iTeh StandardsiTeh Standards
EURUSD
Your shopping cart is empty.
CEN

EN 15522-2:2023/prA1

(Amendment)

Oil spill identification - Petroleum and petroleum related products - Part 2: Analytical method and interpretation of results based on GC-FID and GC-low resolution-MS analyses

Oil spill identification - Petroleum and petroleum related products - Part 2: Analytical method and interpretation of results based on GC-FID and GC-low resolution-MS analyses

This document specifies a method to identify and compare the compositional characteristics of oil samples. Specifically, it describes the detailed analytical and data processing methods for identifying the characteristics of spill samples and establishing their correlation to suspected source oils. Even when samples or data from suspected sources are not available for comparison, establishing the specific nature (e.g. refined petroleum, crude oil, waste oil, etc.) of the spilled oil still helps to constrain the possible source(s).
This methodology is restricted to petroleum related products containing a significant proportion of hydrocarbon-components with a boiling point above 150 °C. Examples are: crude oils, higher boiling condensates, diesel oils, residual bunker or heavy fuel oils, lubricants, and mixtures of bilge and sludge samples, as well as distillate fuels and blends. While the specific analytical methods are perhaps not appropriate for lower boiling oils (e.g. kerosene, jet fuel, or gasoline), the general concepts described in this methodology, i.e. statistical comparison of weathering-resistant diagnostic ratios, are applicable in spills involving these kinds of oils.
Paraffin based products (e.g. waxes, etc.) are outside the scope of this method because too many compounds are removed during the production process [37]. However, the method can be used to identify the type of product involved.
Although not directly intended for identifying oil recovered from groundwater, vegetation, wildlife/tissues, soil, or sediment matrices, they are not precluded. However, caution is needed as extractable compounds can be present in these matrices that alter and/or contribute additional compounds compared to the source sample. If unrecognized, the contribution from the matrix can lead to false “non-matches”. It is therefore advisable to analyse background sample(s) of the matrix that appear unoiled.
When analysing “non-oil” matrices additional sample preparation (e.g. clean-up) is often required prior to analysis and the extent to which the matrix affects the correlation achieved is to be considered. Whether the method is applicable for a specific matrix depends upon the oil concentration compared to the “matrix concentration”. In matrices containing high concentrations of oil, a positive match can still be concluded. In matrices containing lower concentrations of oil, a false “non-match” or an “inconclusive match” can result from matrix effects. Evaluation of possible matrix effects is beyond the scope of this document.

Identifizierung von Ölverschmutzungen - Rohöl und Mineralölerzeugnisse - Teil 2: Analytische Methodik und Interpretation der Ergebnisse, basierend auf GC-FID- und GC-MS-Analysen bei niedriger Auflösung

Identification des pollutions pétrolières - Pétrole et produits pétroliers - Partie 2 : Méthode d'analyse et interprétation des résultats sur la base des analyses par CPG-DIF et CPG-SM faible résolution

Prepoznavanje razlitij olj - Nafta in sorodni naftni proizvodi - 2. del: Analizne metode in podajanje rezultatov, izhajajočih iz GC-FID in GC-MS nizke ločljivosti

General Information

Status
Not Published
Publication Date
27-Nov-2025
ICS
13.020.40 - Pollution, pollution control and conservation
75.080 - Petroleum products in general
Technical Committee
CEN/TC 19 - Petroleum products, lubricants and related products
Drafting Committee
CEN/TC 19/WG 9 - Chromatographic test methods
Current Stage
4020 - Submission to enquiry - Enquiry
Start Date
21-Mar-2024
Due Date
12-Jul-2024
Completion Date
21-Mar-2024
Ref Project
SIST EN 15522-2:2023/oprA1:2024 - Oil spill identification - Petroleum and petroleum related products - Part 2: Analytical method and interpretation of results based on GC-FID and GC-low resolution-MS analyses

Relations

Amends
EN 15522-2:2023 - Oil spill identification - Petroleum and petroleum related products - Part 2: Analytical method and interpretation of results based on GC-FID and GC-low resolution-MS analyses
Effective Date
23-Aug-2023

Buy Standard

EN 15522-2:2023/oprA1:2024EN 15522-2:2023/oprA1:2024
PreviousNext
Draft
EN 15522-2:2023/oprA1:2024
English language
8 pages
sale 10% off
Preview
sale 10% off
Preview
e-Library read for
1 day

Standards Content (Sample)

SLOVENSKI STANDARD
SIST EN 15522-2:2023/oprA1:2024
01-marec-2024
Prepoznavanje razlitij olj - Nafta in sorodni naftni proizvodi - 2. del: Analizne
metode in podajanje rezultatov, izhajajočih iz GC-FID in GC-MS nizke ločljivosti
Oil spill identification - Petroleum and petroleum related products - Part 2: Analytical
method and interpretation of results based on GC-FID and GC-low resolution-MS
analyses
Identifizierung von Ölverschmutzungen - Rohöl und Mineralölerzeugnisse - Teil 2:
Analytische Methodik und Interpretation der Ergebnisse, basierend auf GC-FID- und GC-
MS-Analysen bei niedriger Auflösung
Identification des pollutions pétrolières - Pétrole et produits pétroliers - Partie 2 :
Méthode d'analyse et interprétation des résultats sur la base des analyses par CPG DIF
et CPG-SM faible résolution
Ta slovenski standard je istoveten z: EN 15522-2:2023/prA1
ICS:
13.020.40 Onesnaževanje, nadzor nad Pollution, pollution control
onesnaževanjem in and conservation
ohranjanje
13.060.99 Drugi standardi v zvezi s Other standards related to
kakovostjo vode water quality
75.080 Naftni proizvodi na splošno Petroleum products in
general
SIST EN 15522-2:2023/oprA1:2024 en
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------
SIST EN 15522-2:2023/oprA1:2024

---------------------- Page: 2 ----------------------
SIST EN 15522-2:2023/oprA1:2024


DRAFT
EUROPEAN STANDARD
EN 15522-2:2023
NORME EUROPÉENNE

EUROPÄISCHE NORM
prA1
March 2024
ICS 13.020.40; 75.080
English Version

Oil spill identification - Petroleum and petroleum related
products - Part 2: Analytical method and interpretation of
results based on GC-FID and GC-low resolution-MS
analyses
Identification des pollutions pétrolières - Pétrole et Identifizierung von Ölverschmutzungen - Rohöl und
produits pétroliers - Partie 2 : Méthode d'analyse et Mineralölerzeugnisse - Teil 2: Analytische Methodik
interprétation des résultats sur la base des analyses und Interpretation der Ergebnisse, basierend auf GC-
par CPG DIF et CPG-SM faible résolution FID- und GC-MS-Analysen bei niedriger Auflösung
This draft amendment is submitted to CEN members for enquiry. It has been drawn up by the Technical Committee CEN/TC 19.

This draft amendment A1, if approved, will modify the European Standard EN 15522-2:2023. If this draft becomes an
amendment, CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for
inclusion of this amendment into the relevant national standard without any alteration.

This draft amendment was established by CEN in three official versions (English, French, German). A version in any other
language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC
Management Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and
United Kingdom.

Recipients of this draft are invited to submit, with their comments, notification of any relevant patent rights of which they are
aware and to provide supporting documentation.

Warning : This document is not a European Standard. It is distributed for review and comments. It is subject to change without
notice and shall not be referred to as a European Standard.


EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2024 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN 15522-2:2023/prA1:2024 E
worldwide for CEN national Members.

---------------------- Page: 3 ----------------------
SIST EN 15522-2:2023/oprA1:2024
EN 15522-2:2023/prA1:2024 (E)
Contents Page
European foreword . 3
1 Modifications to Clause 1, “Scope” . 4
2 Modifications to Clause 3, "Terms and definitions" . 4
3 Modification to 5.2, "GC-FID and GC-MS analysis" . 5
4 Modifications to 6.3.3, "Oil samples from an Ethylene-tetrafluorethylene (ETFE) net" . 5
5 Modification to 6.4.5, "Silica or Florisil® column clean-up" .
...

Questions, Comments and Discussion

Ask us and Technical Secretary will try to provide an answer. You can facilitate discussion about the standard in here.

This May Also Interest You

CEN
EN 15522-2:2023(Main)
Oil spill identification - Petroleum and petroleum related products - Part 2: Analytical method and interpretation of results based on GC-FID and GC-low resolution-MS analyses
SIST EN 15522-2:2023

This document specifies a method to identify and compare the compositional characteristics of oil samples. Specifically, it describes the detailed analytical and data processing methods for identifying the characteristics of spill samples and establishing their correlation to suspected source oils. Even when samples or data from suspected sources are not available for comparison, establishing the specific nature (e.g. refined petroleum, crude oil, waste oil, etc.) of the spilled oil still helps to constrain the possible source(s).
This methodology is restricted to petroleum related products containing a significant proportion of hydrocarbon-components with a boiling point above 150 °C. Examples are: crude oils, higher boiling condensates, diesel oils, residual bunker or heavy fuel oils, lubricants, and mixtures of bilge and sludge samples, as well as distillate fuels and blends. While the specific analytical methods are perhaps not appropriate for lower boiling oils (e.g. kerosene, jet fuel, or gasoline), the general concepts described in this methodology, i.e. statistical comparison of weathering-resistant diagnostic ratios, are applicable in spills involving these kinds of oils.
Paraffin based products (e.g. waxes, etc.) are outside the scope of this method because too many compounds are removed during the production process [37]. However, the method can be used to identify the type of product involved.
Although not directly intended for identifying oil recovered from groundwater, vegetation, wildlife/tissues, soil, or sediment matrices, they are not precluded. However, caution is needed as extractable compounds can be present in these matrices that alter and/or contribute additional compounds compared to the source sample. If unrecognized, the contribution from the matrix can lead to false “non-matches”. It is therefore advisable to analyse background sample(s) of the matrix that appear unoiled.
When analysing “non-oil” matrices additional sample preparation (e.g. clean-up) is often required prior to analysis and the extent to which the matrix affects the correlation achieved is to be considered. Whether the method is applicable for a specific matrix depends upon the oil concentration compared to the “matrix concentration”. In matrices containing high concentrations of oil, a positive match can still be concluded. In matrices containing lower concentrations of oil, a false “non-match” or an “inconclusive match” can result from matrix effects. Evaluation of possible matrix effects is beyond the scope of this document.

  • Standard
    219 pages
    English language
    sale 10% off
    e-Library read for
    1 day
CEN
EN 15522-1:2023(Main)
Oil spill identification - Petroleum and petroleum related products - Part 1: Sampling
SIST EN 15522-1:2023

This document provides guidance on taking and handling samples related to oil spill identification in legal proceedings. Guidance is given on obtaining samples from both the spill and its potential source.
Preservation of evidence is an essential part of legal procedures and this document presents appropriate oil sampling procedures.
WARNING - The use of this document can involve hazardous materials, operations and equipment.
This document does not purport to address all of the safety problems associated with its use. It is the responsibility of users of this document to take appropriate measures to ensure the safety and health of personnel prior to the application of the standard, and to determine the applicability of any other restrictions for this purpose.
IMPORTANT - Most countries have teams with specialists trained in sampling on board of ships. Do not take unnecessary risks, seek assistance from such teams where available.
NOTE   For the sake of clarity, the word ‘oil’ is used throughout this document. It can equally refer to crude oil, a petroleum product or mixtures of such.

  • Standard
    31 pages
    English language
    sale 10% off
    e-Library read for
    1 day
CEN
EN 15522-2:2023(Main)
Oil spill identification - Petroleum and petroleum related products - Part 2: Analytical method and interpretation of results based on GC-FID and GC-low resolution-MS analyses
SIST EN 15522-2:2023

This document specifies a method to identify and compare the compositional characteristics of oil samples. Specifically, it describes the detailed analytical and data processing methods for identifying the characteristics of spill samples and establishing their correlation to suspected source oils. Even when samples or data from suspected sources are not available for comparison, establishing the specific nature (e.g. refined petroleum, crude oil, waste oil, etc.) of the spilled oil still helps to constrain the possible source(s).
This methodology is restricted to petroleum related products containing a significant proportion of hydrocarbon-components with a boiling point above 150 °C. Examples are: crude oils, higher boiling condensates, diesel oils, residual bunker or heavy fuel oils, lubricants, and mixtures of bilge and sludge samples, as well as distillate fuels and blends. While the specific analytical methods are perhaps not appropriate for lower boiling oils (e.g. kerosene, jet fuel, or gasoline), the general concepts described in this methodology, i.e. statistical comparison of weathering-resistant diagnostic ratios, are applicable in spills involving these kinds of oils.
Paraffin based products (e.g. waxes, etc.) are outside the scope of this method because too many compounds are removed during the production process [37]. However, the method can be used to identify the type of product involved.
Although not directly intended for identifying oil recovered from groundwater, vegetation, wildlife/tissues, soil, or sediment matrices, they are not precluded. However, caution is needed as extractable compounds can be present in these matrices that alter and/or contribute additional compounds compared to the source sample. If unrecognized, the contribution from the matrix can lead to false “non-matches”. It is therefore advisable to analyse background sample(s) of the matrix that appear unoiled.
When analysing “non-oil” matrices additional sample preparation (e.g. clean-up) is often required prior to analysis and the extent to which the matrix affects the correlation achieved is to be considered. Whether the method is applicable for a specific matrix depends upon the oil concentration compared to the “matrix concentration”. In matrices containing high concentrations of oil, a positive match can still be concluded. In matrices containing lower concentrations of oil, a false “non-match” or an “inconclusive match” can result from matrix effects. Evaluation of possible matrix effects is beyond the scope of this document.

  • Standard
    219 pages
    English language
    sale 10% off
    e-Library read for
    1 day
CEN
EN 15522-1:2023(Main)
Oil spill identification - Petroleum and petroleum related products - Part 1: Sampling
SIST EN 15522-1:2023

This document provides guidance on taking and handling samples related to oil spill identification in legal proceedings. Guidance is given on obtaining samples from both the spill and its potential source.
Preservation of evidence is an essential part of legal procedures and this document presents appropriate oil sampling procedures.
WARNING - The use of this document can involve hazardous materials, operations and equipment.
This document does not purport to address all of the safety problems associated with its use. It is the responsibility of users of this document to take appropriate measures to ensure the safety and health of personnel prior to the application of the standard, and to determine the applicability of any other restrictions for this purpose.
IMPORTANT - Most countries have teams with specialists trained in sampling on board of ships. Do not take unnecessary risks, seek assistance from such teams where available.
NOTE   For the sake of clarity, the word ‘oil’ is used throughout this document. It can equally refer to crude oil, a petroleum product or mixtures of such.

  • Standard
    31 pages
    English language
    sale 10% off
    e-Library read for
    1 day
CEN
EN ISO 22435:2024(Main)
Gas cylinders - Cylinder valves with integrated pressure regulators - Specification and type testing (ISO 22435:2024)
kSIST FprEN ISO 22435:2024

This document specifies design, type test methods, marking and instruction requirements for cylinder valves with integrated pressure regulators (VIPRs) intended to be fitted to gas cylinders, pressure drums or tubes or used as a main valve for bundles of cylinders that convey compressed, liquefied or dissolved gases.
These are requirements for VIPRs that are in addition to those given in the relevant closure standard, for example, in ISO 10297 for cylinder valves, in ISO 17871 for quick-release cylinder valves, in ISO 17879 for self-closing cylinder valves or in ISO 23826 for ball valves. For ISO 17871, these requirements are only applicable to quick-release cylinder valves types B, C, D and E.
NOTE 1        If the pressure regulating system of a VIPR is acting as the primary valve operating mechanism, it is covered by the relevant closure standard, e.g. ISO 10297, ISO 17871, ISO 17879 and ISO 23826. This also includes designs where closure of the primary valve operating mechanism of a VIPR is obtained by closing the seat of the pressure regulating system.
NOTE 2        If the primary valve operating mechanism of a VIPR is located at the low-pressure side of the pressure regulating system, it is covered by the relevant closure standard, e.g. ISO 10297, ISO 17871, ISO 17879 and ISO 23826.
NOTE 3        The term “pressure receptacle” is used within this document to cover instances where no differentiation is necessary between gas cylinders, bundles of cylinders, pressure drums and tubes.
This document does not apply to VIPRs for
a)       medical applications (see ISO 10524-3);
b)       liquefied petroleum gas (LPG);
c)        cryogenic applications.
NOTE 4        Additional requirements for a VIPR with a residual pressure device (RPD) are specified in ISO 15996.
NOTE 5        Additional requirements for pressure relief valves can exist in international/regional regulations/ standards.

  • Draft
    39 pages
    English language
    sale 10% off
    e-Library read for
    1 day
CEN
EN 17015-1:2024(Main)
Electronic Public Procurement - Catalogue - Part 1: Choreographies
kSIST FprEN 17015-1:2024

The purpose of this deliverable is to specify and describe choreographies for exchanging an electronic product catalogue (“catalogues”) as part of the business processes in the pre-award and post-award area, so that catalogues can serve as a basis for placing orders as well as evaluating tenders. The key aspects covered by this choreography specification are:
-   processes for submitting catalogues from the selling to the buying side;
-   processes for submitting catalogue-related data as part of a tendering process;
-   processes integrating sell-side procurement systems.
This document does not apply to the transactions used in the specified choreographies. These transactions are specified in EN 17015 2. The relationship between the choreographies and the transaction is described in Clause 8.
The identifier of this choreographies document is EN 17015 1:2024.
How to claim compliance to this choreography is specified in 6.2.3.

  • Draft
    38 pages
    English language
    sale 10% off
    e-Library read for
    1 day
CEN
EN ISO/ASTM 52927:2024(Main)
Additive manufacturing - General principles - Main characteristics and corresponding test methods (ISO/ASTM 52927:2024)
kSIST FprEN ISO/ASTM 52927:2024

This document specifies the principal requirements applied to the testing of parts produced by additive manufacturing processes.
This document
—     identifies quality characteristics for feedstock and parts and the corresponding test procedures,
—     provides the specific procedures to build specimens using additive manufacturing process, and
—     recommends the scope and content of test and supply agreements.
This document is aimed at machine manufacturers, feedstock suppliers, AM system users, part providers, and customers to facilitate the communication on main quality characteristics. It applies wherever additive manufacturing processes are used.
NOTE            It is the intent to include, in future versions of this document, other characteristics such as thermal properties, electrical requirements and physical and physico-chemical properties based upon material types.

  • Draft
    28 pages
    English language
    sale 10% off
    e-Library read for
    1 day
CEN
EN ISO 8362-2:2024(Main)
Injection containers and accessories - Part 2: Closures for injection vials (ISO 8362-2:2024)
SIST EN ISO 8362-2:2024

This document specifies the shape, dimensions, material, performance requirements and labelling of closures for injection vials covered by ISO 8362-1 and ISO 8362-4.
The dimensional requirements are not applicable to barrier-coated closures.
Closures specified in this document are intended for single use only.
NOTE            The potency, purity, stability and safety of a medicinal product during its manufacture and storage can strongly be affected by the nature and performance of the primary packaging.

  • Draft
    10 pages
    English language
    sale 10% off
    e-Library read for
    1 day
CEN
EN ISO 16739-1:2024(Main)
Industry Foundation Classes (IFC) for data sharing in the construction and facility management industries - Part 1: Data schema (ISO 16739-1:2024)
kSIST FprEN ISO 16739-1:2024

This document represents an open international standard for information used in Building Information Modeling (BIM) that is exchanged and shared among software applications used by the various participants in the construction or facility management industry sector. This document includes definitions that cover information required for buildings and infrastructure works over their life cycle. This edition of the document added coverage of information required for infrastructure facilities including bridges, roads, railways, waterways and port facilities.
This document comprises the publication of a data schema, its documentation, the property and quantity set definitions and the mechanism of an exchange file format structure.
Definitions from this document are used to support different recognized work flows in the construction and facility management industry sector, representing information deliveries. Such information deliveries can be described according to ISO 29481.
Different implementation levels of this document can be defined to better support multiple information deliveries, they are referred to as a Model View Definition (MVD). Each MVD identifies which subset of the definitions of this document imposes requirements for implementation in software applications. Conforming software applications need to identify the model view definition they conform to when applying for software certification.
The following are within the scope of this edition of this document:
BIM exchange format definitions that are required during the life cycle phases of buildings and infrastructure:
demonstrating the need;
conception of need;
outline feasibility;
substantive feasibility study and outline financial authority;
outline conceptual design;
full conceptual design;
coordinated design;
procurement and full financial authority;
production information;
construction;
operation and maintenance.
BIM exchange format definitions that are required by the various disciplines involved within the life cycle phases:
architecture and civil engineering design;
service and utilities engineering;
structural engineering;
procurement;
construction planning;
facility and utility management;
project management;
client requirement management;
industry authorities for permits and approval.
BIM exchange format definitions including:
project structure;
physical components;
spatial components;
analysis items;
processes;
resources;
controls;
actors;
context definition.

  • Draft
    406 pages
    English language
    sale 10% off
    e-Library read for
    1 day
CEN
EN ISO 2620:2024(Main)
Analysis of natural gas - Biomethane - Determination of VOCs by thermal desorption gas chromatography with flame ionization and/or mass spectrometry detectors (ISO 2620:2024)
kSIST FprEN ISO 2620:2024

This document describes a method for sampling and analysis of volatile organic compounds (VOCs), including siloxanes, terpenes, organic sulfur compounds, in natural gas and biomethane matrices, using thermal desorption gas chromatography with flame ionization and/or mass spectrometry detectors (TD-GC-FID/MS).

  • Draft
    13 pages
    English language
    sale 10% off
    e-Library read for
    1 day