EN 16174:2012

Sludge, treated biowaste and soil - Digestion of aqua regia soluble fractions of elements

This European Standard specifies two methods for digestion of sludge, treated biowaste and soil by the use of aqua regia as digestion solution.
This European Standard is applicable for the following elements:
Aluminium (Al), antimony (Sb), arsenic (As), barium (Ba), beryllium (Be), bismuth (Bi), boron (B), cadmium (Cd), calcium (Ca), cerium (Ce), cesium (Cs), chromium (Cr), cobalt (Co), copper (Cu), dysprosium (Dy), erbium (Er), europium (Eu), gadolinium (Gd), gallium (Ga), germanium (Ge), gold (Au), hafnium (Hf), holmium (Ho), indium (In), iridium (Ir), iron (Fe), lanthanum (La), lead (Pb), lithium (Li), lutetium (Lu), magnesium (Mg), manganese (Mn), mercury (Hg), molybdenum (Mo), neodymium (Nd), nickel (Ni), palladium (Pd), phosphorus (P), platinum (Pt), potassium (K), praseodymium (Pr), rubidium (Rb), rhenium (Re), rhodium (Rh), ruthenium (Ru), samarium (Sm), scandium (Sc), selenium (Se), silicon (Si), silver (Ag), sodium (Na), strontium (Sr), sulphur (S), tellurium (Te), terbium (Tb), thallium (Tl), thorium (Th), thulium (Tm), tin (Sn), titanium (Ti), tungsten (W), uranium (U), vanadium (V), ytterbium (Yb), yttrium (Y), zinc (Zn), and zirconium (Zr).
This European Standard may also be applicable for the digestion of other elements.
Digestion with aqua regia will not necessarily accomplish total decomposition of the sample. The extracted analyte concentrations may not necessarily reflect the total content in the sample.

Schlamm, behandelter Bioabfall und Boden - Aufschluss von mit Königswasser löslichen Anteilen von Elementen

Diese Europäische Norm legt zwei Verfahren zum Aufschluss von Schlamm, behandeltem Bioabfall und Boden mit Königswasser als Aufschlusslösung fest.
Diese Europäische Norm ist auf folgende Elemente anwendbar:
Aluminium (Al), Antimon (Sb), Arsen (As), Barium (Ba), Beryllium (Be), Bismuth (Bi), Blei (Pb), Bor (B), Cadmium (Cd), Cäsium (Cs), Calcium (Ca), Cerium (Ce), Chrom (Cr), Cobalt (Co), Dysprosium (Dy), Eisen (Fe), Erbium (Er), Europium (Eu), Gadolinium (Gd), Gallium (Ga), Germanium (Ge), Gold (Au), Hafnium (Hf), Holmium (Ho), Indium (In), Iridium (Ir), Kalium (K), Kupfer (Cu), Lanthan (La), Lithium (Li), Lutetium (Lu), Magnesium (Mg), Mangan (Mn), Molybdän (Mo), Natrium (Na), Neodym (Nd), Nickel (Ni), Palladium (Pd), Phosphor (P), Platin (Pt), Praseodymium (Pr), Quecksilber (Hg), Rhenium (Re), Rhodium (Rh), Rubidium (Rb), Ruthenium (Ru), Samarium (Sm), Scandium (Sc), Schwefel (S), Selen (Se), Silicon (Si), Strontium (Sr), Tellur (Te), Terbium (Tb), Thallium (Tl), Thorium (Th), Thulium (Tm), Titan (Ti), Tungsten (W), Uran (U), Vanadium (V), Ytterbium (Yb), Yttrium (Y), Zinn (Sn), Zink (Zn), and Zirconium (Zr).
Diese Europäische Norm darf auch auf andere Elemente angewendet werden.
Beim Aufschluss mit Königswasser, der verfahrensbedingt festgelegt ist, werden nicht unbedingt alle Elemente vollständig aufgeschlossen.

Boues, biodéchets traités et sols - Digestion des éléments solubles dans l'eau régale

La présente Norme européenne spécifie deux méthodes de digestion des boues, des biodéchets traités et des sols avec de l'eau régale comme solution de digestion.
La présente Norme européenne est applicable aux éléments suivants :
Aluminium (Al), antimoine (Sb), arsenic (As), baryum (Ba), béryllium (Be), bismuth (Bi), bore (B), cadmium (Cd), calcium (Ca), cérium (Ce), césium (Cs), chrome (Cr), cobalt (Co), cuivre (Cu), dysprosium (Dy), erbium (Er), europium (Eu), gadolinium (Gd), gallium (Ga), germanium (Ge), or (Au), hafnium (Hf), holmium (Ho), indium (In), iridium (Ir), fer (Fe), lanthane (La), plomb (Pb), lithium (Li), lutétium (Lu), magnésium (Mg), manganèse (Mn), mercure (Hg), molybdène (Mo), néodyme (Nd), nickel (Ni), palladium (Pd), phosphore (P), platine (Pt), potassium (K), praséodyme (Pr), rubidium (Rb), rhénium (Re), rhodium (Rh), ruthénium (Ru), samarium (Sm), scandium (Sc), sélénium (Se), silicium (Si), argent (Ag), sodium (Na), strontium (Sr), soufre (S), tellure (Te), terbium (Tb), thallium (Tl), thorium (Th), thulium (Tm), étain (Sn), titane (Ti), tungstène (W), uranium (U), vanadium (V), ytterbium (Yb), yttrium (Y), zinc (Zn) et zirconium (Zr).
La présente Norme européenne peut également s'appliquer à la digestion d'autres éléments.
La digestion à l'eau régale n'aboutit pas nécessairement à une décomposition totale de l'échantillon. Les concentrations d'analytes extraits ne reflètent pas nécessairement les teneurs totales dans l'échantillon.

Blato, obdelani biološki odpadki in tla - Razklop v zlatotopki topnih frakcij elementov

Ta evropski standard določa pripravo blata, obdelanih bioloških odpadkov in tal (vključno z materiali, ki so podobni tlom), ki so obravnavani v analizi organskih in anorganskih kemijskih in fizikalno-kemijskih parametrov. Priprava vzorcev je namenjena pripravi (majhnega) preskusnega vzorca, ki je reprezentativen za izvorni vzorec. V tem evropskem standardu sta opisani priprava, ki se lahko po potrebi izvede na prostem, in priprava vzorca v laboratorijskih pogojih. V tem evropskem standardu so za določitev anorganskih kemijskih in fizikalno-kemijskih parametrov opisani postopki za pripravo: – preskusnih vzorcev za preskuse v vlažnih razmerah na prostem; – preskusnih vzorcev za preskušanje po sušenju, drobljenju, mletju, sejanju itd.; – preskusnih vzorcev tekočega blata. Za določanje organskih spojin so opredeljene tri metode priprave: – metoda priprave v primeru merjenja hlapnih organskih spojin; – metoda priprave, če se merijo slabo hlapne do nehlapne organske spojine, pri čemer bo rezultat naslednje analize natančen in ponovljiv; – metoda priprave, če se merijo slabo hlapne do nehlapne organske spojine in je za postopek ekstrakcije potreben vzorec vlage na prostem ali če so potrebni samo nakazalni rezultati. Izbira metode je odvisna predvsem od hlapnosti analita. Odvisna je tudi od razporeditve delcev po velikosti materiala, raznovrstnosti vzorca in naslednjega analiznega postopka.

General Information

• Status: Withdrawn
• Publication Date: 21-Aug-2012
• Withdrawal Date: 14-Sep-2021
• ICS: 13.030.01 - Wastes in general
• ICS: 13.080.10 - Chemical characteristics of soils
• Technical Committee: CEN/TC 444 - Environmental characterization
• Drafting Committee: CEN/TC 444/WG 3 - Inorganic analysis
• Current Stage: 9960 - Withdrawal effective - Withdrawal
• Completion Date: 15-Sep-2021
• Directive: 86/278/EEC - Protection of the environment, and in particular of the soil, when sewage sludge is used in agriculture
• Mandate: M/330 - Mandate given to CEN for the development of horizontal standards in the fields of sludge, biowaste and soil.
• Ref Project: SIST EN 16174:2013 - Sludge, treated biowaste and soil - Digestion of aqua regia soluble fractions of elements

Standards Content (Sample)

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Blato, obdelani biološki odpadki in tla - Razklop v zlatotopki topnih frakcij elementovSchlamm, behandelter Bioabfall und Boden - Aufschluss von mit Königswasser löslichen Anteilen von ElementenBoue, biodéchet traité et sol - Digestion des éléments solubles dans l'eau régaleSludge, treated biowaste and soil - Digestion of aqua regia soluble fractions of elements13.080.10Chemical characteristics of soils13.030.20Liquid wastes. SludgeICS:Ta slovenski standard je istoveten z:EN 16174:2012SIST EN 16174:2013en,fr,de01-februar-2013SIST EN 16174:2013SLOVENSKI
STANDARD



SIST EN 16174:2013



EUROPEAN STANDARD NORME EUROPÉENNE EUROPÄISCHE NORM
EN 16174
August 2012 ICS 13.030.01; 13.080.10 English Version
Sludge, treated biowaste and soil - Digestion of aqua regia soluble fractions of elements
Boues, biodéchets traités et sols - Digestion des éléments solubles dans l'eau régale
Schlamm, behandelter Bioabfall und Boden - Aufschluss von mit Königswasser löslichen Anteilen von Elementen This European Standard was approved by CEN on 24 May 2012.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION EUROPÄISCHES KOMITEE FÜR NORMUNG
Management Centre:
Avenue Marnix 17,
B-1000 Brussels © 2012 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN 16174:2012: ESIST EN 16174:2013



EN 16174:2012 (E) 2 Contents Page Foreword .3Introduction .41 Scope .52 Normative references .53 Terms and definitions .54 Principle .55 Interferences and sources of errors .66 Reagents .67 Apparatus .68 Procedure .88.1 General .88.2 Blank test .88.3 Method A: Thermal heating under reflux conditions .98.4 Method B: Microwave heating with temperature control at (175 ± 5) °C .99 Test report . 10Annex A (informative)
Repeatability and reproducibility data . 11A.1 Materials used i
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