Soft soldering fluxes - Test methods - Part 16: Flux efficacy test, wetting balance method (ISO 9455-16:2013)

ISO 9455-16:2013 specifies a method for the assessment of the efficacy of a soft soldering flux, known as the wetting balance method. It gives a qualitative assessment of the comparative efficacy of two fluxes (for example, a standard and a test flux), based on their capacity to promote wetting of a metal surface by liquid solder. The method is applicable to all flux types in liquid form classified in ISO 9454‑1.

Flussmittel zum Weichlöten - Prüfverfahren - Teil 16: Bestimmung der Wirksamkeit des Flussmittels, Verfahren zur Messung der Benetzungskraft (ISO 9455-16:2013)

Dieser Teil der ISO 9455 legt ein Verfahren zum Beurteilen der Wirksamkeit eines Flussmittels zum
Weichlöten fest, das als Verfahren zur Messung der Benetzungskraft bezeichnet wird. Es bietet eine
qualitative Beurteilung für den Vergleich der Wirksamkeit zweier Flussmittel (z. B. ein Standard-Flussmittel mit
einem zu prüfenden Flussmittel) hinsichtlich ihrer Fähigkeiten, die Benetzung einer Metalloberfläche durch ein
flüssiges Weichlot zu fördern. Das Verfahren ist für alle flüssigen Flussmitteltypen anwendbar, die in
ISO 9454-1 aufgeführt sind.
ANMERKUNG Es ist anzunehmen, dass zukünftige Entwicklungen, welche mit verbesserten Verfahren einen
reproduzierbaren Oberflächenbereich zum Prüfen ergeben, es möglich machen, dieses Verfahren zum Beurteilen der
Flussmittelwirksamkeit quantitativ einzusetzen. Aus diesem Grund sind verschiedene alternative Verfahren zur
Vorbereitung der Prüfstückoberfläche in der vorliegenden Norm enthalten.

Flux de brasage tendre - Méthodes d'essai - Partie 16: Essai d'efficacité du flux, méthode à la balance de mouillage (ISO 9455-16:2013)

L'ISO 9455-16:2013 spécifie une méthode pour l'évaluation de l'efficacité d'un flux de brasage tendre, connue sous le nom de méthode à la balance de mouillage. Elle permet une évaluation qualitative de l'efficacité comparée de deux flux faisant l'objet d'une comparaison (par exemple un flux de référence et un flux d'essai), évaluation fondée sur la capacité de ces flux à faciliter le mouillage de la surface d'un métal par le produit d'apport liquide. Cette méthode est applicable à tous les types de flux sous forme liquide classés dans l'ISO 9454-1.

Talila za mehko spajkanje - Preskusne metode - 16. del: Preskus učinkovitosti, postopek za merjenje omočljivosti (ISO 9455-16:2013)

Ta del ISO 9455 določa metodo za oceno učinkovitosti talila za mehko spajkanje, znano kot postopek za merjenje omočljivosti. Na osnovi zmogljivosti spodbujanja omočljivosti kovinske površine s tekočim talilom podaja kvalitativno oceno primerjalne učinkovitosti dveh talil (npr. standardnega in preskusnega talila). Ta metoda velja za vse vrste talil v tekoči obliki iz ISO 9454-1.

General Information

Status
Withdrawn
Publication Date
16-Apr-2013
Withdrawal Date
15-Oct-2019
Technical Committee
Drafting Committee
Current Stage
9960 - Withdrawal effective - Withdrawal
Completion Date
16-Oct-2019

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SLOVENSKI STANDARD
01-september-2013
1DGRPHãþD
SIST EN ISO 9455-16:2002
7DOLOD]DPHKNRVSDMNDQMH3UHVNXVQHPHWRGHGHO3UHVNXVXþLQNRYLWRVWL
SRVWRSHN]DPHUMHQMHRPRþOMLYRVWL ,62
Soft soldering fluxes - Test methods - Part 16: Flux efficacy test, wetting balance method
(ISO 9455-16:2013)
Flussmittel zum Weichlöten - Prüfverfahren - Teil 16: Bestimmung der Wirksamkeit des
Flussmittels, Verfahren zur Messung der Benetzungskraft (ISO 9455-16:2013)
Flux de brasage tendre - Méthodes d'essai - Partie 16: Essai d'efficacité du flux,
méthode à la balance de mouillage (ISO 9455-16:2013)
Ta slovenski standard je istoveten z: EN ISO 9455-16:2013
ICS:
25.160.50 Trdo in mehko lotanje Brazing and soldering
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

EUROPEAN STANDARD
EN ISO 9455-16
NORME EUROPÉENNE
EUROPÄISCHE NORM
April 2013
ICS 25.160.50 Supersedes EN ISO 9455-16:2001
English Version
Soft soldering fluxes - Test methods - Part 16: Flux efficacy test,
wetting balance method (ISO 9455-16:2013)
Flux de brasage tendre - Méthodes d'essai - Partie 16: Flussmittel zum Weichlöten - Prüfverfahren - Teil 16:
Essai d'efficacité du flux, méthode à la balance de Bestimmung der Wirksamkeit des Flussmittels, Verfahren
mouillage (ISO 9455-16:2013) zur Messung der Benetzungskraft (ISO 9455-16:2013)
This European Standard was approved by CEN on 2 February 2013.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European
Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national
standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member.

This European Standard exists in three official versions (English, French, German). A version in any other language made by translation
under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same
status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United
Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

Management Centre: Avenue Marnix 17, B-1000 Brussels
© 2013 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 9455-16:2013: E
worldwide for CEN national Members.

Contents Page
Foreword .3
Foreword
This document (EN ISO 9455-16:2013) has been prepared by Technical Committee ISO/TC 44 "Welding and
allied processes" in collaboration with Technical Committee CEN/TC 121 “Welding” the secretariat of which is
held by DIN.
This European Standard shall be given the status of a national standard, either by publication of an identical
text or by endorsement, at the latest by October 2013, and conflicting national standards shall be withdrawn at
the latest by October 2013.
Attention is drawn to the possibility that some of the elements of this document may be the subject of patent
rights. CEN [and/or CENELEC] shall not be held responsible for identifying any or all such patent rights.
This document supersedes EN ISO 9455-16:2001.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the following
countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech
Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece,
Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,
Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom.
Endorsement notice
The text of ISO 9455-16:2013 has been approved by CEN as EN ISO 9455-16:2013 without any modification.

INTERNATIONAL ISO
STANDARD 9455-16
Second edition
2013-04-15
Soft soldering fluxes — Test methods —
Part 16:
Flux efficacy test, wetting balance
method
Flux de brasage tendre — Méthodes d’essai —
Partie 16: Essai d’efficacité du flux, méthode à la balance de mouillage
Reference number
ISO 9455-16:2013(E)
©
ISO 2013
ISO 9455-16:2013(E)
© ISO 2013
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized otherwise in any form
or by any means, electronic or mechanical, including photocopying, or posting on the internet or an intranet, without prior
written permission. Permission can be requested from either ISO at the address below or ISO’s member body in the country of
the requester.
ISO copyright office
Case postale 56 • CH-1211 Geneva 20
Tel. + 41 22 749 01 11
Fax + 41 22 749 09 47
E-mail copyright@iso.org
Web www.iso.org
Published in Switzerland
ii © ISO 2013 – All rights reserved

ISO 9455-16:2013(E)
Contents Page
Foreword .iv
1 Scope . 1
2 Normative references . 1
3 Symbols . 1
4 Principle . 2
5 Reagents . 2
6 Apparatus . 2
7 Test pieces . 3
8 Procedure. 3
8.1 Preparation of the test pieces. 3
8.2 Test method . 3
9 Reference value using standard flux . 4
10 Presentation of results . 4
11 Calculation and expression of results . 6
12 Test report . 7
Annex A (normative) Method for the preparation of standard rosin (colophony) based liquid
fluxes having 25 % (by mass) non-volatile content
......................................................................................................... 8
Annex B (normative) Method for the production of test pieces with a controlled-contaminated
surface for the wetting balance test (artificial sulfidation method) .10
ISO 9455-16:2013(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.
ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2.
The main task of technical committees is to prepare International Standards. Draft International
Standards adopted by the technical committees are circulated to the member bodies for voting.
Publication as an International Standard requires approval by at least 75 % of the member bodies
casting a vote.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights.
ISO 9455-16 was prepared by Technical Committee ISO/TC 44, Welding and allied processes, Subcommittee
SC 12, Soldering materials.
This second edition cancels and replaces the first edition (ISO 9455-16:1998), which has been
technically revised.
ISO 9455 consists of the following parts, under the general title Soft soldering fluxes — Test methods:
— Part 1: Determination of non-volatile matter, gravimetric method
— Part 2: Determination of non-volatile matter, ebulliometric method
— Part 3: Determination of acid value, potentiometric and visual titration methods
— Part 5: Copper mirror test
— Part 6: Determination and detection of halide (excluding fluoride) content
— Part 8: Determination of zinc content
— Part 9: Determination of ammonia content
— Part 10: Flux efficacy test, solder spread method
— Part 11: Solubility of flux residues
— Part 13: Determination of flux spattering
— Part 14: Assessment of tackiness of flux residues
— Part 15: Copper corrosion test
— Part 16: Flux efficacy test, wetting balance method
— Part 17: Surface insulation resistance comb test and electrochemical migration test of flux residues
Requests for official interpretations of any aspect of this part of ISO 9455 should be directed to the
Secretariat of ISO/TC 44/SC 12 via your national standards body. A complete listing of these bodies can
be found at www.iso.org.
iv © ISO 2013 – All rights reserved

INTERNATIONAL STANDARD ISO 9455-16:2013(E)
Soft soldering fluxes — Test methods —
Part 16:
Flux efficacy test, wetting balance method
1 Scope
This part of ISO 9455 specifies a method for the assessment of the efficacy of a soft soldering flux, known
as the wetting balance method. It gives a qualitative assessment of the comparative efficacy of two
fluxes (for example, a standard and a test flux), based on their capacity to promote wetting of a metal
surface by liquid solder. The method is applicable to all flux types in liquid form classified in ISO 9454-1.
NOTE It is hoped that future developments using improved techniques for obtaining a reproducible range
of test surfaces will enable this method for assessing flux efficacy to be quantitative. For this reason, several
alternative procedures for preparing the surface of the test piece are included in the present method.
2 Normative references
The following referenced documents are indispensable for the application of this document. For dated
references, only the edition cited applies. For undated references, the latest edition of the referenced
document (including any amendments) applies.
ISO 9453, Soft solder alloys — Chemical compositions and forms
ISO 9454-1, Soft soldering fluxes — Classification and requirements — Part 1: Classification, labelling
and packaging
IEC 60068-2-20:2008, Environmental testing — Part 2-20: Tests — Test T: Test methods for solderability
and resistance to soldering heat of devices with leads
IEC 60068-2-54, Environmental testing — Part 2-54: Tests — Test Ta: Solderability testing of electronic
components by the wetting balance method
IEC 60068-2-78:2001, Environmental testing — Part 2-78: Tests; Test Cab: Damp heat, steady state
3 Symbols
d depth of immersion, in millimetres, of the test piece below the undisturbed solder level
A cross sectional area, in square millimetres, of the test piece at the solder line
ρ density, in grams per millilitre, of the solder under test at the test temperature
F wetting force, in millinewtons
t time at which the test piece first mak
...

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