EN ISO 638-1:2021

Paper, board, pulps and cellulosic nanomaterials - Determination of dry matter content by oven-drying method - Part 1: Materials in solid form (ISO 638-1:2021)

This document specifies an oven-drying method for the determination of the dry matter content in paper, board, pulp and cellulosic nanomaterials in solid form, which all can be produced from virgin and /or recycled materials.
It is also applicable to the determination of the dry matter content of paper and board for recycling.
The procedure is applicable to paper, board, and pulp and cellulosic nanomaterials which do not contain any appreciable quantities of materials other than water that are volatile at the temperature of 105 °C ± 2 °C. It is used, for example, in the case of pulp, paper, and board and cellulosic nanomaterial samples taken for chemical and physical tests in the laboratory, when a concurrent determination of dry matter content is required.
This method is not applicable to the determination of the dry matter content of slush pulp or to the determination of the saleable mass of pulp lots.
NOTE 1: ISO 638-2[1] specifies an oven-drying method for the determination of the dry matter content of suspensions of cellulosic nanomaterials, ISO 287[2] specifies the determination of the moisture content of a lot of paper and board; ISO 4119[3] specifies the determination of stock concentration of pulps; ISO 801 (all parts)[4] specifies the determination of the saleable mass in lots.
NOTE 2: This document determines the total dry matter content of the sample, including any dissolved solids. If only the cellulosic material content free of dissolved solids is desired, dissolved solids are removed prior to measuring the dry matter content e.g. by washing or dialysis, taking care to retain all cellulosic material; in cases where the sample is filterable without loss of cellulosic solids, ISO 4119[3] can be used to determine the stock consistency (content of cellulosic material in solid form)

Papier, Pappe, Faserstoff und cellulosehaltige Nanomaterialien - Bestimmung des Trockengehaltes durch das Wärmeschrankverfahren - Teil 1: Materialien in fester Form (ISO 638-1:2021)

Dieses Dokument legt ein Wärmeschrankverfahren für die Bestimmung des Trockengehaltes von Papier, Pappe, Faserstoff und cellulosehaltigen Nanomaterialien in fester Form fest, die jeweils aus Neumaterial und/oder recyceltem Material hergestellt werden können.
Es ist zudem anzuwenden für die Bestimmung des Trockengehaltes von Papier und Pappe für das Recycling.
Das Verfahren ist anzuwenden für Papier, Pappe und Faserstoff sowie cellulosehaltige Nanomaterialien, die außer Wasser keine nennenswerten Mengen von Materialien enthalten, die bei einer Temperatur von 105 °C ± 2 °C flüchtig sind. Es wird z. B. im Fall von Faserstoff-, Papier- und Pappe Durchschnittsproben sowie Durchschnittsproben von cellulosehaltigen Nanomaterialien verwendet, die für chemische und physikalische Prüfungen im Laboratorium entnommen werden, wenn eine gleichzeitige Bestimmung des Trockengehaltes erforderlich ist.
Dieses Verfahren ist nicht anzuwenden für die Bestimmung des Trockengehaltes von Faserstoff Suspensionen oder für die Bestimmung der verkaufsfähigen Masse von Faserstoff Lieferposten.
ANMERKUNG 1 ISO 638 2 [1] legt ein Wärmeschrankverfahren für die Bestimmung des Trockengehaltes von Suspensionen von cellulosehaltigen Nanomaterialien fest; ISO 287 [2] legt die Bestimmung des Feuchtegehaltes in einem Lieferposten Papier oder Pappe fest; ISO 4119 [3] legt die Bestimmung der Stoffdichte von Faserstoffen fest; ISO 801 (alle Teile) [4] legt die Bestimmung der verkaufsfähigen Masse in Lieferposten fest.
ANMERKUNG 2 Dieses Dokument dient der Bestimmung des Gesamttrockengehaltes der Durchschnittsprobe einschließlich jeglicher gelöster Feststoffe. Wird nur der Gehalt an cellulosehaltigem Material ohne die gelösten Feststoffe gewünscht, werden gelöste Feststoffe vor der Messung des Trockengehaltes z. B. durch Waschen oder Dialyse entfernt, wobei darauf geachtet wird, dass das gesamte cellulosehaltige Material erhalten bleibt; in Fällen, in denen die Durchschnittsprobe ohne Verlust von cellulosehaltigen Feststoffen gefiltert werden kann, kann ISO 4119 [3] angewendet werden, um die Stoffdichte (Gehalt an cellulosehaltigem Material in fester Form) zu bestimmen.

Papiers, cartons, pâtes et nanomatériaux cellulosiques - Détermination de la teneur en matières sèches par séchage à l'étuve - Partie 1: Matériaux sous forme solide (ISO 638-1:2021)

Le présent document spécifie une méthode de séchage à l’étuve pour la détermination de la teneur en matières sèches dans le papier, le carton, la pâte et les nanomatériaux cellulosiques sous forme solide, tous pouvant être produits à partir de matériaux vierges et/ou recyclés.
Elle est aussi applicable pour la détermination de la teneur en matières sèches du papier et du carton à recycler.
La méthode est applicable au papier, au carton, à la pâte et aux nanomatériaux cellulosiques ne contenant pas des quantités appréciables de matières autres que l’eau volatiles à la température de 105 °C ± 2 °C. Elle est utilisée, par exemple, dans le cas d’échantillons de pâte, de papier, de carton et de nanomatériaux cellulosiques prélevés en vue d’analyses chimiques et physiques effectuées en laboratoire lorsqu’il faut procéder à une détermination simultanée de la teneur en matières sèches.
Cette méthode n’est pas applicable pour la détermination de la teneur en matières sèches d’une suspension de pâte, ni pour la détermination de la masse marchande de lots de pâte.
NOTE 1   L’ISO 638-2[1] spécifie une méthode de séchage à l’étuve pour la détermination de la teneur en matières sèches dans des suspensions de nanomatériaux cellulosiques, l’ISO 287[2] spécifie la méthode de détermination de la teneur en humidité d’un lot de papier et carton, l’ISO 4119[3] spécifie la méthode de détermination de la concentration en pâte de suspensions aqueuses de pâtes, l’ISO 801 (toutes les parties)[4] spécifie la méthode de détermination de la masse marchande de lots.
NOTE 2   Le présent document permet de déterminer la teneur totale en matières sèches d’un échantillon, y compris tout solide dissous. Pour obtenir la teneur en matériaux cellulosiques sans solides dissous, ces derniers sont éliminés avant de mesurer la teneur en matières sèches, par exemple par lavage ou dialyse, en prenant soin de conserver l’ensemble des matériaux cellulosiques. Lorsque l’échantillon peut être filtré sans perte de solides cellulosiques, l’ISO 4119[3] peut être utilisée pour déterminer la concentration en pâte (teneur en matériaux cellulosiques sous forme solide).

Papir, karton, lepenka in vlaknine ter celulozni nanomateriali - Določevanje suhe snovi - Metoda sušenja v sušilniku - 1. del: Materiali v trdni obliki (ISO 638-1:2021)

General Information

• Status: Withdrawn
• Publication Date: 18-May-2021
• Withdrawal Date: 05-Apr-2022
• ICS: 85.040 - Pulps
• ICS: 85.060 - Paper and board
• Technical Committee: CEN/TC 172 - Pulp, paper and board
• Drafting Committee: CEN/TC 172 - Pulp, paper and board
• Current Stage: 9960 - Withdrawal effective - Withdrawal
• Completion Date: 06-Apr-2022
• Ref Project: SIST EN ISO 638-1:2021 - Paper, board, pulps and cellulosic nanomaterials - Determination of dry matter content by oven-drying method - Part 1: Materials in solid form (ISO 638-1:2021)

Relations

• Replaces: EN ISO 638:2008 - Paper, board and pulps - Determination of dry matter content - Oven-drying method (ISO 638:2008)
• Effective Date: 08-Jun-2022
• Replaced By: EN ISO 638-1:2022 - Paper, board, pulps and cellulosic nanomaterials - Determination of dry matter content by oven-drying method - Part 1: Materials in solid form (ISO 638-1:2022)
• Effective Date: 01-Sep-2021

Standards Content (Sample)

SLOVENSKI STANDARD
01-september-2021
Nadomešča:
SIST EN ISO 638:2009
Papir, karton, lepenka in vlaknine ter celulozni nanomateriali - Določevanje suhe
snovi - Metoda sušenja v sušilniku - 1. del: Materiali v trdni obliki (ISO 638-1:2021)
Paper, board, pulps and cellulosic nanomaterials - Determination of dry matter content
by oven-drying method - Part 1: Materials in solid form (ISO 638-1:2021)
Papier, Pappe, Faserstoff und cellulosehaltige Nanomaterialien - Bestimmung des
Trockengehaltes - Wärmeschrankverfahren - Teil 1: Materialien in fester Form (ISO 638-
1:2021)
Papiers, cartons, pâtes et nanomatériaux cellulosiques - Détermination de la teneur en
matières sèches par séchage à l'étuve - Partie 1: Matériaux sous forme solide (ISO 638-
1:2021)
Ta slovenski standard je istoveten z: EN ISO 638-1:2021
ICS:
85.040 Vlaknine Pulps
85.060 Papir, karton in lepenka Paper and board
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

EN ISO 638-1
EUROPEAN STANDARD
NORME EUROPÉENNE
May 2021
EUROPÄISCHE NORM
ICS 85.040; 85.060 Supersedes EN ISO 638:2008
English Version
Paper, board, pulps and cellulosic nanomaterials -
Determination of dry matter content by oven-drying
method - Part 1: Materials in solid form (ISO 638-1:2021)
Papiers, cartons, pâtes et nanomatériaux cellulosiques Papier, Pappe, Faserstoff und cellulosehaltige
- Détermination de la teneur en matières sèches par Nanomaterialien - Bestimmung des Trockengehaltes -
séchage à l'étuve - Partie 1: Matériaux sous forme Wärmeschrankverfahren - Teil 1: Materialien in fester
solide (ISO 638-1:2021) Form (ISO 638-1:2021)
This European Standard was approved by CEN on 6 May 2021.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and
United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2021 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 638-1:2021 E
worldwide for CEN national Members.

Contents Page
European foreword . 3

European foreword
This document (EN ISO 638-1:2021) has been prepared by Technical Committee ISO/TC 6 "Paper,
board and pulps" in collaboration with Technical Committee CEN/TC 172 “Pulp, paper and board” the
secretariat of which is held by DIN.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by November 2021, and conflicting national standards
shall be withdrawn at the latest by November 2021.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
This document supersedes EN ISO 638:2008.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland,
Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Republic of
North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the
United Kingdom.
Endorsement notice
The text of ISO 638-1:2021 has been approved by CEN as EN ISO 638-1:2021 without any modification.

INTERNATIONAL ISO
STANDARD 638-1
First edition
2021-05
Paper, board, pulps and cellulosic
nanomaterials — Determination of
dry matter content by oven-drying
method —
Part 1:
Materials in solid form
Papiers, cartons, pâtes et nanomatériaux cellulosiques —
Détermination de la teneur en matières sèches par séchage à
l'étuve —
Partie 1: Matériaux sous forme solide
Reference number
ISO 638-1:2021(E)
©
ISO 2021
ISO 638-1:2021(E)
© ISO 2021
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting
on the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address
below or ISO’s member body in the country of the requester.
ISO copyright office
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Phone: [phone]
Email: [e-mail]
Website: www.iso.org
Published in Switzerland
ii © ISO 2021 – All rights reserved

ISO 638-1:2021(E)
Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Principle . 2
5 Apparatus . 3
6 Sampling . 3
7 Preparation of test pieces . 3
7.1 General . 3
7.2 Paper and board for recycling . 3
7.3 Paper, board, pulp and cellulosic nanomaterial in solid form . 3
8 Procedure. 4
9 Calculation and expression of results . 5
10 Precision . 5
11 Test report . 5
Annex A (informative) Calculation of the moisture content . 6
Annex B (informative) Precision . 7
Bibliography .10
ISO 638-1:2021(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.
ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular, the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see www .iso .org/ directives).
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of
any patent rights identified during the development of the document will be in the Introduction and/or
on the ISO list of patent declarations received (see www .iso .org/ patents).
Any trade name used in this document is information given for the convenience of users and does not
constitute an endorsement.
For an explanation on the meaning of ISO specific terms and expressions related to conformity
assessment, as well as information about ISO's adherence to the World Trade Organization (WTO)
principles in the Technical Barriers to Trade (TBT) see the following URL: www .iso .org/ iso/ foreword
.html.
This document was prepared by Technical Committee ISO/TC 6, Paper, board and pulps.
This first edition of ISO 638-1, together with ISO 638-2, cancels and replaces ISO 638:2008, which has
been technically revised. The main changes compared to the previous edition are as follows:
— inclusion of cellulosic nanomaterials and paper and board for recycling in the scope;
— splitting of the standard in two parts;
— technical revision of the procedure;
— editorial revision of the document;
— update of precision clause.
Any feedback or questions on this document should be directed to the user’s national standards body. A
complete listing of these bodies can be found at www .iso .org/ members .html.
iv © ISO 2021 – All rights reserved

ISO 638-1:2021(E)
Introduction
Determination of dry matter content and moisture content are carried out for different purposes.
This document is used when the dry matter content is needed to calculate the results for chemical
analysis or physical testing, or to determine the moisture content of paper, board, and pulp and cellulosic
nanomaterials in solid form, which all may be produced from virgin and/or recycled materials. An
example of this is where the results of a chemical analysis for cadmium or manganese are required on
the basis of the oven-dry mass of the sample.
[1]
ISO 638-2 is dedicated to the determination of the dry matter content or water content of cellulosic
nanomaterials in the form of suspensions.
[2]
ISO 287 should be used for the purpose of determining the average moisture content and the variation
in moisture content (maximum and minimum values) of a lot of paper and board. In the converting of
paper and board, moisture content is important as it can have an effect on processes such as printing
and copying. Moisture content can have an effect on curl and dimensional stability.
[3]
ISO 4119 should be used in laboratory procedures or is referred to in other International Standards
in which the concentration of an aqueous pulp suspension requires determination.
...