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CEN

EN 13999-1:2006

(Main)

Adhesives - Short term method for measuring the emission properties of low-solvent or solvent-free adhesives after application - Part 1: General procedure

Adhesives - Short term method for measuring the emission properties of low-solvent or solvent-free adhesives after application - Part 1: General procedure

This European Standard describes a conventional standard method for assessing potential emissions from adhesives after their application.
This European Standard applies only to "solvent-free" and "low-solvent" adhesives as they are defined in EN 923. The adhesives shall be applicable at room temperature.

Klebstoffe - Kurzzeit-Verfahren zum Messen der Emissionseigenschaften von lösemittelarmen oder lösemittelfreien Klebstoffen nach der Applikation - Teil 1: Allgemeines Verfahren

Diese Europäische Norm beschreibt ein Konventionsverfahren zur Beurteilung potentieller Emissionen aus
Klebstoffen nach deren Applikation.
Diese Norm gilt nur für 'lösemittelfreie' und 'lösemittelarme' Klebstoffe entsprechend deren Definition in
EN 923. Die Klebstoffe müssen bei Raumtemperatur anwendbar sein.

Adhésifs - Méthode de mesurage rapide des caractéristiques émissives des adhésifs à teneur faible ou nulle en solvant après application - Partie 1 : Mode opératoire général

La présente Norme Européenne décrit une méthode normalisée conventionnelle permettant d’évaluer les
émissions potentielles provenant des adhésifs après leur application.
La présente Norme Européenne n’est applicable qu’aux adhésifs « sans solvant » et aux adhésifs « à faible
teneur en solvant », tels que définis dans l’EN 923. Les adhésifs doivent être applicables à la température
ambiante.

Lepila - Hitra metoda za merjenje emisijskih lastnosti lepil z malo topila ali brez njega po uporabi - 1. del: Splošni postopek

General Information

Status
Withdrawn
Publication Date
29-Aug-2006
Withdrawal Date
03-Dec-2013
ICS
83.180 - Adhesives
Technical Committee
CEN/TC 193 - Adhesives
Drafting Committee
CEN/TC 193/WG 1 - General terminology - General physical and chemical tests
Current Stage
9960 - Withdrawal effective - Withdrawal
Start Date
04-Dec-2013
Completion Date
04-Dec-2013
Ref Project
SIST EN 13999-1:2006 - Adhesives - Short term method for measuring the emission properties of low-solvent or solvent-free adhesives after application - Part 1: General procedure

Relations

Replaces
ENV 13999-1:2001 - Adhesives - Short term method for measuring the emission properties of low-solvent or solvent-free adhesives after application - Part 1: General procedure
Effective Date
22-Dec-2008
Replaced By
EN 13999-1:2013 - Adhesives - Short term method for measuring the emission properties of low-solvent or solvent-free adhesives after application - Part 1: General procedure
Effective Date
11-Dec-2013
Corrected By
EN 13999-1:2006/AC:2007 - Adhesives - Short term method for measuring the emission properties of low-solvent or solvent-free adhesives after application - Part 1: General procedure
Effective Date
08-Jun-2022

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2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Adhesives - Short term method for measuring the emission properties of low-solvent or solvent-free adhesives after application - Part 1: General procedureLepila - Hitra metoda za merjenje emisijskih lastnosti lepil z malo topila ali brez njega po uporabi - 1. del: Splošni postopekAdhésifs - Méthode de mesurage rapide des caractéristiques émissives des adhésifs a teneur faible ou nulle en solvant apres application - Partie 1 : Mode opératoire généralKlebstoffe - Kurzzeit-Verfahren zum Messen der Emissionseigenschaften von lösemittelarmen oder lösemittelfreien Klebstoffen nach der Applikation - Teil 1: Allgemeines VerfahrenTa slovenski standard je istoveten z:EN 13999-1:2006SIST EN 13999-1:2006en83.180LepilaAdhesivesICS:SIST ENV 13999-1:20021DGRPHãþDSLOVENSKI
STANDARDSIST EN 13999-1:200601-december-2006

EUROPEAN STANDARDNORME EUROPÉENNEEUROPÄISCHE NORMEN 13999-1August 2006ICS 83.180Supersedes ENV 13999-1:2001
English VersionAdhesives - Short term method for measuring the emissionproperties of low-solvent or solvent-free adhesives afterapplication - Part 1: General procedureAdhésifs - Méthode de mesurage rapide descaractéristiques émissives des adhésifs à teneur faible ounulle en solvant après application - Partie 1 : Modeopératoire généralKlebstoffe - Kurzzeit-Verfahren zum Messen derEmissionseigenschaften von lösemittelarmen oderlösemittelfreien Klebstoffen nach der Applikation - Teil 1:Allgemeines VerfahrenThis European Standard was approved by CEN on 1 August 2006.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained on application to the Central Secretariat or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its own language and notified to the Central Secretariat has the same status as the officialversions.CEN members are the national standards bodies of Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France,Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania,Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMITÉ EUROPÉEN DE NORMALISATIONEUROPÄISCHES KOMITEE FÜR NORMUNGManagement Centre: rue de Stassart, 36
B-1050 Brussels© 2006 CENAll rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN 13999-1:2006: E

The test shall: • be reliable and reproducible; • give results in a short time to be useful for decisions for development projects; • verify that carcinogenic or sensitising volatile substances are absent; • characterise the emission properties of the adhesive. This can be achieved by sampling the atmosphere around the applied adhesive kept in an environmental test chamber at controlled ambient conditions.

2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 923:2005, Adhesives — Terms and definitions EN 1067, Adhesives — Examination and preparation of samples for testing EN ISO 15605, Adhesives — Sampling (ISO 15605:2000) EN ISO 16000-9:2006, Indoor air — Part 9: Determination of the emission of volatile organic compounds from building products and furnishing — Emission test chamber method (ISO 16000-9:2006)
ENV 13999-2, Adhesives — Short term method for measuring the emission properties of low-solvent or solvent-free adhesives after application — Part 2: Determination of volatile organic compounds ENV 13999-3, Adhesives — Short term method for measuring the emission properties of low-solvent or solvent-free adhesives after application — Part 3:
Determination of volatile aldehydes ENV 13999-4, Adhesives — Short term method for measuring the emission properties of low-solvent or solvent-free adhesives after application — Part 4:
Determination of volatile diisocyanates ISO 554, Standard atmospheres for conditioning and / or testing — Specifications ISO 16000-6:2004, Indoor air —- Part 6: Determination of volatile organic compounds in indoor and test chamber air by active sampling on Tenax TA sorbent, thermal desorption and gas chromatography using MS/FID

specific cumulative emission
(SCE) total volatile organic compounds per unit of test area, emitted in a time interval between 24 h and 240 h after the start of the test 3.2
volatile organic compounds (VOC) organic compounds whose boiling point ranges from (50 °C to 100 °C) to (240 °C to 260 °C) and generally has a saturation pressure of 25 °C greater than 102 kPa 4 Principle The test determines the emissions of volatile organic substances from adhesive coatings. Very volatile and mainly particle bound compounds are not detected with the described procedures. The test is performed in an emission test chamber (Figure 1) at specified constant temperature, relative humidity, air mixing and air exchange. A measurement of the concentrations of the compounds of interest in the air of the exhaust pipe is considered representative of the air in the whole test chamber.
Sampling and analysis of the non-polar and slightly polar volatile organic compounds, as defined in ISO 16000-6, shall be carried out as described in ENV 13999-2. Sampling and analysis of the volatile aldehydes shall be carried out as described in ENV 13999-3. Sampling and analysis of the volatile isocyanates shall be carried out as described in ENV 13999-4. The test includes: • qualitative and quantitative determination of carcinogenic and sensitising substances in an early stage after the application of the adhesive sample; • determination of the VOC specific emission rate at three points of time, a determination of specific cumulative VOC emission in the interval between 24 h and 240 h. NOTE There are specific applications for which an emission test cell (as described in EN ISO 16000-10) may be easier to handle than the emission test chamber. In these cases it is possible to apply the procedures as given in this European Standard with the exception that a test cell is used instead of the test chamber. But, as the air flow rate across the sample is higher than with the chamber method, the results may only be used with supporting correlation data.
5 Apparatus The test apparatus shall be comprised of the following main components: support, air supply and mixing facilities, emission test chamber with monitoring and control systems, air sampling devices and devices for desorption and analysis. 5.1 Support
A stainless
...

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