Guidelines for the checking and treatment of sulphur hexafluoride (SF6) taken from electrical equipment and specification for its re-use

Concerns the re-use of sulfur hexafluoride (SF6) after removal from electrical equipment (for maintenance, or at the end of life). This standard recommends procedures for reclaiming used SF6 and for restoring its quality to an acceptable level, which would allow the filling of new or existing electrical equipment. This standard provides guidance to operational and maintenance personnel for the testing and safe handling of used SF6 . The main changes with respect to the previous edition are listed below: - updating of standard as it relates to environmental issues, storage and analytical methods; - addition of specification for the re-use of gas; - inclusion of a regeneration process for sulfur hexafluoride taken from electrical equipment.

Richtlinien für die Prüfung und Aufbereitung von Schwefelhexafluorid (SF6) nach Entnahme aus elektrischen Betriebsmitteln und Spezifikation für dessen Wiederverwendung

Lignes directrices relatives au contrôle et au traitement de l'hexafluorure de soufre (SF6) prélevé sur le matériel électrique et spécification en vue de sa réutilisation

Concerne l'hexafluorure de soufre (SF6) que l'on retire du matériel électrique (pour la maintenance ou en fin de vie) en vue de sa réutilisation. La présente norme recommande des procédures pour la régénération du SF6 usagé et pour la restauration de sa qualité à un niveau acceptable, afin de permettre le remplissage de nouveaux matériels électriques ou de matériels déjà existants. La présente norme fournit des lignes directrices pour que le personnel d'exploitation ou de maintenance réalise des essais ou traite le SF6 usagé en toute sécurité. Les modifications principales par rapport à l'édition précédente sont indiquées ci-dessous: - mise à jour des questions environnementales, de stockage et des méthodes analytiques; - addition de spécification pour la réutilisation du gaz; - incorporation du processus de régénération de l'hexafluorure de soufre prélevé sur le matériel électrique.

Smernice za preverjanje in ravnanje z žveplovim heksafluoridom (SF6) iz električne opreme in specifikacija za njegovo ponovno uporabo (IEC 60480:2004)

General Information

Status
Withdrawn
Publication Date
15-Dec-2004
Withdrawal Date
31-Oct-2007
Current Stage
9960 - Withdrawal effective - Withdrawal
Start Date
09-May-2022
Completion Date
09-May-2022

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STANDARDSmernice za preverjanje in ravnanje z žveplovim heksafluoridom (SF6) iz električne opreme in specifikacija za njegovo ponovno uporabo (IEC 60480:2004)Guidelines for the checking and treatment of sulfur hexafluoride (SF6) taken from electrical equipment and specification for its re-use (IEC 60480:2004)©
Standard je založil in izdal Slovenski inštitut za standardizacijo. Razmnoževanje ali kopiranje celote ali delov tega dokumenta ni dovoljenoReferenčna številkaSIST EN 60480:2005(en)ICS29.040.20

EUROPEAN STANDARD
EN 60480 NORME EUROPÉENNE EUROPÄISCHE NORM
December 2004 CENELEC European Committee for Electrotechnical Standardization Comité Européen de Normalisation Electrotechnique Europäisches Komitee für Elektrotechnische Normung
Central Secretariat: rue de Stassart 35, B - 1050 Brussels
© 2004 CENELEC - All rights of exploitation in any form and by any means reserved worldwide for CENELEC members.
Ref. No. EN 60480:2004 E
ICS 29.040.20; 29.130
English version
Guidelines for the checking and treatment of sulphur hexafluoride (SF6) taken from electrical equipment and specification for its re-use (IEC 60480:2004)
Lignes directrices relatives au contrôle
et au traitement de l'hexafluorure
de soufre (SF6) prélevé sur le matériel électrique et spécification en vue
de sa réutilisation (CEI 60480:2004)
Richtlinien für die Prüfung und Aufbereitung von Schwefelhexafluorid (SF6) nach Entnahme aus elektrischen Betriebsmitteln und Spezifikation für dessen Wiederverwendung (IEC 60480:2004)
This European Standard was approved by CENELEC on 2004-11-01. CENELEC members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration.
Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the Central Secretariat or to any CENELEC member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CENELEC member into its own language and notified to the Central Secretariat has the same status as the official versions.
CENELEC members are the national electrotechnical committees of Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.

at national level by publication of an identical
national standard or by endorsement
(dop)
2005-08-01 – latest date by which the national standards conflicting
with the EN have to be withdrawn
(dow)
2007-11-01 Annex ZA has been added by CENELEC. __________ Endorsement notice The text of the International Standard IEC 60480:2004 was approved by CENELEC as a European Standard without any modification. In the official version, for Bibliography, the following note has to be added for the standard indicated:
ISO 14040 NOTE Harmonized as EN ISO 14040:1997 (not modified). __________

- 3 - EN 60480:2004
Annex ZA
(normative)
Normative references to international publications
with their corresponding European publications The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. NOTE Where an international publication has been modified by common modifications, indicated by (mod), the relevant EN/HD applies. Publication Year Title EN/HD Year IEC 60050-191 1990 International Electrotechnical Vocabulary (IEV) Chapter 191: Dependability and quality of service
- - IEC 60050-212 1990 Chapter 212: Insulating solids, liquids and gases
- - IEC 60050-441 1984 Chapter 441: Switchgear, controlgear and fuses
- - IEC 60050-826 1982 Chapter 826: Electrical installations of buildings
- - IEC 60376 1971 Specification and acceptance of new sulphur hexafluoride
- - IEC 60376A 1973 First supplement - Section Thirteen: Mineral oil content
- - IEC 60376B 1974 Second supplement - Clause 26
- - IEC 60694 1996 Common specifications for high-voltage switchgear and controlgear standards
EN 60694 + Corr. May 1996 1999 IEC 61634 1995 High-voltage switchgear and controlgear – Use and handling of sulfur hexafluoride (SF6) in high-voltage switchgear and controlgear
- -
NORME INTERNATIONALECEIIEC INTERNATIONAL STANDARD 60480Deuxième éditionSecond edition2004-10 Lignes directrices relatives au contrôle et au traitement de l'hexafluorure de soufre (SF6) prélevé sur le matériel électrique et spécification en vue de sa réutilisation
Guidelines for the checking and treatment of sulfur hexafluoride (SF6) taken from electrical equipment and specification for its re-use
Pour prix, voir catalogue en vigueur For price, see current catalogue IEC 2004
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Copyright - all rights reserved Aucune partie de cette publication ne peut être reproduite ni utilisée sous quelque forme que ce soit et par aucun procédé, électronique ou mécanique, y compris la photocopie et les microfilms, sans l'accord écrit de l'éditeur. No part of this publication may be reproduced or utilized in any form or by any means, electronic or mechanical, including photocopying and microfilm, without permission in writing from the publisher. International Electrotechnical Commission,
3, rue de Varembé, PO Box 131, CH-1211 Geneva 20, SwitzerlandTelephone: +41 22 919 02 11 Telefax: +41 22 919 03 00 E-mail: inmail@iec.ch
Web: www.iec.ch CODE PRIX PRICE CODE V Commission Electrotechnique InternationaleInternational Electrotechnical Commission

60480  IEC:2004 – 3 –
CONTENTS FOREWORD.7 INTRODUCTION.11
1 Scope.13 2 Normative references.13 3 Terms and definitions.15 3.1 General terms.15 3.2 Material aspects.15 3.3 Environmental aspects.17 4 Typical applications of SF6.19 5 Impurities and their sources.19 5.1 Introductory remark.19 5.2 Impurities from handling and in service.19 5.3 Impurities in equipment having only an insulating function.19 5.4 Impurities in switching equipment.19 5.5 Impurities from internal arcs.21 6 Environmental aspects.21 6.1 Introductory remark.21 6.2 Impact on the ecosystem.21 6.3 Ozone depletion.21 6.4 Greenhouse effect.21 6.5 Decomposition products.21 6.6 Conclusion.21 7 Health and safety.23 7.1 Introductory remark.23 7.2 Precautions necessary with SF6.23 7.3 Necessary precautions with used SF6.23 7.4 Health considerations.25 8 Quality specification for re-use of SF6 in new or existing switchgear.25 8.1 Decision flowchart for SF6 removed from electrical equipment for treatment.25 8.2 Maximum acceptable impurity levels for re-use of SF6.29 9 Analytical methods for SF6 and their significance.29 9.1 General.29 9.2 On-site analysis.31 9.3 Laboratory analysis.33 10 Handling, storage and transportation.35 10.1 Introductory remark.35 10.2 Gas handling equipment.35 10.3 General safety requirements.35 10.4 Condition of the SF6 in an enclosure.37 10.5 Removing used SF6 from an enclosure.39 10.6 Storage and transportation of used SF6.39

60480  IEC:2004 – 5 –
Annex A (informative) Derivation of maximum tolerable moisture levels for re-use.41 Annex B (informative) Description of the different methods of analysis (on-site and laboratory).45 Annex C (informative) Reclaiming recommendations and procedures on-site.61
Bibliography.67
Figure 1 – Decision flow chart for the destination of removed SF6.27 Figure 2 – Decision flow chart for on-site analysis.31 Figure A.1 – Moisture levels (ppmv) as a function of gas pressure p.41 Figure B.1 – SF6 gas sampling set-up: evacuation.45 Figure B.2 – SF6 gas sampling set-up: purging.47 Figure B.3 – Typical gas chromatogram of decomposed SF6.53 (analysis performed with a Porapak Q column).53 Figure B.4 – IR spectrum of contaminated SF6.59
Table 1 – Origin of SF6 impurities.19 Table 2 – Maximum acceptable impurity levels.29 Table 3 – On-site methods.33 Table 4 – Laboratory methods.33 Table B.1 – Thermal conductivity detector relative response factor.55 Table B.2 – Peak absorption of SF6 and contaminants.59 Table C.1 – Suggested reclaiming operations.61 Table C.2 – Typical adsorbents for various SF6 impurities.63 Table C.3 – Summary of SF6 transportation regulations.65

60480  IEC:2004 – 7 –
INTERNATIONAL ELECTROTECHNICAL COMMISSION ____________
GUIDELINES FOR THE CHECKING AND TREATMENT OF SULFUR HEXAFLUORIDE (SF6) TAKEN FROM ELECTRICAL EQUIPMENT AND SPECIFICATION FOR ITS RE-USE
FOREWORD 1) The International Electrotechnical Commission (IEC) is a worldwide organization for standardization comprising all national electrotechnical committees (IEC National Committees). The object of IEC is to promote international co-operation on all questions concerning standardization in the electrical and electronic fields. To this end and in addition to other activities, IEC publishes International Standards, Technical Specifications, Technical Reports, Publicly Available Specifications (PAS) and Guides (hereafter referred to as “IEC Publication(s)”). Their preparation is entrusted to technical committees; any IEC National Committee interested in the subject dealt with may participate in this preparatory work. International, governmental and non-governmental organizations liaising with the IEC also participate in this preparation. IEC collaborates closely with the International Organization for Standardization (ISO) in accordance with conditions determined by agreement between the two organizations. 2) The formal decisions or agreements of IEC on technical matters express, as nearl
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