EN 16173:2012

Sludge, treated biowaste and soil - Digestion of nitric acid soluble fractions of elements

This European Standard specifies a method for microwave digestion of sludge, treated biowaste and soil using nitric acid.
This method is applicable for microwave-assisted nitric acid digestion of sludge, treated biowaste and soils for the following elements:
Aluminium (Al), antimony (Sb), arsenic (As), barium (Ba), beryllium (Be), bismuth (Bi), boron (B), cadmium (Cd), calcium (Ca), cerium (Ce), cesium (Cs), chromium (Cr), cobalt (Co), copper (Cu), dysprosium (Dy), erbium (Er), europium (Eu), gadolinium (Gd), gallium (Ga), germanium (Ge), gold (Au), hafnium (Hf), holmium (Ho), indium (In), iridium (Ir), iron (Fe), lanthanum (La), lead (Pb), lithium (Li), lutetium (Lu), magnesium (Mg), manganese (Mn), mercury (Hg), molybdenum (Mo), neodymium (Nd), nickel (Ni), palladium (Pd), phosphorus (P), platinum (Pt), potassium (K), praseodymium (Pr), rubidium (Rb), rhenium (Re), rhodium (Rh), ruthenium (Ru), samarium (Sm), scandium (Sc), selenium (Se), silicon (Si), sodium (Na), strontium (Sr), sulphur (S), tellurium (Te), terbium (Tb), thallium (Tl), thorium (Th), thulium (Tm), tin (Sn), titanium (Ti), tungsten (W), uranium (U), vanadium (V), ytterbium (Yb), yttrium (Y), zinc (Zn), and zirconium (Zr).
This European Standard may also be applicable for the digestion of other elements.
Digestion with nitric acid will not necessarily accomplish total decomposition of the sample. The extracted analyte concentrations may not necessarily reflect the total content in the sample.

Schlamm, behandelter Bioabfall und Boden - Aufschluss von mit Salpetersäure löslichen Anteilen von Elementen

Diese Europäische Norm legt ein Verfahren für den Aufschluss von Schlamm, behandeltem Bioabfall und Boden mittels Mikrowellengerät und Salpetersäure fest.
Das hier beschriebene Verfahren ist für den Säureaufschluss von Bioabfall, Schlamm und Boden mittels Mikrowellengerät auf folgende Elemente anwendbar:
Aluminium (Al), Arsen (As), Barium (Ba), Beryllium (Be), Bismuth (Bi), Blei (Pb), Bor (B), Cadmium (Cd), Cäsium (Cs), Calcium (Ca), Cerium (Ce), Chrom (Cr), Cobalt (Co), Dysprosium (Dy), Eisen (Fe), Erbium (Er), Europium (Eu), Gadolinium (Gd), Gallium (Ga), Germanium (Ge), Gold (Au), Hafnium (Hf), Holmium (Ho), Indium (In), Iridium (Ir), Kalium (K), Kupfer (Cu), Lanthan (La), Lithium (Li), Lutetium (Lu), Magnesium (Mg), Mangan (Mn), Molybdän (Mo), Natrium (Na), Neodym (Nd), Nickel (Ni), Palladium (Pd), Phosphor (P), Platin (Pt), Praseodymium (Pr), Quecksilber (Hg), Rhenium (Re), Rhodium (Rh), Rubidium (Rb), Ruthenium (Ru), Samarium (Sm), Scandium (Sc), Schwefel (S), Selen (Se), Silicon (Si), Strontium (Sr), Tellur (Te), Terbium (Tb), Thallium (Tl), Thorium (Th), Thulium (Tm), Titan (Ti), Tungsten (W), Uran (U), Vanadium (V), Ytterbium (Yb), Yttrium (Y), Zink (Zn), and Zirconium (Zr).
Diese Europäische Norm darf auch für den Aufschluss anderer Elemente angewendet werden.
Der Aufschluss mit Salpetersäure führt nicht notwendigerweise zum vollständigen Abbau der Probe. Die extrahierten Konzentrationen der Analyten geben daher möglicherweise nicht den Gesamtgehalt in der Probe wieder.

Boues, biodéchets traités et sols - Digestion des éléments solubles dans l'acide nitrique

La présente Norme européenne spécifie une méthode de digestion par micro-ondes des boues, des biodéchets traités et des sols en utilisant de l'acide nitrique.
Cette méthode est applicable pour la digestion à l'acide nitrique assistée par micro-ondes des boues, des biodéchets traités et des sols pour les éléments suivants :
Aluminium (Al), antimoine (Sb), arsenic (As), baryum (Ba), béryllium (Be), bismuth (Bi), bore (B), cadmium (Cd), calcium (Ca), cérium (Ce), césium (Cs), chrome (Cr), cobalt (Co), cuivre (Cu), dysprosium (Dy), erbium (Er), europium (Eu), gadolinium (Gd), gallium (Ga), germanium (Ge), or (Au), hafnium (Hf), holmium (Ho), indium (In), iridium (Ir), fer (Fe), lanthane (La), plomb (Pb), lithium (Li), lutétium (Lu), magnésium (Mg), manganèse (Mn), mercure (Hg), molybdène (Mo), néodyme (Nd), nickel (Ni), palladium (Pd), phosphore (P), platine (Pt), potassium (K), praséodyme (Pr), rubidium (Rb), rhénium (Re), rhodium (Rh), ruthénium (Ru), samarium (Sm), scandium (Sc), sélénium (Se), silicium (Si), sodium (Na), strontium (Sr), soufre (S), tellure (Te), terbium (Tb), thallium (Tl), thorium (Th), thulium (Tm), étain (Sn), titane (Ti), tungstène (W), uranium (U), vanadium (V), ytterbium (Yb), yttrium (Y), zinc (Zn) et zirconium (Zr).
La présente Norme européenne peut également s'appliquer à la digestion d'autres éléments.
La digestion à l'acide nitrique n'aboutit pas nécessairement à une minéralisation totale de l'échantillon. Les concentrations en analytes extraits ne reflètent pas nécessairement la teneur totale dans l'échantillon.

Blato, obdelani biološki odpadki in tla - Razklop v dušikovi kislini topnih frakcij elementov

Ta evropski standard določa metodo za mikrovalovni razklop blata, bioloških odpadkov in tal z uporabo dušikove kisline. Ta metoda se uporablja za mikrovalovni razklop blata, obdelanih bioloških odpadkov in tal z dušikovo kislino za naslednje elemente: aluminij (Al), arzen (As), barij (Ba), berilij (Be), bizmut (Bi), bor (B), kadmij (Cd), kalcij (Ca), cerij (Ce), cezij (Cs), krom (Cr), kobalt (Co), baker (Cu), disprozij (Dy), erbij (Er), evropij (Eu), gadolinij (Gd), galij (Ga), germanij (Ge), zlato (Au), hafnij (Hf), holmij (Ho), indij (In), iridij (Ir), železo (Fe), lantan (La), svinec (Pb), litij (Li), lutecij (Lu), magnezij (Mg), mangan (Mn), živo srebro (Hg), molibden (Mo), neodim (Nd), nikelj (Ni), paladij (Pd), fosfor (P), platina (Pt), kalij (K), prazeodim (Pr), rubidij (Rb), renij (Re), rodij (Rh), rutenij (Ru), samarij (Sm), skandij (Sc), selen (Se), silicij (Si), natrij (Na), stroncij (Sr), žveplo (S), telurij (Te), terbij (Tb), talij (Tl), torij (Th), tulij (Tm), titan (Ti), volfram (W), uran (U), vanadij (V), iterbij (Yb), itrij (Y), cink (Zn) in cirkonij (Zr). Ta evropski standard se lahko uporablja tudi za razklop drugih elementov. Z razklopom z dušikovo kislino se ne doseže nujno popolna razgradnja vzorca. Iz ekstrahiranih koncentracij analita ni nujno razvidna skupna vsebina v vzorcu.

General Information

• Status: Published
• Publication Date: 21-Aug-2012
• ICS: 13.030.01 - Wastes in general
• ICS: 13.080.10 - Chemical characteristics of soils
• Technical Committee: CEN/TC 444 - Environmental characterization
• Drafting Committee: CEN/TC 444/WG 3 - Inorganic analysis
• Current Stage: 9060 - Closure of 2 Year Review Enquiry - Review Enquiry
• Start Date: 02-Dec-2023
• Completion Date: 02-Dec-2023
• Directive: 86/278/EEC - Protection of the environment, and in particular of the soil, when sewage sludge is used in agriculture
• Mandate: M/330 - Mandate given to CEN for the development of horizontal standards in the fields of sludge, biowaste and soil.
• Ref Project: SIST EN 16173:2013 - Sludge, treated biowaste and soil - Digestion of nitric acid soluble fractions of elements

Standards Content (Sample)

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Blato, obdelani biološki odpadki in tla - Razklop v dušikovi kislini topnih frakcij elementovSchlamm behandelter Bioabfall und Boden - Aufschluss von mit Salpetersäure löslichen Anteilen von ElementenBoue, biodéchet traité et sol - Digestion des éléments solubles dans l'acide nitriqueSludge, treated biowaste and soil - Digestion of nitric acid soluble fractions of elements13.080.10Chemical characteristics of soils13.030.20Liquid wastes. SludgeICS:Ta slovenski standard je istoveten z:EN 16173:2012SIST EN 16173:2013en,fr,de01-februar-2013SIST EN 16173:2013SLOVENSKI
STANDARD



SIST EN 16173:2013



EUROPEAN STANDARD NORME EUROPÉENNE EUROPÄISCHE NORM
EN 16173
August 2012 ICS 13.080.10; 13.030.01 English Version
Sludge, treated biowaste and soil - Digestion of nitric acid soluble fractions of elements
Boues, biodéchets traités et sols - Digestion des éléments solubles dans l'acide nitrique
Schlamm, behandelter Bioabfall und Boden - Aufschluss von mit Salpetersäure löslichen Anteilen von Elementen This European Standard was approved by CEN on 24 May 2012.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION EUROPÄISCHES KOMITEE FÜR NORMUNG
Management Centre:
Avenue Marnix 17,
B-1000 Brussels © 2012 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN 16173:2012: ESIST EN 16173:2013



EN 16173:2012 (E) 2 Contents Page Foreword .3Introduction .41 Scope .52 Normative references .53 Principle .54 Interferences and sources of errors .55 Reagents .66 Apparatus .67 Digestion procedure .78 Test report .8Annex A (informative)
Repeatability and reproducibility data .9A.1 Materials used in the interlaboratory comparison study .9A.2 Interlaboratory comparison results .9Bibliography . 11 SIST EN 16173:2013



EN 16173:2012 (E) 3 Foreword This document (EN 16173:2012) has been prepared by Technical Committee CEN/TC 400 “Project Committee - Horizontal standards in the fields of sludge, biowaste and soil”, the secretariat of which is held by DIN. This European Standard shal
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