EN 15309:2007

Characterization of waste and soil - Determination of elemental composition by X-ray fluorescence

This European Standard specifies the procedure for a quantitative determination of major and trace element concentrations in homogeneous solid waste, soil and soil-like material by energy dispersive X-ray fluorescence (EDXRF) spectrometry or wavelength dispersive X-ray fluorescence (WDXRF) spectrometry using a calibration with matrix-matched standards.
This European Standard is applicable for the following elements: Na, Mg, Al, Si, P, S, Cl, K, Ca, Ti, V, Cr, Mn, Fe, Co, Ni, Cu, Zn, As, Se, Br, Rb, Sr, Y, Zr, Nb, Mo, Ag, Cd, Sn, Sb, Te, I, Cs, Ba, Ta, W, Hg, Tl, Pb, Bi, Th and U. Concentration levels between approximately 0,000 1 % and 100 % can be determined depending on the element and the instrument used.

Charakterisierung von Abfällen und Böden - Bestimmung der elementaren Zusammensetzung durch Röntgenfluoreszenz-Analyse

Caractérisation des déchets et du sol - Détermination de la composition élémentaire par fluorescence X

La présente norme européenne décrit le mode opératoire de détermination quantitative des concentrations en éléments majeurs et en éléments traces dans les sols, les matériaux de type sol et les déchets solides homogènes à l’aide de spectromètres de fluorescence X à dispersion d’énergie (EDXRF) ou de spectromètres de fluorescence X à dispersion de longueur d’onde (WDXRF), en utilisant un étalonnage réalisé avec des matériaux de référence adaptés à la matrice.
La présente norme européenne est applicable aux éléments suivants : Na, Mg, Al, Si, P, S, Cl, K, Ca, Ti, V, Cr, Mn, Fe, Co, Ni, Cu, Zn, As, Se, Br, Rb, Sr, Y, Zr, Nb, Mo, Ag, Cd, Sn, Sb, Te, I, Cs, Ba, Ta, W, Hg, Tl, Pb, Bi, Th et U. Il est possible de déterminer des niveaux de concentration compris entre 0,0001 % et 100 % selon l’élément dosé et l’instrument utilisé.

Karakterizacija odpadkov in zemljine - Določevanje elementne sestave z rentgensko fluorescenco

General Information

• Status: Published
• Publication Date: 08-May-2007
• Withdrawal Date: 29-Nov-2007
• ICS: 13.030.10 - Solid wastes
• ICS: 13.080.10 - Chemical characteristics of soils
• Technical Committee: CEN/TC 444 - Environmental characterization
• Drafting Committee: CEN/TC 444/WG 3 - Inorganic analysis
• Current Stage: 9093 - Decision to confirm - Review Enquiry
• Completion Date: 17-May-2018
• Directive: 99/31/EC - Landfill of waste
• Ref Project: SIST EN 15309:2007 - Characterization of waste and soil - Determination of elemental composition by X-ray fluorescence

Standards Content (Sample)

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Characterization of waste and soil - Determination of elemental composition by X-ray fluorescenceCaractérisation des déchets et du sol - Détermination de la composition élémentaire par fluorescence XCharakterisierung von Abfällen und Böden - Bestimmung der elementaren Zusammensetzung durch Röntgenfluoreszenz-AnalyseTa slovenski standard je istoveten z:EN 15309:2007SIST EN 15309:2007en13.080.10Chemical characteristics of soils13.030.10Trdni odpadkiSolid wastesICS:SLOVENSKI
STANDARDSIST EN 15309:200701-oktober-2007







EUROPEAN STANDARDNORME EUROPÉENNEEUROPÄISCHE NORMEN 15309May 2007ICS 13.030.10; 13.080.10 English VersionCharacterization of waste and soil - Determination of elementalcomposition by X-ray fluorescenceCaractérisation des déchets et du sol - Détermination de lacomposition élémentaire par fluorescence XCharakterisierung von Abfällen und Böden - Bestimmungder elementaren Zusammensetzung durchRöntgenfluoreszenz-AnalyseThis European Standard was approved by CEN on 22 March 2007.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained on application to the CEN Management Centre or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as theofficial versions.CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland,France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMITÉ EUROPÉEN DE NORMALISATIONEUROPÄISCHES KOMITEE FÜR NORMUNGManagement Centre: rue de Stassart, 36
B-1050 Brussels© 2007 CENAll rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN 15309:2007: E



EN 15309:2007 (E) 2 Contents Page Foreword.3 Introduction.4 1 Scope.5 2 Normative references.5 3 Terms and definitions.5 4 Safety remarks.7 5 Principle.7 6 Apparatus.7 7 Reagents.8 8 Interferences and sources of error.8 9 Sample preparation.9 9.1 General.9 9.2 Drying and determination of dry mass.9 9.3 Preparation of pressed pellet.9 9.4 Preparation of fused beads.10 10 Procedure.10 10.1 Analytical measurement conditions.
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