EN ISO 75-2:2004
(Main)Plastics - Determination of temperature of deflection under load - Part 2: Plastics, ebonite and long-fibre-reinforced composites (ISO 75-2:2004)
Plastics - Determination of temperature of deflection under load - Part 2: Plastics, ebonite and long-fibre-reinforced composites (ISO 75-2:2004)
ISO 75-2:2004 specifies three methods, using different values of constant flexural stress, that can be used for the determination of the temperature of deflection under load of plastics (including filled plastics and fibre-reinforced plastics in which the fibre length, prior to processing, is up to 7,5 mm) and ebonite:
method A, using a flexural stress of 1,80 MPa;
method B, using a flexural stress of 0,45 MPa;
method C, using a flexural stress of 8,00 MPa.
Kunststoffe - Bestimmung der Wärmeformbeständigkeitstemperatur - Teil 2: Kunststoffe, Hartgummi und langfaserverstärkte Kunststoffe (ISO 75-2:2004)
Dieser Teil von ISO 75 beschreibt 3 Verfahren zur Bestimmung der Wärmeformbeständigkeitstemperatur von Kunststoffen, Hartgummi und langfaserverstärkten Kunststoffen unter Verwendung verschiedener Biegespannungen:
Verfahren A, unter Verwendung einer Biegespannung von 1,80 MPa;
Verfahren B, unter Verwendung einer Biegespannung von 0,45 MPa;
Verfahren C, unter Verwendung einer Biegespannung von 8,00 MPa.
Die zur Bestimmung der Wärmeformbeständigkeitstemperatur verwendete Standarddurchbiegung, s, entspricht der in diesem Teil der Norm festgelegten Biegedehnungserhöhung f. Die Anfangs-Biegedehnung bei Belastung des Probekörpers bei Raumtemperatur ist in diesem Teil weder festgelegt noch wird sie gemessen. Das Verhältnis dieses Biegedehnungsunterschieds zur Anfangs-Biegedehnung ist vom Elastizitätsmodul des geprüften Werkstoffes bei Raumtemperatur abhängig. Dieses Verfahren ist daher nur anwendbar zum Vergleich von Werkstoffen mit ähnlichen Elastizitätseigenschaften bei Raumtemperatur.
ANMERKUNG Die Verfahren geben bei amorphen Thermoplasten eine bessere Vergleichpräzision als bei teilkristallinen. Bei einigen Werkstoffen kann es notwendig sein, die Probekörper zu tempern, um zuverlässige Ergebnisse zu erhalten. Falls eine Temperung angewendet wird, führt sie im allgemeinen zu einem Anstieg der Wärmeformbeständigkeitstemperatur (siehe 6.6).
Ergänzende Informationen siehe ISO 75-1:2003, Abschnitt 1.
Plastiques - Détermination de la température de fléchissement sous charge - Plastiques, ébonite et composites renforcés de fibres longues (ISO 75-2:2004)
L'ISO 75-2:2004 spécifie trois méthodes utilisant différentes valeurs de contrainte de flexion constante qui peuvent être utilisées pour la détermination de la température de fléchissement sous charge de plastiques (incluant des plastiques chargés et des plastiques renforcés de fibres, dans lesquels la longueur de fibre avant l'emploi est inférieure ou égale à 7,5 mm) et d'ébonite:
méthode A, utilisant une contrainte de flexion de 1,80 MPa;
méthode B, utilisant une contrainte de flexion de 0,45 MPa;
méthode C, utilisant une contrainte de flexion de 8,00 MPa.
Polimerni materiali - Določanje temperature upogiba pod obremenitvijo - 2. del: Polimerni materiali, ebonit in z dolgimi vlakni ojačeni polimerni materiali (ISO 75-2:2004)
General Information
Relations
Standards Content (Sample)
SLOVENSKI STANDARD
01-oktober-2004
1DGRPHãþD
SIST EN ISO 75-2:2000
3ROLPHUQLPDWHULDOL'RORþDQMHWHPSHUDWXUHXSRJLEDSRGREUHPHQLWYLMRGHO
3ROLPHUQLPDWHULDOLHERQLWLQ]GROJLPLYODNQLRMDþHQLSROLPHUQLPDWHULDOL ,62
Plastics - Determination of temperature of deflection under load - Part 2: Plastics, ebonite
and long-fibre-reinforced composites (ISO 75-2:2004)
Kunststoffe - Bestimmung der Wärmeformbeständigkeitstemperatur - Teil 2: Kunststoffe,
Hartgummi und langfaserverstärkte Kunststoffe (ISO 75-2:2004)
Plastiques - Détermination de la température de fléchissement sous charge - Plastiques,
ébonite et composites renforcés de fibres longues (ISO 75-2:2004)
Ta slovenski standard je istoveten z: EN ISO 75-2:2004
ICS:
83.080.01 Polimerni materiali na Plastics in general
splošno
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.
INTERNATIONAL ISO
STANDARD 75-2
Second edition
2004-05-15
Plastics — Determination of temperature of
deflection under load —
Part 2:
Plastics and ebonite
Plastiques — Détermination de la température de fléchissement sous
charge —
Partie 2: Plastiques et ébonite
Reference number
ISO 75-2:2004(E)
©
ISO 2004
ISO 75-2:2004(E)
PDF disclaimer
This PDF file may contain embedded typefaces. In accordance with Adobe's licensing policy, this file may be printed or viewed but shall not
be edited unless the typefaces which are embedded are licensed to and installed on the computer performing the editing. In downloading this
file, parties accept therein the responsibility of not infringing Adobe's licensing policy. The ISO Central Secretariat accepts no liability in this
area.
Adobe is a trademark of Adobe Systems Incorporated.
Details of the software products used to create this PDF file can be found in the General Info relative to the file; the PDF-creation parameters
were optimized for printing. Every care has been taken to ensure that the file is suitable for use by ISO member bodies. In the unlikely event
that a problem relating to it is found, please inform the Central Secretariat at the address given below.
© ISO 2004
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized in any form or by any means, electronic
or mechanical, including photocopying and microfilm, without permission in writing from either ISO at the address below or ISO's member body
in the country of the requester.
ISO copyright office
Case postale 56 • CH-1211 Geneva 20
Tel. + 41 22 749 01 11
Fax + 41 22 749 09 47
E-mail copyright@iso.org
Web www.iso.org
Published in Switzerland
ii © ISO 2004 – All rights reserved
ISO 75-2:2004(E)
Contents Page
Foreword . iv
Introduction. v
1 Scope. 1
2 Normative references. 1
3 Terms and definitions. 2
4 Principle . 2
5 Apparatus. 2
6 Test specimens . 2
7 Conditioning . 3
8 Procedure (flatwise testing) . 3
9 Expression of results. 4
10 Precision . 4
11 Test report. 5
Annex A (normative) Testing in the edgewise position. 6
Annex B (informative) Precision . 8
Bibliography. 10
ISO 75-2:2004(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO
member bodies). The work of preparing International Standards is normally carried out through ISO technical
committees. Each member body interested in a subject for which a technical committee has been established has
the right to be represented on that committee. International organizations, governmental and non-governmental, in
liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical
Commission (IEC) on all matters of electrotechnical standardization.
International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2.
The main task of technical committees is to prepare International Standards. Draft International Standards adopted
by the technical committees are circulated to the member bodies for voting. Publication as an International
Standard requires approval by at least 75 % of the member bodies casting a vote.
Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights.
ISO shall not be held responsible for identifying any or all such patent rights.
ISO 75-2 was prepared by Technical Committee ISO/TC 61, Plastics, Subcommittee SC 2, Mechanical properties.
This second edition cancels and replaces the first edition (ISO 75-2:1993), which has been technically revised.
ISO 75 consists of the following parts, under the general title Plastics — Determination of temperature of deflection
under load:
Part 1: General test method
Part 2: Plastics and ebonite
Part 3: High-strength thermosetting laminates and long-fibre-reinforced plastics
Annex A forms a normative part of this part of ISO 75. Annex B is for information only.
iv © ISO 2004 – All rights reserved
ISO 75-2:2004(E)
Introduction
ISO 75-1:1993 and ISO 75-2:1993 described three methods (A, B and C) using different test loads and two
specimen positions, edgewise and flatwise. For testing in the flatwise position, test specimens with dimensions
80 mm × 10 mm × 4 mm were required. These can be moulded directly or machined from the central section of the
multipurpose test specimen (see ISO 3167). These “ISO bars” cannot be easily used in the edgewise position,
because this would require both a reduction in span and an increase in test load by the same factor, and this may
be impossible to achieve on existing instruments for edgewise testing. Specimens for testing in the edgewise
position are less closely specified. Using the 80 mm × 10 mm × 4 mm ISO bar has the following advantages:
Thermal expansion of the test specimen has less influence on the test result.
Draft angles do not influence the test result. The specimen does not stand “on edge”.
The moulding parameters and the specimen dimensions are specified more closely.
This increases the comparability of the test results. Therefore, it was decided that the possibility of testing in the
edgewise position would be deleted from the standard. In order to provide a sufficient transition period, in this
edition the flatwise position is described as the preferred and recommended one, while testing in the edgewise
position is optional and has been moved to a normative annex (in this part of ISO 75). This annex and all other
references to edgewise testing will be deleted on occasion of the next revision of this document.
Earlier editions of this International Standard allowed methods other than using a heating bath for heating the test
specimen, namely forced-circulation ovens or fluidized beds. None of these alternative methods is widely used and
no proven instruments are commercially available. Furthermore, there is no general comparability between tests
using different heating methods due to the differences in the heat transfer characteristics and the temperature
control methods described in this standard.
Therefore only heating in heating baths is allowed in this edition.
In order to maintain consistency with ISO 10350-1:1998, T has been used as the symbol for temperature of
f
deflection under load.
INTERNATIONAL STANDARD ISO 75-2:2004(E)
Plastics — Determination of temperature of deflection under
load —
Part 2:
Plastics and ebonite
1 Scope
This part of ISO 75 specifies three methods, using different values of constant flexural stress, that can be used for
the determination of the temperature of deflection under load of plastics (including filled plastics and fibre-
reinforced plastics in which the fibre length, prior to processing, is up to 7,5 mm) and ebonite:
method A, using a flexural stress of 1,80 MPa;
method B, using a flexural stress of 0,45 MPa;
method C, using a flexural stress of 8,00 MPa.
The standard deflection ∆s used to determine the temperature of deflection under load corresponds to a flexural-
strain increase ∆ε defined in this part of ISO 75. The initial flexural strain due to the loading of the specimen at
f
room temperature is neither specified nor measured in this part of ISO 75. The ratio of this flexural-strain difference
to the initial flexural strain depends on the modulus of elasticity, at room temperature, of the material under test.
This method is therefore only suitable for comparing the temperatures of deflection of materials with similar room-
temperature elastic properties.
NOTE The methods give better reproducibility with amorphous plastics than with semi-crystalline ones. With some
materials, it may be necessary to anneal the test specimens to obtain reliable results. Annealing procedures, if used, generally
result in an increase in the temperature of deflection under load (see 6.6).
For additional information, see ISO 75-1:2004, clause 1.
2 Normative references
The following referenced documents are indispensable for the application of this document. For dated references,
only the edition cited applies. For undated references, the latest edition of the referenced document (including any
amendments) applies.
ISO 75-1:2004, Plastics — Determination of temperature of deflection under load — Part 1: General test method
ISO 293, Plastics — Compression moulding test specimens of thermoplastic materials
ISO 294-1, Plastics — Injection moulding of test specimens of thermoplastic materials — Part 1: General principles,
and moulding of multipurpose and bar test specimens
ISO 2818, Plastics — Preparation of test specimens by machining
ISO 75-2:2004(E)
ISO 3167, Plastics — Multipurpose test specimens
ISO 10724-1, Plastics — Injection moulding of test specimens of thermosetting powder moulding compounds
(PMCs) — Part 1: General principles and moulding of multipurpose test specimens
3 Terms and definitions
For the purposes of this document, the terms and definitions given in ISO 75-1 apply.
NOTE Depending on the selected value of the flexural stress (see clause 1), the temperature of deflection under load (see
definition 3.7 in ISO 75-1:2004) is designated as T 0,45, T 1,8 or T 8,0 (where x = f for flatwise testing and x = e for
fx fx fx
edgewise testing).
4 Principle
See ISO 75-1:2004, clause 4.
5 Apparatus
5.1 Means of producing a flexural stress
See ISO 75-1:2004, subclause 5.1.
The span (distance between the lines of contact between specimen and supports) shall be (64 ± 1) mm for testing
in the preferred (flatwise) position. See annex A for testing in the edgewise position.
5.2 Heating equipment
See ISO 75-1:2004, subclause 5.2.
5.3 Weights
See ISO 75-1:2004, subclause 5.3.
5.4 Temperature-measuring instrument
See ISO 75-1:2004, subclause 5.4.
5.5 Deflection-measuring instrument
See ISO 75-1:2004, subclause 5.5.
6 Test specimens
6.1 General
See ISO 75-1:2004, subclause 6.1.
2 © ISO 2004 – All rights reserved
ISO 75-2:2004(E)
6.2 Shape and dimensions
See ISO 75-1:2004, subclause 6.2.
The preferred test-specimen dimensions are:
length l: (80 ± 2,0) mm;
width b: (10 ± 0,2) mm;
thickness h: (4 ± 0,2) mm.
See annex A for dimensions of test specimens for edgewise testing.
6.3 Specimen inspection
See ISO 75-1:2004, subclause 6.3.
6.4 Number of test specimens
See ISO 75-1:2004, subclause 6.4.
6.5 Test-specimen preparation
Test specimens shall be produced in accordance with ISO 293 (and ISO 2818, if applicable), or in accordance with
ISO 294
...
Questions, Comments and Discussion
Ask us and Technical Secretary will try to provide an answer. You can facilitate discussion about the standard in here.