SIST EN 17813:2024
(Main)Environmental solid matrices - Determination of halogens and sulfur by oxidative pyrohydrolytic combustion followed by ion chromatography
Environmental solid matrices - Determination of halogens and sulfur by oxidative pyrohydrolytic combustion followed by ion chromatography
This European Standard specifies a method for the direct determination total fluorine, chlorine, bromine and sulfur content in environmental solid matrices. The method is applicable for the determination of concentrations ≥ 10 mg/kg of each element based on dry matter. The upper limit and exact concentration range covered depends on system blank levels of instrumentation and capacity of the chromatographic separation column used for determination.
Feststoffe in der Umwelt - Bestimmung von Halogenen und Schwefel durch oxidative pyrohydrolytische Verbrennung, gefolgt von Ionenchromatographie
Dieses Dokument legt ein Verfahren für die gleichzeitige direkte Bestimmung des Gesamtgehalts an Fluor, Chlor, Brom und Schwefel in Feststoffen in der Umwelt fest. Das Verfahren gilt für die Bestimmung von Konzentrationen jedes Elements von ≥ 10 mg/kg, bezogen auf die Trockenmasse. Die Höchstgrenze und der exakte Konzentrationsbereich, der abgedeckt wird, hängen von den Blindwerten der Geräte und der Kapazität der für die Bestimmung verwendeten chromatographischen Trennsäule ab.
ANMERKUNG Die gleichzeitige Bestimmung des Gesamtjodgehalts ist möglich, aber derzeit nicht validiert.
Matrices environnementales solides - Méthode de dosage des halogènes et du soufre par combustion pyrohydrolytique oxydative suivie d’une analyse par chromatographie ionique
Le présent document spécifie une méthode de dosage, directe et simultanée, du fluor total, chlore total, brome total et soufre total dans des matrices environnementales solides. Cette méthode s’applique à la détermination, pour chaque élément, de concentrations supérieures ou égales à 10 mg/kg, en masse de matière sèche. La limite supérieure et la plage de concentration exacte couverte dépendent des niveaux de blanc des appareils et de la capacité de la colonne de séparation chromatographique utilisée pour le dosage.
NOTE Le dosage simultané de l’iode total est possible, mais non validé à l’heure actuelle.
Trdni matriksi v okolju - Določanje halogenov in žvepla z ionsko kromatografijo po oksidativnem pirohidrolitskem sežigu
General Information
Standards Content (Sample)
SLOVENSKI STANDARD
oSIST prEN 17813:2022
01-januar-2022
Matriksi z vidika okolja - Določevanje halogenov in žvepla z ionsko kromatografijo
ali komplementarnimi/dopolnilnimi metodami po pirohidrolitskem sežigu
Environmental matrices - Halogens and sulfur by oxidative pyrohydrolytic combustion
followed by ion chromatography detection and complementary determination methods
Umweltbezogene Charakterisierung fester Matrices - Halogene und Schwefel durch
oxidative pyrohydrolytische Verbrennung, gefolgt von ionenchromatographischer
Detektion und komplementären Bestimmungsmethoden
Ta slovenski standard je istoveten z: prEN 17813
ICS:
71.040.40 Kemijska analiza Chemical analysis
71.040.50 Fizikalnokemijske analitske Physicochemical methods of
metode analysis
oSIST prEN 17813:2022 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.
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oSIST prEN 17813:2022
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oSIST prEN 17813:2022
DRAFT
EUROPEAN STANDARD
prEN 17813
NORME EUROPÉENNE
EUROPÄISCHE NORM
January 2022
ICS 71.040.40; 71.040.50
English Version
Environmental matrices - Halogens and sulfur by oxidative
pyrohydrolytic combustion followed by ion
chromatography detection and complementary
determination methods
This draft European Standard is submitted to CEN members for enquiry. It has been drawn up by the Technical Committee
CEN/TC 444.
If this draft becomes a European Standard, CEN members are bound to comply with the CEN/CENELEC Internal Regulations
which stipulate the conditions for giving this European Standard the status of a national standard without any alteration.
This draft European Standard was established by CEN in three official versions (English, French, German). A version in any other
language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC
Management Centre has the same status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and
United Kingdom.
Recipients of this draft are invited to submit, with their comments, notification of any relevant patent rights of which they are
aware and to provide supporting documentation.
Warning : This document is not a European Standard. It is distributed for review and comments. It is subject to change without
notice and shall not be referred to as a European Standard.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2022 CEN All rights of exploitation in any form and by any means reserved Ref. No. prEN 17813:2022 E
worldwide for CEN national Members.
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oSIST prEN 17813:2022
prEN 17813:2022 (E)
Contents Page
European foreword . 4
1 Scope . 5
2 Normative references . 5
3 Terms and definitions . 5
4 Principle . 5
5 Interferences . 5
5.1 Interferences during combustion . 5
5.2 Interferences during absorption . 6
5.3 Interferences during ion chromatography . 6
6 Reagents and gases. 6
6.1 General. 6
6.2 Reagents fo
...
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