EN 13130-7:2004

Materials and articles in contact with foodstuffs - Plastics substances subject to limitation - Part 7: Determination of monoethylene glycol and diethylene glycol in food simulants

This part of this European Standard specifies methods for the determination of monoethylene glycol and diethylene glycol in the food simulants; water, 3 % w/v acetic acid, 15 % v/v ethanol and olive oil and other fatty food simulants, simulants D, e.g. a mixture of synthetic triglycerides or sunflower oil or corn oil.  The methods are capable of determining monoethylene glycol and diethylene glycol in food simulants separately, or combined, at the specific migration limit SML (T) of 30 mg/kg.
NOTE   This method was developed for the determination of monoethylene glycol and diethylene glycol in 15 % v/v aqueous ethanol, as required by the regulations in force at the time the development work was carried out.  However, this method, developed for 15 (v/v) aqueous ethanol, should be applicable to the determination in 10 (v/v) aqueous ethanol.

Werkstoffe und Gegenstände in Kontakt mit Lebensmitteln - Substanzen in Kunststoffen, die Beschränkungen unterliegen - Teil 7: Bestimmung von Monoethylenglycol und Diethylenglycol in Prüflebensmitteln

Matériaux et objets en contact avec les denrées alimentaires - Substances dans les matières plastiques soumises à des limitations - Partie 7 : Détermination du monoéthylène glycol et du diéthylène glycol dans les simulants d'aliments

La présente partie de cette Norme européenne spécifie les méthodes de détermination du monoéthylène glycol et du diéthylène glycol dans les simulants d'aliments : eau, acide acétique à 3 % (m/v), éthanol à 15 % (v/v) et huile d'olive et autres simulants alimentaires gras, simulants D (mélange de triglycérides synthétiques, huile de tournesol ou huile de maïs par exemple). Ces méthodes permettent de déterminer séparément ou en association, le monoéthylène glycol et le diéthylène glycol dans les simulants alimentaires, à la limite de migration spécifique LMS (T) de 30 mg/kg.
NOTE   Cette méthode a été élaborée pour déterminer la quantité de monoéthylène glycol et de diéthylène glycol dans de l'éthanol aqueux à 15 % (v/v), comme exigé par les réglementations en vigueur au moment où le travail de mise au point a été effectué. Cependant, cette méthode, élaborée pour de l'éthanol aqueux à 15 % (v/v), devrait pouvoir s'appliquer à la détermination dans de l'éthanol aqueux à 10 % (v/v).

Materiali in predmeti v stiku z živili - Snovi v polimernih materialih, katerih koncentracija je omejena - 7. del: Določevanje monoetilenglikola in dietilenglikola v modelnih raztopinah za živila

General Information

• Status: Published
• Publication Date: 25-May-2004
• Withdrawal Date: 29-Nov-2004
• ICS: 67.250 - Materials and articles in contact with foodstuffs
• Technical Committee: CEN/TC 194 - Utensils in contact with food
• Drafting Committee: CEN/TC 194/SC 1/WG 2 - Methods of test for monomers
• Current Stage: 9092 - Decision on results of review/2YR ENQ - revise - Review Enquiry
• Completion Date: 10-Apr-2018
• Directive: 89/109/EEC - Materials and articles intended to come into contact with foodstuffs
• Mandate: M/052 - Standardization mandate to CEN concerning methods of analysis for materials and articles intended to come into contact with foodstuffs
• Ref Project: SIST EN 13130-7:2004 - Materials and articles in contact with foodstuffs - Plastics substances subject to limitation - Part 7: Determination of monoethylene glycol and diethylene glycol in food simulants

Relations

• Replaces: ENV 13130-7:1999 - Materials and articles in contact with foodstuffs - Plastics substances subject to limitation - Part 7: Determination of monoethylene glycol and diethylene glycol in food simulants
• Effective Date: 22-Dec-2008

Standards Content (Sample)

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Werkstoffe und Gegenstände in Kontakt mit Lebensmitteln - Substanzen in Kunststoffen, die Beschränkungen unterliegen - Teil 7: Bestimmung von Monoethylenglycol und Diethylenglycol in PrüflebensmittelnMatériaux et objets en contact avec les denrées alimentaires - Substances dans les matieres plastiques soumises a des limitations - Partie 7 : Détermination du monoéthylene glycol et du diéthylene glycol dans les simulants d'alimentsMaterials and articles in contact with foodstuffs - Plastics substances subject to limitation - Part 7: Determination of monoethylene glycol and diethylene glycol in food simulants67.250Materiali in predmeti v stiku z živiliMaterials and articles in contact with foodstuffsICS:Ta slovenski standard je istoveten z:EN 13130-7:2004SIST EN 13130-7:2004en,fr,de01-september-2004SIST EN 13130-7:2004SLOVENSKI
STANDARDSIST ENV 13130-7:20001DGRPHãþD

EUROPEAN STANDARDNORME EUROPÉENNEEUROPÄISCHE NORMEN 13130-7May 2004ICS 67.250English versionMaterials and articles in contact with foodstuffs - Plasticssubstances subject to limitation - Part 7: Determination ofmonoethylene glycol and diethylene glycol in food simulantsMatériaux et objets en contact avec les denréesalimentaires - Substances dans les matières plastiquessoumises à des limitations - Partie 7 : Détermination dumonoéthylène glycol et du diéthylène glycol dans lessimulants d'alimentsWerkstoffe und Gegenstände in Kontakt mit Lebensmitteln- Substanzen in Kunststoffen, die Beschränkungenunterliegen - Teil 7: Bestimmung von Monoethylenglykolund Diethylenglykol in Lebensmittel-SimulantienThis European Standard was approved by CEN on 24 March 2004.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained on application to the Central Secretariat or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its own language and notified to the Central Secretariat has the same status as the officialversions.CEN members are the national standards bodies of Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France,Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Slovakia,Slovenia, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMITÉ EUROPÉEN DE NORMALISATIONEUROPÄISCHES KOMITEE FÜR NORMUNGManagement Centre: rue de Stassart, 36
B-1050 Brussels© 2004 CENAll rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN 13130-7:2004: ESIST EN 13130-7:2004

EN 13130 are as follows. Part 1: Guide to test methods for the specific migration of substances from plastics to foods and food simulants and the determination of substances in plastics and the selection of conditions of exposure to food simulants Part 2: Determination of terephthalic acid in food simulants Part 3: Determination of acrylonitrile in food and food simulants Part 4: Determination of 1,3-butadiene in plastics
Part 5: Determination of vinylidene chloride in food simulants Part 6: Determination of vinylidene chloride in plastics Part 8: Determination of isocyanates in plastics Part 9: Determination of acetic acid, vinyl ester in food simulants Part 10: Determination of acrylamide in food simulants
Part 11: Determination of 11-aminoundecanoic acid in food simulants
Part 12: Determination of 1,3-benzenedimethanamine in food simulants Part 13: Determination of 2,2-bis(4-hydroxyphenyl)propane (Bisphenol A) in food simulants Part 14: Determination of 3,3-bis(3-methyl-4-hydroxyphenyl)-2-indoline in food simulants SIST EN 13130-7:2004

Part 16: Determination of caprolactam and caprolactam salt in food simulants Part 17: Determination of carbonyl chloride in plastics
Part 18: Determination of 1,2-dihydroxybenzene, 1,3- dihydroxybenzene, 1,4- dihydroxybenzene, 4,4’-dihydroxybenzophenone and 4,4’dihydroxybiphenyl in food simulants Part 19: Determination of dimethylaminoethanol in food simulants Part 20: Determination of epichlorohydrin in plastics Part 21: Determination of ethylenediamine and hexamethylenediamine in food simulants Part 22: Determination of ethylene oxide and propylene oxide in plastics Part 23: Determination of formaldehyde and hexamethylenetetramine in food simulants Part 24: Determination of maleic acid and maleic anhydride in food simulants Part 25: Determination of 4-methyl-pentene in food simulants Part 26: Determination of 1-octene and tetrahydrofuran in food simulants Part 27: Determination of 2,4,6-triamino-1,3,5-triazine in food simulants Part 28: Determination of 1,1,1-trimethylopropane in food simulants
Parts 1 to 8 are European Standards.
Parts 9 to 28 are Technical Specifications, prepared within the Standards, Measurement and Testing project, MAT1-CT92-0006, “Development of Methods of Analysis for Monomers”. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom. SIST EN 13130-7:2004

Residues of monoethylene glycol and diethylene glycol can remain in the plastic after processing to form materials and articles for food contact use, and can migrate into foodstuffs.
NOTE Commission Directive 2002/72/EC lists a combined specific migration limit of 30 mg/kg (T) of monoethylene glycol and diethylene glycol in foods or food simulants.
1 Scope This part of this European Standard specifies methods for the determination of monoethylene glycol and diethylene glycol in the food simulants; water, 3 % (w/v) acetic acid, 15 % (v/v) ethanol and olive oil and other fatty food simulants, simulants D, e.g. a mixture of synthetic triglycerides or sunflower oil or corn oil.
The methods are capable of determining monoethylene glycol and diethylene glycol in food simulants separately, or combined, at the specific migration limit SML (T) of 30 mg/kg.
NOTE This method was developed for the determination of monoethylene glycol and diethylene glycol in 15 % (v/v) aqueous ethanol, as required by the regulations in force at the time the development work was carried out.
However, this method, developed for 15 (v/v) aqueous ethanol, should be applicable to the determination in 10 (v/v) aqueous ethanol. 2 Normative references This European Standard incorporates by dated or undated reference, provisions from other publications.
These normative references are cited at the appropriate places in the text, and the publications are listed hereafter.
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