthiocarbe sulphoxyde présent dans les poivrons verts et dans les pommes à des niveaux se situant entre 0,08 et 0,9 mg/kg.
On ne dispose d'aucunes données inter-laboratoires concernant l'efficacité de la méthode pour la détermination d'autres métabolites importants ; on sait toutefois que la méthode ne convient pas pour les oximes de l'oxamyl et du méthomyl.

Hrana, ki ne vsebuje maščobe - Določevanje ostankov N-metil karbamata - 1. del: Metoda HPLC s čiščenjem SPE

General Information

• Status: Withdrawn
• Publication Date: 22-Apr-2003
• Withdrawal Date: 19-Nov-2019
• ICS: 67.060 - Cereals, pulses and derived products
• ICS: 67.080.01 - Fruits, vegetables and derived products in general
• Technical Committee: CEN/TC 275 - Food analysis - Horizontal methods
• Drafting Committee: CEN/TC 275/WG 3 - Pesticides and PCB's in foods of animal origin
• Current Stage: 9960 - Withdrawal effective - Withdrawal
• Completion Date: 20-Nov-2019
• Ref Project: SIST EN 14185-1:2003 - Non-fatty food - Determination of N-methylcarbamate residues - Part 1: HPLC-method with SPE clean-up

Standards Content (Sample)

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Fettarme Lebensmittel - Bestimmung von N-Methylcarbamat-Rückständen - Teil 1: HPLC-Verfahren mit Reinigung durch FestphasenextraktionAliments non gras - Dosages des N-méthylcarbamates - Partie 1: Méthode CLHP avec purification par SPENon-fatty food - Determination of N-methylcarbamate residues - Part 1: HPLC-method with SPE clean-up67.050Splošne preskusne in analizne metode za živilske proizvodeGeneral methods of tests and analysis for food productsICS:Ta slovenski standard je istoveten z:EN 14185-1:2003SIST EN 14185-1:2003en01-november-2003SIST EN 14185-1:2003SLOVENSKI
STANDARD
EUROPEAN STANDARDNORME EUROPÉENNEEUROPÄISCHE NORMEN 14185-1April 2003ICS 67.060; 67.080.01English versionNon-fatty food - Determination of N-methylcarbamate residues -Part 1: HPLC-method with SPE clean-upAliments non gras - Dosages des résidus de N-méthylcarbamates - Partie 1: Méthode par CLHP avecpurification SPEFettarme Lebensmittel - Bestimmung von N-Methylcarbamat-Rückständen - Teil 1: HPLC-Verfahren mitReinigung durch FestphasenextraktionThis European Standard was approved by CEN on 20 February 2003.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained on application to the Management Centre or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its own language and notified to the Management Centre has the same status as the officialversions.CEN members are the national standards bodies of Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece,Hungary, Iceland, Ireland, Italy, Luxembourg, Malta, Netherlands, Norway, Portugal, Slovakia, Spain, Sweden, Switzerland and UnitedKingdom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMITÉ EUROPÉEN DE NORMALISATIONEUROPÄISCHES KOMITEE FÜR NORMUNGManagement Centre: rue de Stassart, 36
B-1050 Brussels© 2003 CENAll rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN 14185-1:2003 ESIST EN 14185-1:2003

Precision Data.11Annex B (informative)
Alternative HPLC operating conditions.15Bibliography.16SIST EN 14185-1:2003

1)Bond-Elut® is a trade name of a product supplied by Analytichem International, Harbor City, CA, USA. LiChroCARTÒ andSuperspherÒ are trade names of products supplied by Merck, Darmstadt, Germany. Aminex® is a trade name of a productsupplied by Bio-Rad, Hercules, CA, USA. These informations are given for the convenience of users of this European Standardand do not constitute an endorsement by CEN of the products named. Equivalent products may be used if they can be shown tolead to the same results.SIST EN 14185-1:2003
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