ASTM E2554-13
(Practice)Standard Practice for Estimating and Monitoring the Uncertainty of Test Results of a Test Method Using Control Chart Techniques
Standard Practice for Estimating and Monitoring the Uncertainty of Test Results of a Test Method Using Control Chart Techniques
SIGNIFICANCE AND USE
4.1 This practice provides one way for a laboratory to develop data-based Type A estimates of uncertainty as referred to in Section A22 in Form and Style of ASTM Standards.
4.2 Laboratories accredited under ISO/IEC 17025 are required to present uncertainty estimates for their test results. This practice provides procedures that use test results to develop uncertainty estimates for an individual laboratory.
4.3 Generally, these test results will be from a single sample of stable and homogeneous material known as a control or check sample.
4.4 The true value of the characteristic(s) of the control sample being measured will ordinarily be unknown. However, this methodology may also be used if the control sample is a reference material, in which case the test method bias may also be estimated and incorporated into the uncertainty estimate. Many test methods do not have true reference materials available to provide traceable chains of uncertainty estimation.
4.5 This practice also allows for ongoing monitoring of the laboratory uncertainty. As estimates of the level of uncertainty change, possibly as contributions to uncertainty are identified and minimized, revision to the laboratory uncertainty will be possible.
SCOPE
1.1 This practice describes techniques for a laboratory to estimate the uncertainty of a test result using data from test results on a control sample. This standard provides one method for a laboratory to estimate Measurement Uncertainty in accordance with Section A22.3 in Form and Style of ASTM Standards.
1.2 Uncertainty as defined by this practice applies to the capabilities of a single laboratory. Any estimate of uncertainty determined through the use of this practice applies only to the individual laboratory for which the data are presented.
1.3 The laboratory uses a well defined and established test method in determining a series of test results. The uncertainty estimated using this practice only applies when the same test method is followed. The uncertainty only applies for the material types represented by the control samples, and multiple control samples may be needed, especially if the method has different precision for different sample types or response levels.
1.4 The uncertainty estimate determined by this practice represents the intermediate precision of test results. This estimate seeks to quantify the total variation expected within a single laboratory using a single established test method while incorporating as many known sources of variation as possible.
1.5 This practice does not establish error estimates (error budget) attributed to individual factors that could influence uncertainty.
1.6 This practice describes the use of control charts to evaluate the data obtained and presents a special type of control chart to monitor the estimate of uncertainty.
1.7 The system of units for this standard is not specified. Dimensional quantities in the standard are presented only as illustrations of calculation methods. The examples are not binding on products or test methods treated.
1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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Designation: E2554 − 13 An American National Standard
Standard Practice for
Estimating and Monitoring the Uncertainty of Test Results
1
of a Test Method Using Control Chart Techniques
This standard is issued under the fixed designation E2554; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 1.8 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the
1.1 This practice describes techniques for a laboratory to
responsibility of the user of this standard to establish appro-
estimate the uncertainty of a test result using data from test
priate safety and health practices and determine the applica-
results on a control sample.This standard provides one method
bility of regulatory limitations prior to use.
for a laboratory to estimate Measurement Uncertainty in
1.9 This international standard was developed in accor-
accordance with Section A22.3 in Form and Style of ASTM
dance with internationally recognized principles on standard-
Standards.
ization established in the Decision on Principles for the
1.2 Uncertainty as defined by this practice applies to the
Development of International Standards, Guides and Recom-
capabilities of a single laboratory.Any estimate of uncertainty
mendations issued by the World Trade Organization Technical
determined through the use of this practice applies only to the
Barriers to Trade (TBT) Committee.
individual laboratory for which the data are presented.
2. Referenced Documents
1.3 The laboratory uses a well defined and established test
2
2.1 ASTM Standards:
method in determining a series of test results. The uncertainty
D5184 Test Methods for Determination of Aluminum and
estimated using this practice only applies when the same test
Silicon in Fuel Oils by Ashing, Fusion, Inductively
method is followed. The uncertainty only applies for the
Coupled Plasma Atomic Emission Spectrometry, and
materialtypesrepresentedbythecontrolsamples,andmultiple
Atomic Absorption Spectrometry
control samples may be needed, especially if the method has
E177 Practice for Use of the Terms Precision and Bias in
differentprecisionfordifferentsampletypesorresponselevels.
ASTM Test Methods
1.4 The uncertainty estimate determined by this practice
E456 Terminology Relating to Quality and Statistics
represents the intermediate precision of test results. This
E2282 Guide for Defining the Test Result of a Test Method
estimate seeks to quantify the total variation expected within a
E2587 Practice for Use of Control Charts in Statistical
single laboratory using a single established test method while
Process Control
incorporating as many known sources of variation as possible.
ISO/ASTM 51707 Guide for Estimating Uncertainties in
1.5 This practice does not establish error estimates (error Dosimetry for Radiation Processing
2
budget) attributed to individual factors that could influence 2.2 ASTM Publications:
uncertainty. Form and Style for ASTM Standards
Manual on Presentation of Data and Control Chart Analy-
1.6 This practice describes the use of control charts to
sis 7th Edition
evaluatethedataobtainedandpresentsaspecialtypeofcontrol
3
2.3 ISO Standard:
chart to monitor the estimate of uncertainty.
ISO/IEC 17025 General Requirements for the Competence
1.7 The system of units for this standard is not specified.
of Testing and Calibration Laboratories
Dimensional quantities in the standard are presented only as
3. Terminology
illustrations of calculation methods. The examples are not
binding on products or test methods treated.
3.1 Definitions—The terminology of Terminology E456
applies to this practice except as modified herein.
1 2
This practice is under the jurisdiction ofASTM Committee E11 on Quality and For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Statistics and is the direct responsibility of Subcommittee E11.20 on Test Method contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Evaluation and Quality Control. Standards volume information, refer to the standard’s Document Summary page on
Current edition approved April 1, 2013. Published May 2013. Originally the ASTM website.
3
approved in 2007. Last previous edition approved in 2007 as E2554 – 07. DOI: Available fromAmerican National Standards Institute (ANSI), 25 W. 43rd St.,
10.1520/E2554-13. 4th Floor, New York, NY 10036, http://www.ansi.org.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
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E2554 − 13
3.1.1 control sa
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This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: E2554 − 07 E2554 − 13 An American National Standard
Standard Practice for
Estimating and Monitoring the Uncertainty of Test Results
of a Test Method in a Single Laboratory Using a Control
1
Sample ProgramUsing Control Chart Techniques
This standard is issued under the fixed designation E2554; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This practice describes techniques for a laboratory to estimate the uncertainty of a test result using data from test results on
a control sample. This standard provides one method for a laboratory to estimate Measurement Uncertainty in accordance with
Section A22.3 in Form and Style of ASTM Standards.
1.2 Uncertainty as defined by this practice applies to the capabilities of a single laboratory. Any estimate of uncertainty
determined through the use of this practice applies only to the individual laboratory for which the data are presented.
1.3 The laboratory uses a well defined and established test method in determining a series of test results. The uncertainty
estimated using this practice only applies when the same test method is followed. The uncertainty only applies for the material
types represented by the control samples, and multiple control samples may be needed, especially if the method has different
precision for different sample types or response levels.
1.4 The uncertainty estimate determined by this practice represents the intermediate precision of test results. This estimate seeks
to quantify the total variation expected within a single laboratory using a single established test method while incorporating as
many known sources of variation as possible.
1.5 This practice does not establish error estimates (error budget) attributed to individual factors that could influence
uncertainty.
1.6 This practice describes the use of control charts to evaluate the data obtained and presents a special type of control chart
to monitor the estimate of uncertainty.
1.7 The system of units for this Standardstandard is not specified. Dimensional quantities in the Standardstandard are presented
only as illustrations of calculation methods. The examples are not binding on products or test methods treated.
1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
D5184 Test Methods for Determination of Aluminum and Silicon in Fuel Oils by Ashing, Fusion, Inductively Coupled Plasma
Atomic Emission Spectrometry, and Atomic Absorption Spectrometry
E177 Practice for Use of the Terms Precision and Bias in ASTM Test Methods
E456 Terminology Relating to Quality and Statistics
51707 Guide for Estimating Uncertainties in Dosimetry for Radiation Processing
E2282 Guide for Defining the Test Result of a Test Method
E2587 Practice for Use of Control Charts in Statistical Process Control
ISO/ASTM 51707 Guide for Estimating Uncertainties in Dosimetry for Radiation Processing
1
This practice is under the jurisdiction of ASTM Committee E11 on Quality and Statistics and is the direct responsibility of Subcommittee E11.20 on Test Method
Evaluation and Quality Control.
Current edition approved May 1, 2007April 1, 2013. Published June 2007May 2013. Originally approved in 2007. Last previous edition approved in 2007 as E2554 –
07. DOI: 10.1520/E2554-07.10.1520/E2554-13.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
E2554 − 13
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2.2 ASTM Publication:Publications:
Form and Style for ASTM Standards
Manual on Presentation of Data and Control Chart Analysis,Analysis 7th Edition
3
2.3 ISO Standard:
ISOISO/IEC 17025 General Requirements for the Competence of Testing and Calibration Laboratories
3. Terminology
3.1 Definitions:Definitions
3.1.1 The terminology of Term
...
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