EN ISO 13503-1:2011
(Main)Petroleum and natural gas industries - Completion fluids and materials - Part 1: Measurement of viscous properties of completion fluids (ISO 13503-1:2011)
Petroleum and natural gas industries - Completion fluids and materials - Part 1: Measurement of viscous properties of completion fluids (ISO 13503-1:2011)
2011-04-08 EMA: Draft for // final vote received in ISO/CS (see notification of 2011-04-05 in dataservice).
Erdöl- und Erdgasindustrie - Komplettierungsflüssigkeiten und Materialien - Teil 1: Messung der Fließeigenschaften von Komplettierungsflüssigkeiten (ISO 13503-1:2011)
Industries du pétrole et du gaz naturel - Fluides de complétion et matériaux - Partie 1: Mesurage des propriétés visqueuses des fluides de complétion (ISO 13503-1:2011)
L'ISO 13503-1:2011 fournit une méthodologie cohérente de détermination de la viscosité des fluides de complétion utilisés dans les industries du pétrole et du gaz naturel. Dans certains cas, des méthodes sont également fournies pour déterminer les propriétés rhéologiques d'un fluide.
Industrija za predelavo nafte in zemeljskega plina - Tekočine in materiali za zaključna dela - 1. del: Merjenje viskoznosti tekočin za zaključna dela (ISO 13503-1:2011)
Ta del ISO 13503 podaja dosledno metodologijo za določevanje viskoznosti tekočin za zaključna dela, ki se uporabljajo v industriji za predelavo nafte in zemeljskega plina. V nekaterih primerih so navedene tudi metode za določevanje reoloških lastnosti tekočine.
General Information
Relations
Standards Content (Sample)
SLOVENSKI STANDARD
01-januar-2012
1DGRPHãþD
SIST EN ISO 13503-1:2005
SIST EN ISO 13503-1:2005/AC:2008
,QGXVWULMD]DSUHGHODYRQDIWHLQ]HPHOMVNHJDSOLQD7HNRþLQHLQPDWHULDOL]D
]DNOMXþQDGHODGHO 0HUMHQMHYLVNR]QRVWLWHNRþLQ]D]DNOMXþQDGHOD ,62
Petroleum and natural gas industries - Completion fluids and materials - Part 1:
Measurement of viscous properties of completion fluids (ISO 13503-1:2011)
Erdöl- und Erdgasindustrie - Komplettierungsflüssigkeiten und Materialien - Teil 1:
Messung der Fließeigenschaften von Komplettierungsflüssigkeiten (ISO 13503-1:2011)
Industries du pétrole et du gaz naturel - Fluides de complétion et matériaux - Partie 1:
Mesurage des propriétés visqueuses des fluides de complétion (ISO 13503-1:2011)
Ta slovenski standard je istoveten z: EN ISO 13503-1:2011
ICS:
75.180.30 Oprema za merjenje Volumetric equipment and
prostornine in merjenje measurements
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.
EUROPEAN STANDARD
EN ISO 13503-1
NORME EUROPÉENNE
EUROPÄISCHE NORM
November 2011
ICS 75.100 Supersedes EN ISO 13503-1:2005
English Version
Petroleum and natural gas industries - Completion fluids and
materials - Part 1: Measurement of viscous properties of
completion fluids (ISO 13503-1:2011)
Industries du pétrole et du gaz naturel - Fluides de Erdöl- und Erdgasindustrie - Komplettierungsflüssigkeiten
complétion et matériaux - Partie 1: Mesurage des und Materialien - Teil 1: Messung der Fließeigenschaften
propriétés visqueuses des fluides de complétion (ISO von Komplettierungsflüssigkeiten (ISO 13503-1:2011)
13503-1:2011)
This European Standard was approved by CEN on 31 October 2011.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European
Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national
standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation
under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same
status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland,
Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
Management Centre: Avenue Marnix 17, B-1000 Brussels
© 2011 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 13503-1:2011: E
worldwide for CEN national Members.
Contents Page
Foreword .3
Foreword
This document (EN ISO 13503-1:2011) has been prepared by Technical Committee ISO/TC 67 "Materials,
equipment and offshore structures for petroleum, petrochemical and natural gas industries" in collaboration
with Technical Committee CEN/TC 12 “Materials, equipment and offshore structures for petroleum,
petrochemical and natural gas industries” the secretariat of which is held by AFNOR.
This European Standard shall be given the status of a national standard, either by publication of an identical
text or by endorsement, at the latest by May 2012, and conflicting national standards shall be withdrawn at the
latest by May 2012.
Attention is drawn to the possibility that some of the elements of this document may be the subject of patent
rights. CEN [and/or CENELEC] shall not be held responsible for identifying any or all such patent rights.
This document supersedes EN ISO 13503-1:2005.
According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following
countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech
Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia,
Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain,
Sweden, Switzerland and the United Kingdom.
Endorsement notice
The text of ISO 13503-1:2011 has been approved by CEN as a EN ISO 13503-1:2011 without any
modification.
INTERNATIONAL ISO
STANDARD 13503-1
Second edition
2011-11-01
Petroleum and natural gas industries —
Completion fluids and materials —
Part 1:
Measurement of viscous properties of
completion fluids
Industries du pétrole et du gaz naturel — Fluides de complétion et
matériaux — Partie 1: Mesurage des propriétés visqueuses des fluides
de complétion
Reference number
ISO 13503-1:2011(E)
©
ISO 2011
ISO 13503-1:2011(E)
© ISO 2011
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized in any form or by any means,
electronic or mechanical, including photocopying and microfilm, without permission in writing from either ISO at the address below or ISO’s
member body in the country of the requester.
ISO copyright office
Case postale 56 • CH-1211 Geneva 20
Tel. + 41 22 749 01 11
Fax + 41 22 749 09 47
E-mail copyright@iso.org
Web www.iso.org
Published in Switzerland
ii © ISO 2011 – All rights reserved
ISO 13503-1:2011(E)
Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Terms and definitions . 1
3 Measurement and precision . 2
4 Fluid preparation . 2
5 Fluid preparation using shear-history simulation (optional) . 3
5.1 General . 3
5.2 Requirements for proper shear-history simulation . 4
5.3 Conditions for sample delivery . 4
5.4 Conditions for standard shear-history simulation . 4
5.5 Operational considerations . 4
6 Instrument calibration . 4
7 Measurement procedures . 4
7.1 General . 4
7.2 Non-crosslinked fluids (see 2.6) . 5
7.3 Crosslinked polymer and surfactant fluids . 11
8 Calculation procedures .12
8.1 General concepts .12
8.2 Brief review of geometry-independent rheology versus nominal rheology .13
8.3 Limitations/problems that can produce erroneous results .14
8.4 Calculation method for concentric-cylinder viscometers .14
8.5 Calculations for optional shear-history simulation .16
9 Test report .18
Bibliography .20
© ISO 2011 – All rights reserved iii
ISO 13503-1:2011(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies
(ISO member bodies). The work of preparing International Standards is normally carried out through ISO
technical committees. Each member body interested in a subject for which a technical committee has been
established has the right to be represented on that committee. International organizations, governmental and
non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International
Electrotechnical Commission (IEC) on all matters of electrotechnical standardization.
International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2.
The main task of technical committees is to prepare International Standards. Draft International Standards
adopted by the technical committees are circulated to the member bodies for voting. Publication as an
International Standard requires approval by at least 75 % of the member bodies casting a vote.
Attention is drawn to the possibility that some of the elements of this document may be the subject of patent
rights. ISO shall not be held responsible for identifying any or all such patent rights.
ISO 13503-1 was prepared by Technical Committee ISO/TC 67, Materials, equipment and offshore structures
for petroleum, petrochemical and natural gas industries, Subcommittee SC 3, Drilling and completion fluids,
and well cements.
This second edition cancels and replaces the first edition (ISO 13503-1:2003), which has been technically
revised. It also incorporates the Technical Corrigendum ISO 13503-1:2003/Cor.1:2005.
ISO 13503 consists of the following parts, under the general title Petroleum and natural gas industries —
Completion fluids and materials:
— Part 1: Measurement of viscous properties of completion fluids
— Part 2: Measurement of properties of proppants used in hydraulic fracturing and gravel-packing operations
— Part 3: Testing of heavy brines
— Part 4: Procedure for measuring stimulation and gravel-pack fluid leakoff under static conditions
— Part 5: Procedures for measuring the long-term conductivity of proppants
— Part 6: Procedure for measuring leakoff of completion fluids under dynamic conditions
iv © ISO 2011 – All rights reserved
ISO 13503-1:2011(E)
Introduction
For the purposes of this part of ISO 13503, completion fluids are defined as viscosified treating fluids used
during the completion or workover of a petroleum- or natural-gas-producing well. The objective of this part
of ISO 13503 is to provide a standard procedure for measuring the viscous properties of single-phase, non-
particulate-laden completion fluids. These fluids are viscosified brines, gravel-pack carrier fluids, and fracturing
fluids. These fluids can be either crosslinked or non-crosslinked (aqueous, hydrocarbon- or acid-based).
An optional shear-history simulation procedure is provided for fluids that are potentially shear-sensitive.
This procedure is designed to simulate the shearing effects experienced by a fluid in surface apparatus and
during the time it is being conveyed down the wellbore. Shear-history simulation is most often used during the
development of new fracturing fluids to characterize their sensitivity to shear.
These standard procedures were compiled on the basis of several years of comparative testing, debate,
discussion, and continued research by the industry.
This standard procedure is largely based on API RP 13M, first edition, July 2004.
In this part of ISO 13503, where practical, US Customary units (USC) are included in parentheses for
convenience.
© ISO 2011 – All rights reserved v
INTERNATIONAL STANDARD ISO 13503-1:2011(E)
Petroleum and natural gas industries — Completion fluids and
materials —
Part 1:
Measurement of viscous properties of completion fluids
1 Scope
This part of ISO 13503 provides consistent methodology for determining the viscosity of completion fluids used
in the petroleum and natural
...
SLOVENSKI STANDARD
01-januar-2012
Nadomešča:
SIST EN ISO 13503-1:2005
SIST EN ISO 13503-1:2005/AC:2008
Industrija za predelavo nafte in zemeljskega plina - Tekočine in materiali za
zaključna dela - 1. del: Merjenje viskoznosti tekočin za zaključna dela (ISO 13503-
1:2011)
Petroleum and natural gas industries - Completion fluids and materials - Part 1:
Measurement of viscous properties of completion fluids (ISO 13503-1:2011)
Erdöl- und Erdgasindustrie - Komplettierungsflüssigkeiten und Materialien - Teil 1:
Messung der Fließeigenschaften von Komplettierungsflüssigkeiten (ISO 13503-1:2011)
Industries du pétrole et du gaz naturel - Fluides de complétion et matériaux - Partie 1:
Mesurage des propriétés visqueuses des fluides de complétion (ISO 13503-1:2011)
Ta slovenski standard je istoveten z: EN ISO 13503-1:2011
ICS:
75.100 Maziva Lubricants, industrial oils and
related products
75.180.30 Oprema za merjenje Volumetric equipment and
prostornine in merjenje measurements
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.
EUROPEAN STANDARD
EN ISO 13503-1
NORME EUROPÉENNE
EUROPÄISCHE NORM
November 2011
ICS 75.100 Supersedes EN ISO 13503-1:2005
English Version
Petroleum and natural gas industries - Completion fluids and
materials - Part 1: Measurement of viscous properties of
completion fluids (ISO 13503-1:2011)
Industries du pétrole et du gaz naturel - Fluides de Erdöl- und Erdgasindustrie - Komplettierungsflüssigkeiten
complétion et matériaux - Partie 1: Mesurage des und Materialien - Teil 1: Messung der Fließeigenschaften
propriétés visqueuses des fluides de complétion (ISO von Komplettierungsflüssigkeiten (ISO 13503-1:2011)
13503-1:2011)
This European Standard was approved by CEN on 31 October 2011.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European
Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national
standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation
under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same
status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland,
Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
Management Centre: Avenue Marnix 17, B-1000 Brussels
© 2011 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 13503-1:2011: E
worldwide for CEN national Members.
Contents Page
Foreword .3
Foreword
This document (EN ISO 13503-1:2011) has been prepared by Technical Committee ISO/TC 67 "Materials,
equipment and offshore structures for petroleum, petrochemical and natural gas industries" in collaboration
with Technical Committee CEN/TC 12 “Materials, equipment and offshore structures for petroleum,
petrochemical and natural gas industries” the secretariat of which is held by AFNOR.
This European Standard shall be given the status of a national standard, either by publication of an identical
text or by endorsement, at the latest by May 2012, and conflicting national standards shall be withdrawn at the
latest by May 2012.
Attention is drawn to the possibility that some of the elements of this document may be the subject of patent
rights. CEN [and/or CENELEC] shall not be held responsible for identifying any or all such patent rights.
This document supersedes EN ISO 13503-1:2005.
According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following
countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech
Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia,
Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain,
Sweden, Switzerland and the United Kingdom.
Endorsement notice
The text of ISO 13503-1:2011 has been approved by CEN as a EN ISO 13503-1:2011 without any
modification.
INTERNATIONAL ISO
STANDARD 13503-1
Second edition
2011-11-01
Petroleum and natural gas industries —
Completion fluids and materials —
Part 1:
Measurement of viscous properties of
completion fluids
Industries du pétrole et du gaz naturel — Fluides de complétion et
matériaux — Partie 1: Mesurage des propriétés visqueuses des fluides
de complétion
Reference number
ISO 13503-1:2011(E)
©
ISO 2011
ISO 13503-1:2011(E)
© ISO 2011
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized in any form or by any means,
electronic or mechanical, including photocopying and microfilm, without permission in writing from either ISO at the address below or ISO’s
member body in the country of the requester.
ISO copyright office
Case postale 56 • CH-1211 Geneva 20
Tel. + 41 22 749 01 11
Fax + 41 22 749 09 47
E-mail copyright@iso.org
Web www.iso.org
Published in Switzerland
ii © ISO 2011 – All rights reserved
ISO 13503-1:2011(E)
Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Terms and definitions . 1
3 Measurement and precision . 2
4 Fluid preparation . 2
5 Fluid preparation using shear-history simulation (optional) . 3
5.1 General . 3
5.2 Requirements for proper shear-history simulation . 4
5.3 Conditions for sample delivery . 4
5.4 Conditions for standard shear-history simulation . 4
5.5 Operational considerations . 4
6 Instrument calibration . 4
7 Measurement procedures . 4
7.1 General . 4
7.2 Non-crosslinked fluids (see 2.6) . 5
7.3 Crosslinked polymer and surfactant fluids . 11
8 Calculation procedures .12
8.1 General concepts .12
8.2 Brief review of geometry-independent rheology versus nominal rheology .13
8.3 Limitations/problems that can produce erroneous results .14
8.4 Calculation method for concentric-cylinder viscometers .14
8.5 Calculations for optional shear-history simulation .16
9 Test report .18
Bibliography .20
© ISO 2011 – All rights reserved iii
ISO 13503-1:2011(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies
(ISO member bodies). The work of preparing International Standards is normally carried out through ISO
technical committees. Each member body interested in a subject for which a technical committee has been
established has the right to be represented on that committee. International organizations, governmental and
non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International
Electrotechnical Commission (IEC) on all matters of electrotechnical standardization.
International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2.
The main task of technical committees is to prepare International Standards. Draft International Standards
adopted by the technical committees are circulated to the member bodies for voting. Publication as an
International Standard requires approval by at least 75 % of the member bodies casting a vote.
Attention is drawn to the possibility that some of the elements of this document may be the subject of patent
rights. ISO shall not be held responsible for identifying any or all such patent rights.
ISO 13503-1 was prepared by Technical Committee ISO/TC 67, Materials, equipment and offshore structures
for petroleum, petrochemical and natural gas industries, Subcommittee SC 3, Drilling and completion fluids,
and well cements.
This second edition cancels and replaces the first edition (ISO 13503-1:2003), which has been technically
revised. It also incorporates the Technical Corrigendum ISO 13503-1:2003/Cor.1:2005.
ISO 13503 consists of the following parts, under the general title Petroleum and natural gas industries —
Completion fluids and materials:
— Part 1: Measurement of viscous properties of completion fluids
— Part 2: Measurement of properties of proppants used in hydraulic fracturing and gravel-packing operations
— Part 3: Testing of heavy brines
— Part 4: Procedure for measuring stimulation and gravel-pack fluid leakoff under static conditions
— Part 5: Procedures for measuring the long-term conductivity of proppants
— Part 6: Procedure for measuring leakoff of completion fluids under dynamic conditions
iv © ISO 2011 – All rights reserved
ISO 13503-1:2011(E)
Introduction
For the purposes of this part of ISO 13503, completion fluids are defined as viscosified treating fluids used
during the completion or workover of a petroleum- or natural-gas-producing well. The objective of this part
of ISO 13503 is to provide a standard procedure for measuring the viscous properties of single-phase, non-
particulate-laden completion fluids. These fluids are viscosified brines, gravel-pack carrier fluids, and fracturing
fluids. These fluids can be either crosslinked or non-crosslinked (aqueous, hydrocarbon- or acid-based).
An optional shear-history simulation procedure is provided for fluids that are potentially shear-sensitive.
This procedure is designed to simulate the shearing effects experienced by a fluid in surface apparatus and
during the time it is being conveyed down the wellbore. Shear-history simulation is most often used during the
development of new fracturing fluids to characterize their sensitivity to shear.
These standard procedures were compiled on the basis of several years of comparative testing, debate,
discussion, and continued research by the industry.
This standard procedure is largely based on API RP 13M, first edition, July 2004.
In this part of ISO 13503, where practical, US Customary units (USC) are included in parentheses for
convenience.
© ISO 2011 – All rights reserved v
INTERNATIONAL STANDARD ISO 13503-1:2011(E)
Petroleum and natural gas industries — Completion fluids and
materials —
Part 1:
Measurement of viscous properties of completion fluids
1 Scope
This part of ISO 13503 provides consistent methodology for determining the viscosity of completion
...
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