D34.01.02 - Sampling Techniques
Sampling Techniques
General Information
SIGNIFICANCE AND USE
4.1 This practice can be used in sampling ash from a kiln or incinerator, soils, and process waste from conveying systems, such as a conveyer and vertical lifts. Some slurries, such as the bottom solids, can be sampled from the quench waters at the end of a kiln.
4.2 This practice can be used to determine material balances for burner efficiency studies and compliance studies.
4.3 This practice can be used on lifts, sloping, and horizontal conveyor systems. The type of conveyor and the amount and type of sample required will dictate the type of sampling equipment required to get a representative sample.
4.4 The sample is taken directly from the conveyor before emptying into the waste container or pile for disposal or recycling using a scoop, dipper, or shovel depending upon the sample requirements (see Practice D5633). The sample is then put into the sample container for analysis.
4.5 The place, quantity, frequency, and time of sampling is dependent upon the conveying system equipment, data quality objectives (DQOs) (Practice D5792), work or sampling plan (see Practice D5283 and Guide D4687), and analysis to be run.
4.5.1 Large particles can be mechanically excluded on a belt system. Large particles may accumulate at the bottom of an inclined/sloped belt system. Therefore, steps, if possible, need to be taken so that particles of all sizes have equal chances of being sampled.
4.5.2 The number of samples and sample time is dependent upon the system, the precision required, the decisions that are to be made, the cost, and the degree of heterogeneity of the material (see Guides D5956 and D6311).
4.5.3 In general, the ideal sampling location is nearest to the point of generation since temperature, oxidation, and air movement may change some samples with time.
4.6 The practice does not address issues related to the heterogeneity of the sample.
SCOPE
1.1 This practice describes standard procedures for sampling waste on open and closed conveying systems and is applicable to any waste material that can be conveyed to a waste pile or container. The conveyor system can be a vertical (vertical lifts), sloped, or horizontal type.
1.2 This practice is intended for particles and slurries, which can be sampled using scoop, dipper, or shovel type samplers.
1.3 The practice is not intended for large size sample constituents, such as boulders, large rocks, and debris.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
- Standard3 pagesEnglish language
- Standard3 pagesEnglish language
SIGNIFICANCE AND USE
5.1 This practice is intended for use in collecting samples of unconsolidated solid materials from drums or similar containers, including those that are unstable, ruptured, or compromised otherwise. Special handling procedures (for example, remote drum opening, overpressurized drum opening, drum deheading, etc.) are described in EPA/600/2-86/013, Drum Handling Practices at Hazardous Waste Sites.
SCOPE
1.1 This practice covers typical equipment and methods for collecting samples of unconsolidated solids in drums or similar containers. These methods are adapted specifically for sampling drums having a volume of 110 U.S. gal (416 L) or less. These methods are applicable to hazardous material, product, or waste. Specific sample collection and handling requirements should be described in the site-specific work plan.
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
- Standard6 pagesEnglish language
SIGNIFICANCE AND USE
5.1 This practice is intended for use in collecting samples of single and multilayered liquids, with or without solids, from drums or similar containers, including those that are unstable, ruptured, or otherwise compromised. Special handling procedures (for example, remote drum opening, over-pressurized drum opening, drum deheading, etc.) are described in Drum Handling Practices at Hazardous Waste Sites.
SCOPE
1.1 This practice covers typical equipment and methods for collecting samples of single or multilayered liquids, with or without solids, in drums or similar containers. These methods are adapted specifically for sampling drums having a volume of 110 gal (416 L) or less. These methods are applicable to hazardous material, product, or waste. Specific sample collection and handling requirements should be described in the site-specific work plan.
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in 7.2.4, 7.2.7.1, and Notes 1 and 2.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
- Standard6 pagesEnglish language
- Standard6 pagesEnglish language
SIGNIFICANCE AND USE
5.1 This practice is intended for use in the waste management industries to collect samples of unconsolidated waste from trucks. The sampling procedures described are general and should be used in conjunction with a site-specific work plan.
5.2 The purpose of collecting waste samples directly from a truck (rather than the waste source) is often to verify (usually with screening analyses) that the waste contained in the truck is the same or similar material from a waste source that has been previously characterized and approved for treatment or disposal, or both. Additionally, it may be a safer or logistically easier to sample the waste from a truck over the waste source.
SCOPE
1.1 This practice covers several methods for collecting waste samples from trucks. These methods are adapted specifically for sampling unconsolidated solid wastes in bulk loads using several types of sampling equipment.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. See Section 6 for specific precautionary statements.
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
- Standard4 pagesEnglish language
- Standard4 pagesEnglish language
SIGNIFICANCE AND USE
5.1 This practice is intended to assist field personnel in obtaining samples from tanks for laboratory analysis. The cost associated with sampling and analysis, along with other reasons, make it essential that samples be taken correctly before submitting them for chemical analysis, physical testing, or both. Incorrect sampling can invalidate resulting data.
5.2 This practice provides guidance in choosing the sampling technique and equipment suitable for specific situations. It is recommended that this guide be used as a supplement to a written field sampling plan.
5.3 The procedures for sampling tanks using a COLIWASA, liquid profiler sampler, bacon bomb sampler, and peristaltic pump and tubing are delineated.
SCOPE
1.1 This practice covers information for field personnel to follow in order to collect samples from tanks.
1.2 The purpose of this practice is to help field personnel in planning and obtaining samples from vertical and horizontal tanks, open-topped rectangular/square tanks, railroad and truck tankers, vacuum trucks, and tanks with multiple compartments using equipment and techniques that will assist in meeting the sampling objectives.
1.3 The practice is applicable to hazardous materials, products, raw materials, by-product, or waste.
1.4 Sampling from circulating pump discharge valves and tank transfer lines is not addressed in this practice.
1.5 Units—The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
- Standard6 pagesEnglish language
- Standard6 pagesEnglish language
SIGNIFICANCE AND USE
5.1 This guide describes sample collection and handling procedures designed to minimize losses of VOCs. The principal mechanisms for the loss of VOCs from materials during collection, handling, and storage are volatilization and biodegradation. Susceptibility of various VOCs to these two loss mechanisms is both compound and matrix specific. In general, compounds with higher vapor pressures are more susceptible to volatilization than compounds with lower vapor pressures. Also, aerobically degradable compounds are generally more susceptible to biodegradation than anaerobically degradable compounds. In some cases, the formation of other compounds not originally present in the material can occur. Loss or gain of VOCs leads to analytical results that are unrepresentative of field conditions.
5.2 Ancillary information concerning sample collection, handling, and storage for VOC analysis is provided in Appendix X1 – Appendix X3. These appendixes and cited references are recommended reading for those unfamiliar with the many challenges presented during the collection, handling, and storage of samples for VOC analysis.
SCOPE
1.1 This guide describes recommended procedures for the collection, handling, and preparation of solid waste, soil, and sediment samples for subsequent determination of volatile organic compounds (VOCs). This class of compounds includes low molecular weight aromatics, hydrocarbons, halogenated hydrocarbons, ketones, acetates, nitriles, acrylates, ethers, and sulfides with boiling points below 200° Celsius (C) that are insoluble or slightly soluble in water.
1.2 Methods of sample collection, handling, storage, and preparation for analysis are described.
1.3 This guide does not cover the details of sampling design, laboratory preparation of containers, and the analysis of the samples.
1.4 It is recommended that this guide be used in conjunction with Guide D4687.
1.5 This guide offers an organized collection of information or a series of options and does not recommend a specific course of action. This document cannot replace education or experience and should be used in conjunction with professional judgment. Not all aspects of this guide may be applicable in all circumstances. This ASTM standard is not intended to represent or replace the standard of care by which the adequacy of a given professional service must be judged, nor should this document be applied without consideration of a project’s many unique aspects. The word “standard” in the title of this document means only that the document has been approved through the ASTM consensus process.
1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. Reporting of test results in units other than SI shall not be regarded as nonconformance with this standard.
1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
- Guide16 pagesEnglish language
- Guide16 pagesEnglish language
SIGNIFICANCE AND USE
5.1 The quality of ground water has become an issue of national concern. Ground-water monitoring wells are one of the more important tools for evaluating the quality of ground water, delineating contamination plumes, and establishing the integrity of hazardous material management facilities.
5.2 The goal in sampling ground-water monitoring wells is to obtain samples that meet the DQOs. This guide discusses the advantages and disadvantages of various well sampling methods, equipment, and sample preservation techniques. It reviews the variables that need to be considered in developing a valid sampling plan.
SCOPE
1.1 This guide covers sampling equipment and procedures and “in the field” preservation, and it does not include well location, depth, well development, design and construction, screening, or analytical procedures that also have a significant bearing on sampling results. This guide is intended to assist a knowledgeable professional in the selection of equipment for obtaining representative samples from ground-water monitoring wells that are compatible with the formations being sampled, the site hydrogeology, and the end use of the data.
1.2 This guide is only intended to provide a review of many of the most commonly used methods for collecting ground-water quality samples from monitoring wells and is not intended to serve as a ground-water monitoring plan for any specific application. Because of the large and ever increasing number of options available, no single guide can be viewed as comprehensive. The practitioner must make every effort to ensure that the methods used, whether or not they are addressed in this guide, are adequate to satisfy the monitoring objectives at each site.
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are provided for information only.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
- Guide17 pagesEnglish language
SIGNIFICANCE AND USE
5.1 This guide is intended to assist field personnel in obtaining samples from drums and similar containers for field and laboratory analysis. The need for accurate data, and the costs associated with sampling and analysis, make it essential that samples be taken correctly before submitting them for chemical analysis or physical testing, or both. Incorrect sampling can invalidate resulting data.
5.2 This guide may be used by personnel who have no formal workplan. It draws their attention to issues that must be addressed before, during, and after taking a sample. It provides guidance in choosing the sampling technique and equipment suitable for specific situations. It can serve as a training tool for those who are unfamiliar with sampling. It is recommended that this guide be used as a supplement to a written workplan.
5.3 Some sections of this guide contain flow charts (see Figs. 1-5) that must be worked through, starting from the top of each page. By answering the questions in the diamond-shaped boxes, and following the appropriate arrows, the person planning to sample will be guided toward the most suitable procedures and equipment. The numbers at the bottom of some boxes refer to corresponding paragraphs in the text, which provide information to help the person sampling answer the questions.
FIG. 8 COLIWASA
FIG. 9 Concentric Tube Thief
FIG. 10 Dipper
FIG. 11 Drum Thief
FIG. 12 Peristaltic Pumps
FIG. 13 Scoop, Spoon, Trowel
FIG. 14 Syringe Sampler
FIG. 15 Trier
SCOPE
1.1 This guide covers information, including flow charts, for field personnel to follow in order to collect samples from drums and similar containers.
1.2 The purpose of this guide is to help field personnel in planning and obtaining samples from drums and similar containers, using equipment and techniques that will ensure that the objectives of the sampling activity will be met. It can also be used as a training tool.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. See specific warnings in 7.4.3 and 7.4.4.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
- Guide19 pagesEnglish language
SIGNIFICANCE AND USE
4.1 The procedure outlined in these practices are guides for obtaining descriptive samples of solid, semisolid, and liquid waste from flowing streams, and incorporate many of the same procedures and equipment covered in the Referenced Documents. These practices by themselves will not necessarily result in the collection of samples representative of the total waste mass. The degree to which samples describe a waste mass must be estimated by application of appropriate statistical methods and measures of quality assurance. It is recommended that those practices be used in conjunction with Guide D4687.
SCOPE
1.1 These practices provide guidance for obtaining samples of waste at discharge points from pipes, sluiceways, conduits, and conveyor belts. The following are included:
Sections
Practice A – Liquid or Slurry Discharges
Practice B – Solid or Semisolid Discharges
7–9
10–12
1.2 These practices are intended for situations in which there are no other applicable ASTM sampling methods (see Practices D140/D140M and D75/D75M) for the specific industry.
1.3 These practices do not address flow and time-proportional samplers and other automatic sampling devices.
1.4 Samples are taken from a flowing waste stream or moving waste mass and, therefore, are descriptive only within a certain period. The length of the period for which a sample is descriptive will depend on the sampling frequency and compositing scheme.
1.5 It is recommended that these practices be used in conjunction with Guide D4687.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. See Section 5 for more information.
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
- Standard4 pagesEnglish language
- Standard4 pagesEnglish language
SIGNIFICANCE AND USE
5.1 Wipe sampling is typically used by persons involved in hazardous waste site investigations to characterize the areal extent and the level of contamination on walls, floors, equipment, etc. Wipe sampling is also used to determine compliance with regulations.
5.2 There are many factors that contribute to variation in sampling results during wipe sampling, including the use of different pressures applied to the wipe, different kinds of wipes, different wiping patterns, the texture of the surface being wiped, and perhaps even the duration of wiping. The significance of this practice is that it standardizes wiping procedures to reduce sampling variability in the collection of samples from smooth, nonporous surfaces such as metal, glass, painted or sealed surfaces, tile, etc., in and around buildings and from pipes, tanks, decontaminated equipment, etc.
SCOPE
1.1 This practice addresses sampling of organic compounds (that is, PCBs, dioxins, many pesticides and similar compounds) from smooth nonporous surfaces using a solvent-wetted wipe sampling method. Samples are collected in a manner that permits the solvent extraction of the organic compound(s) of interest from the wipes and subsequent determination using a laboratory analysis technique such as gas chromatography with a suitable detector. This practice is, however, unsuitable for the collection of volatile organic compounds.
1.2 This practice should only be used to collect samples for the determination of organic compound(s) on a loading basis (for example, mass per unit area). It cannot be used to collect samples for the determination of organic compounds on a concentration basis (for example, mass per unit mass).
1.3 This wipe sampling practice is not recommended for collecting samples of organic compounds from rough or porous surfaces such as upholstery, carpeting, brick, rough concrete, ceiling tiles, and bare wood. It is also not intended for the collection of dust samples (see Guide E1278) or sampling to estimate human exposure to contaminated surfaces.
1.4 To ensure valid conclusions are reached, a sufficient number of samples must be obtained as directed by a sampling design (the number and location of samples including quality control samples) and a quality assurance/quality control plan. This practice does not address the sampling designs used to achieve the data quality objectives (see Practice D5792).
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
- Standard3 pagesEnglish language
- Standard3 pagesEnglish language
SIGNIFICANCE AND USE
5.1 This practice is intended for use in collecting samples of consolidated or compacted materials from drums or similar containers, but only in compliance with a suitable work plan prepared according to Practice D5283 and Guide D4687. If the plan so provides, samples may be collected from drums not intended to be opened and from drums that are unstable, ruptured or otherwise compromised. Special handling procedures (for example, remote drum opening, overpressurized drum opening, drum deheading, etc.) are described in Drum Handling Practices at Hazardous Waste Sites.
SCOPE
1.1 This practice covers typical equipment and methods for collecting samples of consolidated solids in drums or similar containers. These methods are adapted specifically for sampling drums having a volume of 110 U.S. gal (416 L) or less. These methods are applicable to hazardous material, product, or waste. Specific sample collection and handling requirements should be described in the site-specific work plan.
1.2 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
- Standard5 pagesEnglish language
- Standard5 pagesEnglish language
SIGNIFICANCE AND USE
4.1 The procedure outlined in these practices are guides for obtaining descriptive samples of solid, semisolid and liquid waste from flowing streams, and incorporate many of the same procedures and equipment covered in the Referenced Documents. These practices by themselves will not necessarily result in the collection of samples representative of the total waste mass. The degree to which samples describe a waste mass must be estimated by application of appropriate statistical methods and measures of quality assurance. It is recommended that those practices be used in conjunction with Guide D4687.
SCOPE
1.1 These practices provide guidance for obtaining samples of waste at discharge points from pipes, sluiceways, conduits, and conveyor belts. The following are included:
Sections
Practice A—Liquid or Slurry Discharges
Practice B—Solid or Semisolid Discharges
7 through 9
10 through 12
1.2 These practices are intended for situations in which there are no other applicable ASTM sampling methods (see Practices D140 and D75) for the specific industry.
1.3 These practices do not address flow and time-proportional samplers and other automatic sampling devices.
1.4 Samples are taken from a flowing waste stream or moving waste mass and, therefore, are descriptive only within a certain period. The length of the period for which a sample is descriptive will depend on the sampling frequency and compositing scheme.
1.5 It is recommended that these practices be used in conjunction with Guide D4687.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See Section 5 for more information.
- Standard4 pagesEnglish language
- Standard4 pagesEnglish language
SIGNIFICANCE AND USE
4.1 This practice can be used in sampling ash from a kiln or incinerator, soils, and process waste from conveying systems, such as, a conveyer and vertical lifts. Some slurries, such as the bottom solids, can be sampled from the quench waters at the end of a kiln.
4.2 This practice can be used to determine material balances for burner efficiency studies and compliance studies.
4.3 This practice can be used on lifts, sloping, and horizontal conveyor systems. The type of conveyor and the amount and type of sample required will dictate the type of sampling equipment required to get a representative sample.
4.4 The sample is taken directly from the conveyor before emptying into the waste container or pile for disposal or recycling using a scoop, dipper, or shovel depending upon the sample requirements (see Practice D5633). The sample is then put into the sample container for analysis.
4.5 The place, quantity, frequency, and time of sampling is dependent upon the conveying system equipment, data quality objectives (DQOs) (Practice D5792), work or sampling plan (See Practice D5283 and Guide D4687), and analysis to be run.
4.5.1 Large particles can be mechanically excluded on a belt system. Large particles may accumulate at the bottom of an inclined/sloped belt system. Therefore, steps, if possible, need to be taken so that particles of all sizes have equal chances of being sampled.
4.5.2 The number of samples and sample time is dependent upon the system, the precision required, the decisions that are to be made, the cost, and the degree of heterogeneity of the material (see Guide D5956, Practice D6250, and Guide D6311).
4.5.3 In general, the ideal sampling location is nearest to the point of generation since temperature, oxidation, and air movement may change some samples with time.
4.6 The practice does not address issues related to the heterogeneity of the sample.
SCOPE
1.1 This practice describes standard procedures for sampling waste on open and closed conveying systems and is applicable to any waste material that can be conveyed to a waste pile or container. The conveyor system can be a vertical (vertical lifts), sloped or horizontal type.
1.2 This practice is intended for particles and slurries, which can be sampled using scoop, dipper, or shovel type samplers.
1.3 The practice is not intended for large size sample constituents, such as boulders, large rocks, and debris.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
- Standard4 pagesEnglish language
- Standard4 pagesEnglish language
- Standard4 pagesEnglish language
SIGNIFICANCE AND USE
5.1 This guide describes sample collection and handling procedures designed to minimize losses of VOCs. The principal mechanisms for the loss of VOCs from materials during collection, handling and storage are volatilization and biodegradation. Susceptibility of various VOCs to these two loss mechanisms is both compound and matrix specific. In general, compounds with higher vapor pressures are more susceptible to volatilization than compounds with lower vapor pressures. Also, aerobically degradable compounds are generally more susceptible to biodegradation than anaerobically degradable compounds. In some cases, the formation of other compounds not originally present in the material can occur. Loss or gain of VOCs leads to analytical results that are unrepresentative of field conditions.
5.2 Ancillary information concerning sample collection, handling and storage for VOC analysis is provided in Appendix X1, Appendix X2, and Appendix X3. These appendixes and cited references are recommended reading for those unfamiliar with the many challenges presented during the collection, handling and storage of samples for VOC analysis.
SCOPE
1.1 This guide describes recommended procedures for the collection, handling, and preparation of solid waste, soil, and sediment samples for subsequent determination of volatile organic compounds (VOCs). This class of compounds includes low molecular weight aromatics, hydrocarbons, halogenated hydrocarbons, ketones, acetates, nitriles, acrylates, ethers, and sulfides with boiling points below 200° Celsius (C) that are insoluble or slightly soluble in water.
1.2 Methods of sample collection, handling, storage, and preparation for analysis are described.
1.3 This guide does not cover the details of sampling design, laboratory preparation of containers, and the analysis of the samples.
1.4 It is recommended that this guide be used in conjunction with Guide D4687.
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
- Guide15 pagesEnglish language
- Guide15 pagesEnglish language
SIGNIFICANCE AND USE
5.1 This practice is intended for use in collecting samples of unconsolidated solid materials from drums or similar containers, including those that are unstable, ruptured, or compromised otherwise. Special handling procedures (for example, remote drum opening, over pressurized drum opening, drum deheading, etc.) are described in EPA/600/2-86/013 Drum Handling Practices at Hazardous Waste Sites.
SCOPE
1.1 This practice covers typical equipment and methods for collecting samples of unconsolidated solids in drums or similar containers. These methods are adapted specifically for sampling drums having a volume of 110 U.S. gal (416 L) or less. These methods are applicable to hazardous material, product, or waste. Specific sample collection and handling requirements should be described in the site-specific work plan.
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
- Standard6 pagesEnglish language
- Standard6 pagesEnglish language
SIGNIFICANCE AND USE
5.1 This practice is intended for use in collecting samples of single and multilayered liquids, with or without solids, from drums or similar containers, including those that are unstable, ruptured, or otherwise compromised. Special handling procedures (for example, remote drum opening, overpressurized drum opening, drum deheading, etc.) are described in Drum Handling Practices at Hazardous Waste Sites.
SCOPE
1.1 This practice covers typical equipment and methods for collecting samples of single or multilayered liquids, with or without solids, in drums or similar containers. These methods are adapted specifically for sampling drums having a volume of 110 gal (416 L) or less. These methods are applicable to hazardous material, product, or waste. Specific sample collection and handling requirements should be described in the site-specific work plan.
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in 7.2.7.1 and Notes 1 and 2.
- Standard6 pagesEnglish language
SIGNIFICANCE AND USE
5.1 This practice is intended for use in the waste management industries to collect samples of unconsolidated waste from trucks. The sampling procedures described are general and should be used in conjunction with a site-specific work plan.
5.2 The purpose of collecting waste samples directly from a truck (rather than the waste source) is to verify (usually with screening analyses) that the waste contained in the truck is the same or similar material from a waste source that has been previously characterized and approved for treatment or disposal, or both.
SCOPE
1.1 This practice covers several methods for collecting waste samples from trucks. These methods are adapted specifically for sampling unconsolidated solid wastes in bulk loads using several types of sampling equipment.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See Section 6 for specific precautionary statements.
- Standard4 pagesEnglish language
- Standard4 pagesEnglish language
SIGNIFICANCE AND USE
5.1 The quality of ground water has become an issue of national concern. Ground-water monitoring wells are one of the more important tools for evaluating the quality of ground water, delineating contamination plumes, and establishing the integrity of hazardous material management facilities.
5.2 The goal in sampling ground-water monitoring wells is to obtain samples that meet the DQOs. This guide discusses the advantages and disadvantages of various well sampling methods, equipment, and sample preservation techniques. It reviews the variables that need to be considered in developing a valid sampling plan.
SCOPE
1.1 This guide covers sampling equipment and procedures and “in the field” preservation, and it does not include well location, depth, well development, design and construction, screening, or analytical procedures that also have a significant bearing on sampling results.This guide is intended to assist a knowledgeable professional in the selection of equipment for obtaining representative samples from ground-water monitoring wells that are compatible with the formations being sampled, the site hydrogeology, and the end use of the data.
1.2 This guide is only intended to provide a review of many of the most commonly used methods for collecting ground-water quality samples from monitoring wells and is not intended to serve as a ground-water monitoring plan for any specific application. Because of the large and ever increasing number of options available, no single guide can be viewed as comprehensive. The practitioner must make every effort to ensure that the methods used, whether or not they are addressed in this guide, are adequate to satisfy the monitoring objectives at each site.
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are provided for information only.
1.4 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
- Guide17 pagesEnglish language
SIGNIFICANCE AND USE
5.1 This practice is intended to assist field personnel in obtaining samples from tanks for laboratory analysis. The cost associated with sampling and analysis make it essential that samples be taken correctly before submitting them for chemical analysis, physical testing, or both. Incorrect sampling can invalidate resulting data.
5.2 This practice provides guidance in choosing the sampling technique and equipment suitable for specific situations. It is recommended that this guide be used as a supplement to a written field sampling plan.
5.3 The procedures for sampling tanks using a COLIWASA, liquid profiler sampler, Bacon Bomb sampler, and peristaltic pump and tubing are delineated.
SCOPE
1.1 This practice covers information for field personnel to follow in order to collect samples from tanks.
1.2 The purpose of this practice is to help field personnel in planning and obtaining samples from vertical and horizontal tanks, open-topped rectangular/square tanks, railroad and truck tankers, vacuum trucks and tanks with multiple compartments using equipment and techniques that will assist in meeting the sampling objectives.
1.3 The practice is applicable to hazardous materials, products, raw materials, by-product, or waste.
1.4 Sampling from circulating pump discharge valves and tank transfer lines are not addressed in this practice.
1.5 Units—The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
- Standard7 pagesEnglish language
SIGNIFICANCE AND USE
5.1 This practice is intended for use in collecting samples of consolidated or compacted materials from drums or similar containers, including those that are unstable, ruptured, or compromised otherwise. Special handling procedures (for example, remote drum opening, overpressurized drum opening, drum deheading, etc.) are described in Drum Handling Practices at Hazardous Waste Sites.
SCOPE
1.1 This practice covers typical equipment and methods for collecting samples of consolidated solids in drums or similar containers. These methods are adapted specifically for sampling drums having a volume of 110 U.S. gal (416 L) or less. These methods are applicable to hazardous material, product, or waste. Specific sample collection and handling requirements should be described in the site-specific work plan.
1.2 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
- Standard5 pagesEnglish language
SCOPE
1.1 This guide covers information, including flow charts, for field personnel to follow in order to collect samples from drums and similar containers.
1.2 The purpose of this guide is to help field personnel in planning and obtaining samples from drums and similar containers, using equipment and techniques that will ensure that the objectives of the sampling activity will be met. It can also be used as a training tool.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See specific Warnings in 7.4.3 and 7.4.4.
- Guide19 pagesEnglish language
- Guide19 pagesEnglish language
SIGNIFICANCE AND USE
Wipe sampling is typically used by persons involved in hazardous waste site investigations to characterize the areal extent and the level of contamination on walls, floors, equipment, etc. Wipe sampling is also used to determine compliance with regulations.
There are many factors that contribute to variation in sampling results during wipe sampling including, the use of different pressures applied to the wipe, different kinds of wipes, different wiping patterns, the texture of the surface being wiped, and perhaps even the duration of wiping. The significance of this practice is that it standardizes wiping procedures to reduce sampling variability in the collection of samples from smooth, nonporous surfaces such as metal, glass, painted or sealed surfaces, tile, etc., in and around buildings, and from pipes, tanks, decontaminated equipment, etc.
SCOPE
1.1 This practice addresses sampling of organic compounds (i.e., PCBs, dioxins, many pesticides and similar compounds) from smooth nonporous surfaces using a solvent-wetted wipe sampling method. Samples are collected in a manner that permits the solvent extraction of the organic compound(s) of interest from the wipes and subsequent determination using a laboratory analysis technique such as gas chromatography with a suitable detector. This practice is, however, unsuitable for the collection of volatile organic compounds.
1.2 This practice should only be used to collect samples for the determination of organic compound(s) on a loading basis (e.g., mass per unit area). It cannot be used to collect samples for the determination of organic compounds on a concentration basis (e.g., mass per unit mass).
1.3 This wipe sampling practice is not recommended for collecting samples of organic compounds from rough or porous surfaces such as upholstery, carpeting, brick, rough concrete, ceiling tiles, and bare wood. It is also not intended for the collection of dust samples (see Practice E1278) or sampling to estimating human exposure to contaminated surfaces.
1.4 To ensure valid conclusions are reached, a sufficient number of samples must be obtained as directed by a sampling design (the number and location of samples including quality control samples) and a quality assurance/quality control plan. This practice does not address the sampling designs used to achieve the data quality objectives (see Practice D5792).
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
- Standard3 pagesEnglish language
- Standard3 pagesEnglish language
SIGNIFICANCE AND USE
This practice is intended for use in collecting samples of unconsolidated solid materials from drums or similar containers, including those that are unstable, ruptured, or compromised otherwise. Special handling procedures (for example, remote drum opening, over pressurized drum opening, drum deheading, etc.) are described in EPA/600/2-86/013 Drum Handling Practices at Hazardous Waste Sites.
SCOPE
1.1 This practice covers typical equipment and methods for collecting samples of unconsolidated solids in drums or similar containers. These methods are adapted specifically for sampling drums having a volume of 110 U.S. gal (416 L) or less. These methods are applicable to hazardous material, product, or waste. Specific sample collection and handling requirements should be described in the site-specific work plan.
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
- Standard6 pagesEnglish language
- Standard6 pagesEnglish language
SIGNIFICANCE AND USE
This guide describes sample collection and handling procedures designed to minimize losses of VOCs. The principal mechanisms for the loss of VOCs from materials during collection, handling and storage are volatilization and biodegradation. Susceptibility of various VOCs to these two loss mechanisms is both compound and matrix specific. In general, compounds with higher vapor pressures are more susceptible to volatilization than compounds with lower vapor pressures. Also, aerobically degradable compounds are generally more susceptible to biodegradation than anaerobically degradable compounds. In some cases, the formation of other compounds not originally present in the material can occur. Loss or gain of VOCs leads to analytical results that are unrepresentative of field conditions.
Ancillary information concerning sample collection, handling and storage for VOC analysis is provided in Appendices Appendix X1, Appendix X2, and Appendix X3. These appendixes and cited references are recommended reading for those unfamiliar with the many challenges presented during the collection, handling and storage of samples for VOC analysis.
SCOPE
1.1 This guide describes recommended procedures for the collection, handling, and preparation of solid waste, soil, and sediment samples for subsequent determination of volatile organic compounds (VOCs). This class of compounds includes low molecular weight aromatics, hydrocarbons, halogenated hydrocarbons, ketones, acetates, nitriles, acrylates, ethers, and sulfides with boiling points below 200° Celsius (C) that are insoluble or slightly soluble in water.
1.2 Methods of sample collection, handling, storage, and preparation for analysis are described.
1.3 This guide does not cover the details of sampling design, laboratory preparation of containers, and the analysis of the samples.
1.4 It is recommended that this guide be used in conjunction with Guide D 4687.
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
- Standard15 pagesEnglish language
- Standard15 pagesEnglish language
SIGNIFICANCE AND USE
The procedure outlined in these practices are guides for obtaining descriptive samples of solid, semisolid and liquid waste from flowing streams, and incorporate many of the same procedures and equipment covered in the Referenced Documents. These practices by themselves will not necessarily result in the collection of samples representative of the total waste mass. The degree to which samples describe a waste mass must be estimated by application of appropriate statistical methods and measures of quality assurance. It is recommended that those practices be used in conjunction with Guide D 4687.
SCOPE
1.1 Those practices provide guidance for obtaining samples of waste at discharge points from pipes, sluiceways, conduits, and conveyor belts. The following are included:
Sections Practice A—Liquid or Slurry Discharges
Practice B—Solid or Semisolid Discharges7 through 9
10 through 12
1.2 These practices are intended for situations in which there are no other applicable ASTM sampling methods (see Practices D 140 and D 75) for the specific industry.
1.3 These practices do not address flow and time-proportional samplers and other automatic sampling devices.
1.4 Samples are taken from a flowing waste stream or moving waste mass and, therefore, are descriptive only within a certain period. The length of the period for which a sample is descriptive will depend on the sampling frequency and compositing scheme.
1.5 It is recommended that these practices be used in conjunction with Guide D 4687.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See Section 5 for more information.
- Standard3 pagesEnglish language
SIGNIFICANCE AND USE
This practice is intended for use in collecting samples of single and multilayered liquids, with or without solids, from drums or similar containers, including those that are unstable, ruptured, or otherwise compromised. Special handling procedures (for example, remote drum opening, overpressurized drum opening, drum deheading, etc.) are described in Drum Handling Practices at Hazardous Waste Sites.
SCOPE
1.1 This practice covers typical equipment and methods for collecting samples of single or multilayered liquids, with or without solids, in drums or similar containers. These methods are adapted specifically for sampling drums having a volume of 110 gal (416 L) or less. These methods are applicable to hazardous material, product, or waste. Specific sample collection and handling requirements should be described in the site-specific work plan.
1.2 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in 7.2.7.1 and Notes 1 and 2.
- Standard6 pagesEnglish language
SIGNIFICANCE AND USE
The quality of ground water has become an issue of national concern. Ground-water monitoring wells are one of the more important tools for evaluating the quality of ground water, delineating contamination plumes, and establishing the integrity of hazardous material management facilities.
The goal in sampling ground-water monitoring wells is to obtain samples that meet the DQOs. This guide discusses the advantages and disadvantages of various well sampling methods, equipment, and sample preservation techniques. It reviews the variables that need to be considered in developing a valid sampling plan.
SCOPE
1.1 This guide covers sampling equipment and procedures and "in the field" preservation, and it does not include well location, depth, well development, design and construction, screening, or analytical procedures that also have a significant bearing on sampling results.This guide is intended to assist a knowledgeable professional in the selection of equipment for obtaining representative samples from ground-water monitoring wells that are compatible with the formations being sampled, the site hydrogeology, and the end use of the data.
1.2 This guide is only intended to provide a review of many of the most commonly used methods for collecting ground-water quality samples from monitoring wells and is not intended to serve as a ground-water monitoring plan for any specific application. Because of the large and ever increasing number of options available, no single guide can be viewed as comprehensive. The practitioner must make every effort to ensure that the methods used, whether or not they are addressed in this guide, are adequate to satisfy the monitoring objectives at each site.
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are provided for information only.
This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
- Guide17 pagesEnglish language
SIGNIFICANCE AND USE
This practice can be used in sampling ash from a kiln or incinerator, soils, and process waste from conveying systems, such as, a conveyer and vertical lifts. Some slurries, such as the bottom solids, can be sampled from the quench waters at the end of a kiln.
This practice can be used to determine material balances for burner efficiency studies and compliance studies.
This practice can be used on lifts, sloping, and horizontal conveyor systems. The type of conveyor and the amount and type of sample required will dictate the type of sampling equipment required to get a representative sample.
The sample is taken directly from the conveyor before emptying into the waste container or pile for disposal or recycling using a scoop, dipper, or shovel depending upon the sample requirements (see Practice D 5633). The sample is then put into the sample container for analysis.
The place, quantity, frequency, and time of sampling is dependent upon the conveying system equipment, DQOs (Practice D 5792), work or sampling plan (See Practice D 5283 and Guide D 4687), and analysis to be run.
4.5.1 Large particles can be mechanically excluded on a belt system. Large particles may accumulate at the bottom of an inclined/sloped belt system. Therefore, steps, if possible, need to be taken so that particles of all sizes have equal chances of being sampled.
4.5.2 The number of samples and sample time is dependent upon the system, the precision required, the decisions that are to be made, the cost, and the degree of heterogeneity of the material (see Guide D 5956, Practice D 6250, and Guide D 6311).
4.5.3 In general, the ideal sampling location is nearest to the point of generation since temperature, oxidation, and air movement may change some samples with time.
The practice does not address issues related to the heterogeneity of the sample.
SCOPE
1.1 This practice describes standard procedures for sampling waste on open and closed conveying systems and is applicable to any waste material that can be conveyed to a waste pile or container. The conveyor system can be a vertical (vertical lifts), sloped or horizontal type.
1.2 This practice is intended for particles and slurries, which can be sampled using scoop, dipper or shovel type samplers.
1.3 The practice is not intended for large size sample constituents, such as boulders, large rocks, and debris.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
- Standard3 pagesEnglish language
SIGNIFICANCE AND USE
This practice is intended for use in collecting samples of consolidated or compacted materials from drums or similar containers, including those that are unstable, ruptured, or compromised otherwise. Special handling procedures (for example, remote drum opening, overpressurized drum opening, drum deheading, etc.) are described in Drum Handling Practices at Hazardous Waste Sites.
SCOPE
1.1 This practice covers typical equipment and methods for collecting samples of consolidated solids in drums or similar containers. These methods are adapted specifically for sampling drums having a volume of 110 U.S. gal (416 L) or less. These methods are applicable to hazardous material, product, or waste. Specific sample collection and handling requirements should be described in the site-specific work plan.
1.2 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
- Standard5 pagesEnglish language
SCOPE
1.1 This guide covers information, including flow charts, for field personnel to follow in order to collect samples from drums and similar containers.
1.2 The purpose of this guide is to help field personnel in planning and obtaining samples from drums and similar containers, using equipment and techniques that will ensure that the objectives of the sampling activity will be met. It can also be used as a training tool.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See specific Warnings in 7.4.3 and 7.4.4.
- Guide19 pagesEnglish language
SIGNIFICANCE AND USE
This practice is intended for use in the waste management industries to collect samples of unconsolidated waste from trucks. The sampling procedures described are general and should be used in conjunction with a site-specific work plan.
The purpose of collecting waste samples directly from a truck (rather than the waste source) is to verify (usually with screening analyses) that the waste contained in the truck is the same or similar material from a waste source that has been previously characterized and approved for treatment or disposal, or both.
SCOPE
1.1 This practice covers several methods for collecting waste samples from trucks. These methods are adapted specifically for sampling unconsolidated solid wastes in bulk loads using several types of sampling equipment.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See Section 6 for specific precautionary statements.
- Standard4 pagesEnglish language
SCOPE
1.1 This practice addresses sampling of organic compounds (i.e., PCBs, dioxins, many pesticides and similar compounds) from smooth nonporous surfaces using a solvent-wetted wipe sampling method. Samples are collected in a manner that permits the solvent extraction of the organic compound(s) of interest from the wipes and subsequent determination using a laboratory analysis technique such as gas chromatography with a suitable detector. This practice is, however, unsuitable for the collection of volatile organic compounds.
1.2 This practice should only be used to collect samples for the determination of organic compound(s) on a loading basis (e.g., mass per unit area). It cannot be used to collect samples for the determination of organic compounds on a concentration basis (e.g., mass per unit mass).
1.3 This wipe sampling practice is not recommended for collecting samples of organic compounds from rough or porous surfaces such as upholstery, carpeting, brick, rough concrete, ceiling tiles, and bare wood. It is also not intended for the collection of dust samples (see Practice E 1728) or sampling to estimating human exposure to contaminated surfaces.
1.4 To ensure valid conclusions are reached, a sufficient number of samples must be obtained as directed by a sampling design (the number and location of samples including quality control samples) and a quality assurance/quality control plan. This practice does not address the sampling designs used to achieve the data quality objectives (see Practice D 5792).
1.5 The values stated in SI units are to be regarded as the standard.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
- Standard3 pagesEnglish language
SIGNIFICANCE AND USE
Bacteria and fungi present in municipal solid wastes (as well as in other forms of waste) may become airborne as dusts during waste processing. Several investigations to determine the health significance of these microbiological aerosols have been hindered by the lack of standardized procedures for sampling airborne bacteria and fungi in an industrial environment and by the absence of standards for assessing their health significance. Because it is difficult to correlate airborne levels of bacteria and fungi with epidemiological data, this standard is designed to permit the formation of a data base to aid in the assessment of the health significance of airborne microorganisms. It is intended that the use of this practice will improve sampling precision and thereby facilitate comparisons between sampling results.
SCOPE
1.1 This practice covers sampling of airborne microorganisms at municipal solid-waste processing facilities, hereafter referred to as facilities. Investigators should consult Practice D 1357 for the general principles of conducting an air-sampling program.
1.2 This practice applies only to sampling airborne bacteria and fungi, not viruses. Since sampling airborne viruses is significantly more difficult than sampling bacteria and fungi, reliable methods of sampling viruses are not yet available.
- Standard5 pagesEnglish language
SIGNIFICANCE AND USE
This guide describes sample collection and handling procedures designed to minimize losses of VOCs. The principal mechanisms for the loss of VOCs from materials during collection, handling and storage are volatilization and biodegradation. Susceptibility of various VOCs to these two loss mechanisms is both compound and matrix specific. In general, compounds with higher vapor pressures are more susceptible to volatilization than compounds with lower vapor pressures. Also, aerobically degradable compounds are generally more susceptible to biodegradation than anaerobically degradable compounds. In some cases, the formation of other compounds not originally present in the material can occur. Loss or gain of VOCs leads to analytical results that are unrepresentative of field conditions.
Ancillary information concerning sample collection, handling and storage for VOC analysis is provided in Appendix X1 and Appendix X2. These appendixes and cited references are recommended reading for those unfamiliar with the many challenges presented during the collection, handling and storage of samples for VOC analysis.
SCOPE
1.1 This guide describes recommended procedures for the collection, handling, and preparation of solid waste, soil, and sediment samples for subsequent determination of volatile organic compounds (VOCs). This class of compounds includes low molecular weight aromatics, hydrocarbons, halogenated hydrocarbons, ketones, acetates, nitriles, acrylates, ethers, and sulfides with boiling points below 200 Celsius (C) that are insoluble or slightly soluble in water.
1.2 Methods of sample collection, handling, storage, and preparation for analysis are described.
1.3 This guide does not cover the details of sampling design, laboratory preparation of containers, and the analysis of the samples.
1.4 It is recommended that this guide be used in conjunction with Guide D 4687.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See and for specific warnings.
- Standard12 pagesEnglish language
SCOPE
1.1 This guide describes recommended procedures for the collection, handling, and preparation of solid waste, soil, and sediment samples for subsequent determination of volatile organic compounds (VOCs). This class of compounds includes low molecular weight aromatics, hydrocarbons, halogenated hydrocarbons, ketones, acetates, nitriles, acrylates, ethers, and sulfides with boiling points below 200° Celsius (C) that are insoluble or slightly soluble in water.
1.2 Methods of sample collection, handling, storage, and preparation for analysis are described.
1.3 This guide does not cover the details of sampling design, laboratory preparation of containers, and the analysis of the samples.
1.4 It is recommended that this guide be used in conjunction with Guide D 4687.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See 7.2 and 8.1.1 for specific warnings.
- Standard11 pagesEnglish language
SIGNIFICANCE AND USE
This practice is intended for use in collecting samples of single and multilayered liquids, with or without solids, from drums or similar containers, including those that are unstable, ruptured, or otherwise compromised. Special handling procedures (for example, remote drum opening, overpressurized drum opening, drum deheading, etc.) are described in Drum Handling Practices at Hazardous Waste Sites.
SCOPE
1.1 This practice covers typical equipment and methods for collecting samples of single or multilayered liquids, with or without solids, in drums or similar containers. These methods are adapted specifically for sampling drums having a volume of 110 gal (416 L) or less. These methods are applicable to hazardous material, product, or waste. Specific sample collection and handling requirements should be described in the site-specific work plan.
1.2 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in 7.2.7.1 and Notes 1 and 2.
- Standard6 pagesEnglish language
SCOPE
1.1 This guide covers sampling equipment and procedures and "in the field" preservation, and it does not include well location, depth, well development, design and construction, screening, or analytical procedures that also have a significant bearing on sampling results.This guide is intended to assist a knowledgeable professional in the selection of equipment for obtaining representative samples from ground-water monitoring wells that are compatible with the formations being sampled, the site hydrogeology, and the end use of the data.
1.2 This guide is only intended to provide a review of many of the most commonly used methods for collecting ground-water quality samples from monitoring wells and is not intended to serve as a ground-water monitoring plan for any specific application. Because of the large and ever increasing number of options available, no single guide can be viewed as comprehensive. The practitioner must make every effort to ensure that the methods used, whether or not they are addressed in this guide, are adequate to satisfy the monitoring objectives at each site.
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are provided for information only.
1.4 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
- Guide17 pagesEnglish language
SCOPE
1.1 This guide covers sampling equipment and procedures and "in the field" preservation, and it does not include well location, depth, well development, design and construction, screening, or analytical procedures that also have a significant bearing on sampling results.This guide is intended to assist a knowledgeable professional in the selection of equipment for obtaining representative samples from ground-water monitoring wells that are compatible with the formations being sampled, the site hydrogeology, and the end use of the data.
1.2 This guide is only intended to provide a review of many of the most commonly used methods for collecting ground-water quality samples from monitoring wells and is not intended to serve as a ground-water monitoring plan for any specific application. Because of the large and ever increasing number of options available, no single guide can be viewed as comprehensive. The practitioner must make every effort to ensure that the methods used, whether or not they are addressed in this guide, are adequate to satisfy the monitoring objectives at each site.
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are provided for information only.
1.4 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
- Guide17 pagesEnglish language
SCOPE
1.1 This practice addresses sampling of organic compounds (i.e., PCBs, dioxins, many pesticides and similar compounds) from smooth nonporous surfaces using a solvent-wetted wipe sampling method. Samples are collected in a manner that permits the solvent extraction of the organic compound(s) of interest from the wipes and subsequent determination using a laboratory analysis technique such as gas chromatography with a suitable detector. This practice is, however, unsuitable for the collection of volatile organic compounds.
1.2 This practice should only be used to collect samples for the determination of organic compound(s) on a loading basis (e.g., mass per unit area). It cannot be used to collect samples for the determination of organic compounds on a concentration basis (e.g., mass per unit mass).
1.3 This wipe sampling practice is not recommended for collecting samples of organic compounds from rough or porous surfaces such as upholstery, carpeting, brick, rough concrete, ceiling tiles, and bare wood. It is also not intended for the collection of dust samples (see Practice E1728) or sampling to estimating human exposure to contaminated surfaces.
1.4 To ensure valid conclusions are reached, a sufficient number of samples must be obtained as directed by a sampling design (the number and location of samples including quality control samples) and a quality assurance/quality control plan. This practice does not address the sampling designs used to achieve the data quality objectives (see Practice D5792).
1.5 The values stated in SI units are to be regarded as the standard.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
- Standard3 pagesEnglish language
SCOPE
1.1 This practice covers typical equipment and methods for collecting samples of unconsolidated solids in drums or similar containers. These methods are adapted specifically for sampling drums having a volume of 110 U.S. gal (416 L) or less. These methods are applicable to hazardous material, product, or waste. Specific sample collection and handling requirements should be described in the site-specific work plan.
1.2 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
- Standard5 pagesEnglish language
SCOPE
1.1 This practice covers several methods for collecting waste samples from trucks. These methods are adapted specifically for sampling unconsolidated solid wastes in bulk loads using several types of sampling equipment.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See Section 6 for specific precautionary statements.
- Standard4 pagesEnglish language
SCOPE
1.1 This guide covers information, including flow charts, for field personnel to follow in order to collect samples from drums and similar containers.
1.2 The purpose of this guide is to help field personnel in planning and obtaining samples from drums and similar containers, using equipment and techniques that will ensure that the objectives of the sampling activity will be met. It can also be used as a training tool.
1.3This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
- Guide18 pagesEnglish language
SIGNIFICANCE AND USE
This practice is intended for use in collecting samples of unconsolidated solid materials from drums or similar containers, including those that are unstable, ruptured, or compromised otherwise. Special handling procedures (for example, remote drum opening, overpressurized drum opening, drum deheading, etc.) are described in Drum Handling Practices at Hazardous Waste Sites.
SCOPE
1.1 This practice covers typical equipment and methods for collecting samples of unconsolidated solids in drums or similar containers. These methods are adapted specifically for sampling drums having a volume of 110 U.S. gal (416 L) or less. These methods are applicable to hazardous material, product, or waste. Specific sample collection and handling requirements should be described in the site-specific work plan.
1.2 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
- Standard5 pagesEnglish language
SCOPE
1.1 This practice covers sampling of airborne microorganisms at municipal solid-waste processing facilities, hereafter referred to as facilities. Investigators should consult Practice D1357 for the general principles of conducting an air-sampling program.
1.2 This practice applies only to sampling airborne bacteria and fungi, not viruses. Since sampling airborne viruses is significantly more difficult than sampling bacteria and fungi, reliable methods of sampling viruses are not yet available.
- Standard5 pagesEnglish language
SCOPE
1.1 This practice covers sampling of airborne microorganisms at municipal solid-waste processing facilities, hereafter referred to as facilities. Investigators should consult Practice D1357 for the general principles of conducting an air-sampling program.
1.2 This practice applies only to sampling airborne bacteria and fungi, not viruses. Since sampling airborne viruses is significantly more difficult than sampling bacteria and fungi, reliable methods of sampling viruses are not yet available.
- Standard5 pagesEnglish language
SCOPE
1.1 This guide covers information, including flow charts, for field personnel to follow in order to collect samples from drums and similar containers.
1.2 The purpose of this guide is to help field personnel in planning and obtaining samples from drums and similar containers, using equipment and techniques that will ensure that the objectives of the sampling activity will be met. It can also be used as a training tool.
1.3This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
- Guide18 pagesEnglish language
SCOPE
1.1 This practice covers several methods for collecting waste samples from trucks. These methods are adapted specifically for sampling unconsolidated solid wastes in bulk loads using several types of sampling equipment.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See Section 6 for specific precautionary statements.
- Standard4 pagesEnglish language
SCOPE
1.1 These test methods include descriptions for conducting and reporting throughput and electrical power tests on mechanical conveying equipment for municipal solid waste and recovered products from resource recovery systems. Other aspects of performance testing such as spillage, conveyor tracking, dusting, slippage, transfer points, etc., should be considered in the interpretation of the results. These test methods can be used on equipment handling raw refuse, processed refuse, magnetic scrap metals, nonferrous scrap metals, mixed glass, and residues or tailings. These test methods may also be used for materials in other industries.
1.2 These test methods cover mechanical conveying equipment including apron, belt, drag, flight, screw, slat, and vibrating conveyors and bucket elevators.
1.3 These test methods are applicable specifically to the resource recovery industry since municipal solid wastes are heterogeneous mixtures and the composition and bulk densities vary considerably depending on many factors. Because of the varying composition of municipal solid waste, a number of samples must be taken to determine accurately the performance of the mechanical conveying equipment.
1.4 Test Methods for determining the approximate as-conveyed bulk density of the material and for determining the electrical horsepower input of the equipment motors are also included.
1.5 It is intended that the tests be made and reported by personnel trained in the proper application and use of the various instruments and methods involved.
1.6 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.7 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For hazard statement, see Section 7.
- Standard5 pagesEnglish language
SCOPE
1.1 This practice describes field sampling of solid wastes for subsequent volatile organics analysis in the laboratory. This practice is also intended to apply to soils and sediments that may contain volatile waste constituents.
1.2 Both the collection of the sample and the method of containing the sample for shipment to the laboratory are considered.
1.3 This practice concerns only sampling methods to be used in the field; it does not cover laboratory preparation of containers or solutions or other laboratory techniques related to processing or analysis of the samples.
1.4 It is recommended that this standard be used in conjunction with Guide D4687.
1.5 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific precautionary statements, see Section 6.
- Standard10 pagesEnglish language
SCOPE
1.1 Those practices provide guidance for obtaining samples of waste at discharge points from pipes, sluiceways, conduits, and conveyor belts. The following are included: Sections Practice A---Liquid or Slurry Discharges 7 through 9 Practice B---Solid or Semisolid Discharges 10 through 12
1.2 These practices are intended for situations in which there are no other applicable ASTM sampling methods (see Practices D140 and D75) for the specific industry.
1.3 These practices do not address flow and time-proportional samplers and other automatic sampling devices.
1.4 Samples are taken from a flowing waste stream or moving waste mass and, therefore, are descriptive only within a certain period. The length of the period for which a sample is descriptive will depend on the sampling frequency and compositing scheme.
1.5 It is recommended that these practices be used in conjunction with ASTM Guide D4687.
1.6 This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See Section 5 for more information.
- Standard3 pagesEnglish language
Frequently Asked Questions
D34.01.02 is a Technical Committee within ASTM International. It is named "Sampling Techniques". This committee has published 55 standards.
D34.01.02 develops ASTM standards in the area of Information technology. Currently, there are 55 published standards from this technical committee.
ASTM is a standardization organization that develops and publishes standards to support industry, commerce, and regulatory requirements.
A Technical Committee (TC) in ASTM is a group of experts responsible for developing international standards in a specific technical area. TCs are composed of national member body delegates and work through consensus to create standards that meet global industry needs. Each TC may have subcommittees (SCs) and working groups (WGs) for specialized topics.